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1H-Cycloprop[e]azulen-4-ol, decahydro-1,1,4,7-tetramethyl-, [1aR-(1a«alpha»,4«beta»,4a«beta»,7«alpha»,7a«beta»,7b«alpha»)]-


Van Den Dool and Kratz RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1CP-Sil PONA GBDB-5HP-5DB-5
Column length (m) 50.100.30.30.30.
Carrier gas HeHeHeN2 
Substrate      
Column diameter (mm) 0.220.250.250.250.22
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.140.60.60.60.
Tend (C) 220.230.240.220.240.
Heat rate (K/min) 2.5.3.5.3.
Initial hold (min)  10. 10.2.
Final hold (min) 20.25.   
I 1594.1636.1592.1590.1590.
ReferenceBoti, Koukoua, et al., 2007Cunicao, Lopes, et al., 2007Flamini, Cioni, et al., 2007Flamini, Tebano, et al., 2007Martins, Santos, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Methyl SiliconeRTX-1HP-5MSDB-5DB-5
Column length (m) 30.60.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.220.250.220.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 80.60.60.55.60.
Tend (C) 220.230.280.240.240.
Heat rate (K/min) 2.2.4.3.3.
Initial hold (min)   5.2. 
Final hold (min) 15.35. 15. 
I 1585.1588.1589.1589.1590.
ReferenceMelo, Corrêa, et al., 2007Paolini, Muselli, et al., 2007Saroglou, Marin, et al., 2007Silva, Barbosa, et al., 2007Telascrea, de Araujo, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5HP-5MSHP-5MSHP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.50.60.60.60.
Tend (C) 280.250.280.280.220.
Heat rate (K/min) 3.3.3.3.5.
Initial hold (min)     10.
Final hold (min)  10.   
I 1589.1590.1569.1588.1596.
ReferenceVagionas, Ngassapa, et al., 2007Yu, Liao, et al., 2007Basta, Tzakou, et al., 2006Chorianopoulos N., Evergets E., et al., 2006Flamini, Tebano, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5SPB-1HP-5SPB-1
Column length (m) 30.30.30.25.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (mum) 0.250.250.250.250.2
Tstart (C) 60.60.50.60.70.
Tend (C) 250.260.250.240.220.
Heat rate (K/min) 3.3.5.4.3.
Initial hold (min)   3.  
Final hold (min)   15. 15.
I 1594.1592.1603.1589.1572.
ReferenceJavidnia, Miri, et al., 2006Javidnia K., Miri R., et al., 2006Radulovic, Mananjarasoa, et al., 2006Rezazadeh, Hamedani, et al., 2006Salgueiro L.R., Pinto E., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5HP-5MSDB-1DB-1
Column length (m) 30.30.30.30.25.
Carrier gas HeHeH2N2 
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.50.50.50.60.
Tend (C) 280.250.285.260.180.
Heat rate (K/min) 4.5.4.32.3.
Initial hold (min) 5.2. 3.10.
Final hold (min)    5.10.
I 1590.1593.1605.1599.1603.
ReferenceSaroglou, Dorizas, et al., 2006Su, Ho, et al., 2006Vujisic L., Vuckovic I., et al., 2006Dob T., Berramdane T., et al., 2005bin Jantan, Yalvema, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1SE-54SPB-1HP-5SPB-1
Column length (m) 60.25.30.30.30.
Carrier gas HeH2HeN2He
Substrate      
Column diameter (mm) 0.220.250.250.250.2
Phase thickness (mum) 0.250.20.250.250.2
Tstart (C) 60.50.70.60.70.
Tend (C) 230.250.220.220.220.
Heat rate (K/min) 2.4.3.5.3.
Initial hold (min)    10. 
Final hold (min) 35. 15. 15.
I 1580.1591.1568.1596.1568.
ReferencePaolini, Costa, et al., 2005Simionatto, Porto, et al., 2005Antunes, Sevinate-Pinto, et al., 2004Bertoli, Menichini, et al., 2004Cavaleiro, Salgueiro, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSSPB-1SPB-1BP-1DB-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.250.20.20.320.25
Phase thickness (mum) 0.250.20.20.250.25
Tstart (C) 60.70.70.60.40.
Tend (C) 280.220.220.220.200.
Heat rate (K/min) 3.3.3.5.4.
Initial hold (min)     5.
Final hold (min)  15.15.13.20.
I 1588.1569.1569.1596.1601.
ReferenceChorianopoulos, Kalpoutzakis, et al., 2004Moldão-Martins, Beirão-da-Costa, et al., 2004Moldão-Martins, Beirão-da-Costa, et al., 2004Raina, Kumar, et al., 2004Yu, Kim, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-5DB-5HP-5DB-5
Column length (m) 30.25.30.30.30.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.75.60.60.60.
Tend (C) 200.210.240.280.240.
Heat rate (K/min) 4.3.3.3.3.
Initial hold (min) 5.10.   
Final hold (min) 20.1.30.  
I 1609.1588.1592.1590.1591.
ReferenceYu, Kim, et al., 2004, 2bin Ahmad and bin Jantan, 2003Bader, Caponi, et al., 2003Bougatsos, Meyer, et al., 2003Flamini, Luigi Cioni, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-1RTX-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 75.60.40.45.60.
Tend (C) 230.280.270.250.280.
Heat rate (K/min) 3.4.2.3.4.
Initial hold (min) 10.5.5.6.5.
Final hold (min) 20. 20.  
I 1603.1590.1546.1603.1589.
ReferenceJantan, Ling, et al., 2003Karioti, Skaltsa, et al., 2003Senatore, Lentini, et al., 2003Shellie, Marriott, et al., 2003Skaltsa, Demetzos, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5SPB-1HP-5MSHP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.200.250.25
Phase thickness (mum) 0.250.250.200.250.25
Tstart (C) 60.60.70.60.50.
Tend (C) 280.280.220.300.280.
Heat rate (K/min) 3.3.3.3.3.
Initial hold (min)     5.
Final hold (min)   15.  
I 1593.1592.1568.1594.1590.
ReferenceTsiri, Kretsi, et al., 2003Tzakou, Couladis, et al., 2003Cavaleiro, Salgueiro, et al., 2002Couladis, Chinou, et al., 2002Demetzos, Angelopoulou, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-1SE-30DB-5CP Sil 5 CB
Column length (m) 30.25.25.30.25.
Carrier gas  N2N2HeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.25 0.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 280.180.180.260.280.
Heat rate (K/min) 3.3.3.4.4.
Initial hold (min) 5.10.10. 6.
Final hold (min)  10.10.  
I 1591.1582.1584.1590.1583.
ReferenceFokialakis, Magiatis, et al., 2002bin Jantan and bin Ahmad, 2002bin Jantan, Ayop, et al., 2002Javidnia, Miri, et al., 2002Pino, Marbot, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBCP Sil 5 CBHP-5HP-5HP-5MS
Column length (m) 30.50.30.30.30.
Carrier gas H2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (mum) 0.250.40.250.500.25
Tstart (C) 60.60.60.60.60.
Tend (C) 280.280.280.280.280.
Heat rate (K/min) 2.3.3.3.3.
Initial hold (min) 10.10.5. 5.
Final hold (min) 40.60.   
I 1583.1583.1587.1592.1590.
ReferencePino, Marbot, et al., 2002, 2Pino, Marbot, et al., 2002, 3Aligiannis, Kalpoutzakis, et al., 2001Couladis, Tzakou, et al., 2001Giamakis, Kretsi, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5CP Sil 5 CBHP-5MSHP-5DB-5
Column length (m) 30.50.30.30.30.
Carrier gas H2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (mum) 0.250.40.250.250.25
Tstart (C) 60.60.60.50.60.
Tend (C) 240.280.280.280.240.
Heat rate (K/min) 3.3.4.4.3.
Initial hold (min)  10.5.5.2.
Final hold (min)  60.   
I 1592.1587.1589.1587.1585.
ReferenceNogueira, Bittrich, et al., 2001Pino, Marbot, et al., 2001Skaltsa, Mavrommati, et al., 2001Lazari, Skaltsa, et al., 2000Maia, de Paula, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-1HP-1DB-5
Column length (m) 30.30.60.60.30.
Carrier gas HeHeHeHeH2
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (mum) 0.250.25 0.250.25
Tstart (C) 60.60.60.50.60.
Tend (C) 240.240.230.250.240.
Heat rate (K/min) 3.3.3.2.53.
Initial hold (min) 2.2. 5. 
Final hold (min)   5.  
I 1589.1589.1580.1580.1589.
ReferenceMaia, de Paula, et al., 2000Maia, de Paula, et al., 2000Javidnia and Shafiee, 1999Stashenko, Cervantes, et al., 1999Nogueira, Marsaioli, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1BP-1BP-1DB-1DB-5
Column length (m) 25.50.50.10.60.
Carrier gas H2HeHeH2He
Substrate      
Column diameter (mm) 0.250.220.220.250.24
Phase thickness (mum) 0.30.250.250.25 
Tstart (C) 50.60.60.80.50.
Tend (C) 200.230.230.160.280.
Heat rate (K/min) 3.2.2.5.5.
Initial hold (min) 1.   3.
Final hold (min) 20.35.35.  
I 1554.1576.1583.1553.1594.
ReferenceBicchi, Fresia, et al., 1997Mariotti, Costa, et al., 1997Mariotti, Tomi, et al., 1997Perry, van Klink, et al., 1997Tzakou, Roussis, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Boti, Koukoua, et al., 2007
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Saroglou, Marin, et al., 2007
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bin Jantan, Yalvema, et al., 2005
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Paolini, Costa, et al., 2005
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Simionatto, Porto, et al., 2005
Simionatto, E.; Porto, C.; da Silva, U.F.; Squizani, A.; Dalcol, I.I.; Morel, A.F., Composition and antimicrobial activity of the essential oil from Aloysia sellowii, J. Braz. Chem. Soc., 2005, 16, 6B, 1458-1462, https://doi.org/10.1590/S0103-50532005000800028 . [all data]

Antunes, Sevinate-Pinto, et al., 2004
Antunes, T.; Sevinate-Pinto, I.; Barroso, J.G.; Cavaleiro, C.; Salgueiro, L.R., Micromorphology of trichomes and composition of essential oil of Teucrium capitatum, Flavour Fragr. J., 2004, 19, 4, 336-340, https://doi.org/10.1002/ffj.1310 . [all data]

Bertoli, Menichini, et al., 2004
Bertoli, A.; Menichini, F.; Noccioli, C.; Morelli, I.; Pistelli, L., Volatile constituents of different organs of Psoralea bituminosa L., Flavour Fragr. J., 2004, 19, 2, 166-171, https://doi.org/10.1002/ffj.1315 . [all data]

Cavaleiro, Salgueiro, et al., 2004
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Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References