Adrenaline, 4TMS derivative
- Formula: C21H45NO3Si4
- Molecular weight: 471.9289
- IUPAC Standard InChI: InChI=1S/C21H45NO3Si4/c1-22(26(2,3)4)17-21(25-29(11,12)13)18-14-15-19(23-27(5,6)7)20(16-18)24-28(8,9)10/h14-16,21H,17H2,1-13H3
- IUPAC Standard InChIKey: GAEOAXOOVYAKOZ-UHFFFAOYSA-N
- CAS Registry Number: 54947-77-2
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: Adrenaline tetrakis(trimethylsilyl); Epinephrine, tetrakis-TMS; Epinephrine, TMS
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Kovats' RI, non-polar column, isothermal
| Column type | Active phase | Temperature (C) | I | Reference | Comment |
|---|---|---|---|---|---|
| Packed | OV-1 | 190. | 2010. | Cashaw, Walsh, et al., 1971 | N2, GasChrom Q; Column length: 2. m |
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Packed | OV-1 | 2000. | Butts, 1972 | He, Chromosorb W HP (80-100 mesh), 10. K/min; Column length: 2. m; Tstart: 100. C; Tend: 325. C |
References
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Cashaw, Walsh, et al., 1971
Cashaw, J.L.; Walsh, M.J.; Yamanaka, Y.; Davis, V.E.,
Simultaneous determination of biogenic amines and narcotic alkaloids by gas-liquid chromatography,
J. Chromatogr. Sci., 1971, 9, 2, 98-104, https://doi.org/10.1093/chromsci/9.2.98
. [all data]
Butts, 1972
Butts, W.C.,
Two-Column Gas Chromatography of Trimethylsilyl Derivatives of Biochemically Significant Compounds,
Anal. Biochemistry, 1972, 46, 1, 187-199, https://doi.org/10.1016/0003-2697(72)90411-3
. [all data]
Notes
Go To: Top, Gas Chromatography, References
- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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