Home Symbol which looks like a small house Up Solid circle with an upward pointer in it

2-Butenoic acid, 3-methyl-2-[(trimethylsilyl)oxy]-, trimethylsilyl ester


Van Den Dool and Kratz RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillary
Active phase OV-1SE-52SE-52
Column length (m) 10.25.25.
Carrier gas HeHeHe
Substrate    
Column diameter (mm) 0.220.320.32
Phase thickness (mum) 0.170.520.52
Tstart (C) 70.70.70.
Tend (C) 270.270.270.
Heat rate (K/min) 5.5.5.
Initial hold (min)    
Final hold (min)    
I 1261.1261.1282.
ReferenceLefevere, Verhaeghe, et al., 1989Lefevere, Verhaeghe, et al., 1989Lefevere, Verhaeghe, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Lefevere, Verhaeghe, et al., 1989
Lefevere, M.F.; Verhaeghe, B.J.; Declerck, D.H.; Van Bocxlaer, J.F.; De Leenheer, A.P.; De Sagher, R.M., Metabolic Profiling of Urinary Organic Acids by Single and Multicolumn Capillary Gas Chromatography, J. Chromatogr. Sci., 1989, 27, 1, 23-29, https://doi.org/10.1093/chromsci/27.1.23 . [all data]


Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References