Stigmastanol, TMS derivative


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
Capillary5 % Phenyl methyl siloxane280.3348.Iida, Hikasaka, et al., 200125. m/0.32 mm/0.25 μm, He
Capillary5 % Phenyl methyl siloxane280.3349.Iida, Hikasaka, et al., 200125. m/0.32 mm/0.25 μm, He

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-5 MS3343.Radulovic and Dordevic, 201130. m/0.25 mm/0.25 μm, Helium, 5. K/min, 315. C @ 10. min; Tstart: 70. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-5 MS3349.Radulovic and Dordevic, 201130. m/0.25 mm/0.25 μm, Helium; Program: not specified

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Iida, Hikasaka, et al., 2001
Iida, T.; Hikasaka, M.; Goto, J.; Nambara, T., Capillary gas chromatographic behaviour of tert.-hydroxylated steroids by trialkylsilylation, J. Chromatogr. A, 2001, 937, 1-2, 97-105, https://doi.org/10.1016/S0021-9673(01)01305-X . [all data]

Radulovic and Dordevic, 2011
Radulovic, N.S.; Dordevic, N.D., Sterods from poison hemlock (Conium maculatum L.): a GC-MS analysis, J. Serb. Chem. Soc., 2011, 76, 11, 1471-1483, https://doi.org/10.2298/JSC110206128R . [all data]


Notes

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