2,6-Nonadienal, (E,Z)-


Normal alkane RI, polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase TC-WaxDB-WaxDB-WaxDB-WaxDB-Wax
Column length (m) 60.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.320.320.250.25
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 40.40. 60.60.
Tend (C) 230.230.240.200.200.
Heat rate (K/min) 3.6.6.8.8.
Initial hold (min) 3.2. 3.3.
Final hold (min)  20.5.9.59.5
I 1596.1606.1567.1598.1605.
ReferenceMiyazawa, Fujita, et al., 2010Chen, Song, et al., 2009Mallia, Escher, et al., 2009Rochat, Egger, et al., 2009Rochat, Egger, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxStabilwaxDB-WaxStabilwax
Column length (m) 30.30.30.60.60.
Carrier gas HeliumHeliumHelium Helium
Substrate      
Column diameter (mm) 0.250.250.250.350.25
Phase thickness (μm) 0.250.250.50 0.25
Tstart (C) 60.60.35.40.40.
Tend (C) 200.200.225.200.240.
Heat rate (K/min) 8.8.6.4.3.
Initial hold (min) 3.3.5. 5.
Final hold (min) 9.59.510. 10.
I 1607.1621.1587.1612.1585.
ReferenceRochat, Egger, et al., 2009Rochat, Egger, et al., 2009Watcharananun, Cadwallader, et al., 2009Ganeko, Shoda, et al., 2008Cros, Vandanjon, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Wax 52CBDB-Wax EtrDB-WaxHP-20MHP-Innowax
Column length (m) 60.60.15.50.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.250.320.20.32
Phase thickness (μm) 0.50.250.250.20.5
Tstart (C) 40.40.40.70.60.
Tend (C) 220.230.230.180.220.
Heat rate (K/min) 4.2.6.4.2.
Initial hold (min) 8.5. 4. 
Final hold (min) 20.100.20.15.10.
I 1596.1594.1571.1557.1589.
ReferencePovolo, Contarini, et al., 2007Ibarz, Ferreira, et al., 2006Kishimoto, Wanikawa, et al., 2006Mastelic, Jerkovic, et al., 2006Senger-Emonnot, Rochard, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase ZB-WaxInnowaxDB-WaxDB-WaxDB-Wax
Column length (m) 60.50.30.30.60.
Carrier gas HeHeHeH2H2
Substrate      
Column diameter (mm) 0.320.20.250.320.32
Phase thickness (μm) 0.50.50.250.50.25
Tstart (C) 40.60.40.40.40.
Tend (C) 250.250.210.200.230.
Heat rate (K/min) 3.2.5.4.4.
Initial hold (min) 2.  5.5.
Final hold (min) 10.60.  25.
I 1610.1587.1593.1605.1592.
ReferenceWierda R.L., Fletcher G., et al., 2006Bendimerad and Bendiab, 2005Kumazawa, Kubota, et al., 2005Culleré, Escudero, et al., 2004Dregus and Engel, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-FFAPDB-FFAPDB-FFAPBP-20DB-Wax
Column length (m) 30.30.30.50.30.
Carrier gas H2HeHeH2He
Substrate      
Column diameter (mm) 0.30.320.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 35.40.40.45.40.
Tend (C) 240.230.230.230.250.
Heat rate (K/min) 8.6.6.3.8.
Initial hold (min) 2.52.2.1.5.
Final hold (min) 2.10.10.10.5.
I 1578.1566.1566.1564.1611.
ReferenceTriqui and Bouchriti, 2003Czerny and Schieberle, 2002Czerny and Schieberle, 2002Darriet, Pons, et al., 2002Fu, Yoon, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxDB-WaxDB-WaxDB-Wax
Column length (m) 60.30.60.30.30.
Carrier gas HeHeHeHeH2
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (μm) 0.250.250.250.50.5
Tstart (C) 40.40.40.40.40.
Tend (C) 220.210.210.240.200.
Heat rate (K/min) 3.5.5.7.4.
Initial hold (min) 10.   5.
Final hold (min) 10.  5.60.
I 1582.1593.1590.1601.1599.
ReferenceHayata, Sakamoto, et al., 2002Kumazawa and Masuda, 2002Kumazawa and Masuda, 2002Lin, Rouseff, et al., 2002Aznar, López, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase EC-1000DB-WaxHP-FFAPDB-FFAPDB-Wax
Column length (m) 30.30.50.30.30.
Carrier gas HeH2 HeHe
Substrate      
Column diameter (mm) 0.250.320.320.320.25
Phase thickness (μm) 0.250.50.50.250.25
Tstart (C) 35.40.35.40.50.
Tend (C) 230.200.230.195.220.
Heat rate (K/min) 5.4.6.5.4.
Initial hold (min) 5.5. 5.3.
Final hold (min) 15.60.15.40. 
I 1595.1597.1584.1571.1582.
ReferenceBendall, 2001Ferreira, Aznar, et al., 2001Preininger and Ullrich, 2001Suriyaphan, Drake, et al., 2001Weckerle, Bastl-Borrmann, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax-10DB-WaxDB-WaxDB-WaxDB-Wax
Column length (m) 60.30.30.30.30.
Carrier gas He H2H2He
Substrate      
Column diameter (mm) 0.250.320.320.320.25
Phase thickness (μm) 0.250.250.50.50.25
Tstart (C) 35.40.60.60.50.
Tend (C) 200.280.245.245.240.
Heat rate (K/min) 4.8.3.3.4.
Initial hold (min) 10.5.3.3.3.
Final hold (min)  30.20.20.10.
I 1577.1596.1580.1580.1551.
ReferenceGirard and Durance, 2000Kim, Baek, et al., 2000Kotseridis and Baumes, 2000Kotseridis and Baumes, 2000Parada, Duque, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxInnowaxDB-WaxDB-WaxDB-Wax
Column length (m) 30.60.30.60.60.
Carrier gas HeHe  He
Substrate      
Column diameter (mm) 0.250.250.530.250.32
Phase thickness (μm) 0.250.251.0.250.5
Tstart (C) 50.60.40.40.34.
Tend (C) 240.220.210.210.200.
Heat rate (K/min) 4. 5.5.5.
Initial hold (min) 3.10.  3.
Final hold (min) 10.   10.
I 1576.1597.1598.1605.1627.
ReferenceParada, Duque, et al., 2000Kaya, Baser, et al., 1999Kumazawa and Masuda, 1999Kumazawa and Masuda, 1999Schlüter, Steinhart, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxHP-InnowaxHP-InnowaxInnowax
Column length (m) 60.60.25.25.30.
Carrier gas HeHe   
Substrate      
Column diameter (mm) 0.320.250.320.320.25
Phase thickness (μm) 0.250.25  0.25
Tstart (C) 34.40.35.35.40.
Tend (C) 200.200.250.250.240.
Heat rate (K/min) 5.2.4.4.6.
Initial hold (min) 3.2.  10.
Final hold (min) 10.   25.
I 1567.1580.1553.1553.1585.
ReferenceSchlüter, Steinhart, et al., 1999Umano, Nakahara, et al., 1999Ong and Acree, 1998Ong, Acree, et al., 1998Petersen, Poll, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxSupelcowax-10Carbowax 20MCarbowax 20MCarbowax 20M
Column length (m) 30.60.60.50.50.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.250.25   
Tstart (C) 50.40.60.60.60.
Tend (C) 240.200.180.180.180.
Heat rate (K/min) 6.3.2.2.2.
Initial hold (min) 3.3.4.4.4.
Final hold (min)  30.   
I 1561.1580.1555.1555.1555.
ReferenceHashizume and Samuta, 1997Wong and Lai, 1996Kawakami, Ganguly, et al., 1995Kawakami, Kobayashi, et al., 1993Kawakami and Kobayashi, 1991
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryPacked
Active phase Supelcowax-10Carbowax
Column length (m) 60.3.
Carrier gas HeHe
Substrate  Chromosorb G AW DMCS
Column diameter (mm) 0.25 
Phase thickness (μm) 0.25 
Tstart (C) 40.60.
Tend (C) 175.180.
Heat rate (K/min) 1.4.
Initial hold (min) 5. 
Final hold (min)   
I 1587.1575.
ReferenceHsieh, Williams, et al., 1989Schieberle and Grosch, 1983
Comment MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Miyazawa, Fujita, et al., 2010
Miyazawa, N.; Fujita, A.; Kubota, K., Aroma character impact compounds in Kinokuni Mandarin Orange (Citrus kinikuni) compared with Satsuma Mandarin Orange, Biosci. Biotechnol. Biochem., 2010, 74, 4, 835-842, https://doi.org/10.1271/bbb.90937 . [all data]

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Kumazawa, Kubota, et al., 2005
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Triqui and Bouchriti, 2003
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Fu, Yoon, et al., 2002
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Preininger and Ullrich, 2001
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Suriyaphan, Drake, et al., 2001
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Weckerle, Bastl-Borrmann, et al., 2001
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Girard and Durance, 2000
Girard, B.; Durance, T., Headspace volatiles of sockeye and pink salmon as affected by retort process, Food Chem. Toxicol., 2000, 65, 1, 34-39. [all data]

Kim, Baek, et al., 2000
Kim, D.S.; Baek, H.H.; Ahn, C.B.; Byun, D.S.; Jung, K.J.; Lee, H.G.; Cadwallader, K.R.; Kim, H.R., Development and characterization of a flavoring agent from oyster cooker effluent, J. Agric. Food Chem., 2000, 48, 10, 4839-4843, https://doi.org/10.1021/jf991096n . [all data]

Kotseridis and Baumes, 2000
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Parada, Duque, et al., 2000
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Kaya, Baser, et al., 1999
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Kumazawa and Masuda, 1999
Kumazawa, K.; Masuda, H., Identification of potent odorants in Japanese green tea (Sen-cha), J. Agric. Food Chem., 1999, 47, 12, 5169-5172, https://doi.org/10.1021/jf9906782 . [all data]

Schlüter, Steinhart, et al., 1999
Schlüter, S.; Steinhart, H.; Schwarz, F.J.; Kirchgessner, M., Changes in the odorants of boiled carp fillet (Cyprinus carpio L.) as affected by increasing methionine levels in feed, J. Agric. Food Chem., 1999, 47, 12, 5146-5150, https://doi.org/10.1021/jf9902604 . [all data]

Umano, Nakahara, et al., 1999
Umano, K.; Nakahara, K.; Shoji, A.; Shibamoto, T., Aroma chemicals isolated and identified from leaves of aloe arborescens Mill. Var. natalensis Berger, J. Agric. Food Chem., 1999, 47, 9, 3702-3705, https://doi.org/10.1021/jf990116i . [all data]

Ong and Acree, 1998
Ong, P.K.C.; Acree, T.E., Gas chromatography/olfactory analysis of lychee (Litchi chinesis Sonn.), J. Agric. Food Chem., 1998, 46, 6, 2282-2286, https://doi.org/10.1021/jf9801318 . [all data]

Ong, Acree, et al., 1998
Ong, P.K.C.; Acree, T.E.; Lavin, E.H., Characterization of volatiles in rambutan fruit (Nephelium lappaceum L.), J. Agric. Food Chem., 1998, 46, 2, 611-615, https://doi.org/10.1021/jf970665t . [all data]

Petersen, Poll, et al., 1998
Petersen, M.A.; Poll, L.; Larsen, L.M., Comparison of volatiles in raw and boiled potatoes using a mild extraction technique combined with GC odour profiling and GC-MS, Food Chem., 1998, 61, 4, 461-466, https://doi.org/10.1016/S0308-8146(97)00119-2 . [all data]

Hashizume and Samuta, 1997
Hashizume, K.; Samuta, T., Green odorants of grape cluster stem and their ability to cause a wine stemmy flavor, J. Agric. Food Chem., 1997, 45, 4, 1333-1337, https://doi.org/10.1021/jf960635a . [all data]

Wong and Lai, 1996
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Kawakami, Ganguly, et al., 1995
Kawakami, M.; Ganguly, S.N.; Banerjee, J.; Kobayashi, A., Aroma composition of oolong tea and black tea by brewed extraction method and characterizing compounds of Darjeeling tea aroma, J. Agric. Food Chem., 1995, 43, 1, 200-207, https://doi.org/10.1021/jf00049a037 . [all data]

Kawakami, Kobayashi, et al., 1993
Kawakami, M.; Kobayashi, A.; Kator, K., Volatile constituents of Rooibos tea (Aspalathus linearis) as affected by extraction process, J. Agric. Food Chem., 1993, 41, 4, 633-636, https://doi.org/10.1021/jf00028a023 . [all data]

Kawakami and Kobayashi, 1991
Kawakami, M.; Kobayashi, A., Volatitle constituents of greem mate and roasted mate, J. Agric. Food Chem., 1991, 39, 7, 1275-1279, https://doi.org/10.1021/jf00007a016 . [all data]

Hsieh, Williams, et al., 1989
Hsieh, T.C.Y.; Williams, S.S.; Vejaphan, W.; Meyers, S.P., Characterization of Volatile Components of Menhaden Fish (Brevoortia tyrannus) Oil, J. Amer. Oil Chem. Soc., 1989, 66, 1, 114-117, https://doi.org/10.1007/BF02661797 . [all data]

Schieberle and Grosch, 1983
Schieberle, P.; Grosch, W., Identifizierung von Aromastoffen aus der Kruste von Roggenbrot, Z. Lebensm. Unters. Forsch., 1983, 177, 3, 173-180, https://doi.org/10.1007/BF01146791 . [all data]


Notes

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