Bicyclo[3.1.1]heptan-3-ol, 6,6-dimethyl-2-methylene-, [1S-(1α,3α,5α)]-

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Van Den Dool and Kratz RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Sil PONA GBHP-5DB-5SPB-1HP-5MS
Column length (m) 100.25.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 140.60.60.50.60.
Tend (C) 230.240.240.250.280.
Heat rate (K/min) 5.4.3.5.4.
Initial hold (min) 10.2. 3.5.
Final hold (min) 25.  15. 
I 1143.1132.1141.1143.1134.
ReferenceCunicao, Lopes, et al., 2007Dehghan, Solaimanian, et al., 2007Flamini, Cioni, et al., 2007Radulovic, Lazarevic, et al., 2007Radulovic, Lazarevic, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSHP-5MSDB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.50.60.
Tend (C) 260.280.280.250.240.
Heat rate (K/min) 5.4.3.3.3.
Initial hold (min)  5.  2.
Final hold (min)    10. 
I 1145.1134.1139.1139.1132.
ReferenceSabulal, Dan, et al., 2007Saroglou, Marin, et al., 2007Vagionas, Ngassapa, et al., 2007Yu, Liao, et al., 2007Batista-Pereira, Fernandes, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5BP-1BP-1DB-5BP-1
Column length (m) 30.50.50.30.50.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.250.220.250.320.22
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 240.220.220.240.220.
Heat rate (K/min) 3.2.2.3.2.
Initial hold (min)    3. 
Final hold (min)  20.20.5.20.
I 1147.1119.1125.1129.1124.
ReferenceBlock, Flamini, et al., 2006Boti, Bighelli, et al., 2006Bousmaha, Boti, et al., 2006Dob, Dahmane, et al., 2006Gonny, Cavaleiro, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1SPB-1HP-5MSDB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (μm) 0.250.20.250.250.25
Tstart (C) 50.70.60.50.50.
Tend (C) 250.220.280.250.250.
Heat rate (K/min) 5.3.4.5.5.
Initial hold (min) 3. 5.2.2.
Final hold (min) 15.15.   
I 1143.1119.1138.1139.1139.
ReferenceRadulovic, Lazarevic, et al., 2006Salgueiro L.R., Pinto E., et al., 2006Saroglou, Dorizas, et al., 2006Su, Ho, et al., 2006Su, Ho, et al., 2006, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSCP Sil 5 CBHP-5RTX-1DB-1
Column length (m) 30.25.30.60.30.
Carrier gas H2H2N2 N2
Substrate      
Column diameter (mm) 0.250.250.250.220.32
Phase thickness (μm) 0.25 0.250.250.25
Tstart (C) 50.80.60.60.50.
Tend (C) 285.270.220.220.260.
Heat rate (K/min) 4.310.5.2.2.
Initial hold (min)   10. 3.
Final hold (min)    20.5.
I 1133.1126.1141.1126.1111.
ReferenceVujisic L., Vuckovic I., et al., 2006Ziegenbein, Hanssen, et al., 2006Cioni, Flamini, et al., 2005Cozzani, Muselli, et al., 2005Dob T., Berramdane T., et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5DB-5SE-54SPB-1
Column length (m) 30.30.30.30.30.
Carrier gas  N2HeHeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.60.40.60.70.
Tend (C) 250.220.260.260.220.
Heat rate (K/min) 2.5.2.2.3.
Initial hold (min) 8.10.5.5. 
Final hold (min)   20. 15.
I 1116.1141.1142.1135.1122.
ReferenceDob, Dahmane, et al., 2005Flamini, Luigi Cioni, et al., 2005Senatore, Napolitano, et al., 2005Alma, Nitz, et al., 2004Antunes, Sevinate-Pinto, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1DB-5HP-5MSHP-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (μm) 0.20.250.25 0.25
Tstart (C) 70.60.60.60.60.
Tend (C) 220.240.280.260.260.
Heat rate (K/min) 3.3.4.3.3.
Initial hold (min)   5.  
Final hold (min) 15.    
I 1119.1141.1134.1138.1139.
ReferenceCavaleiro, Salgueiro, et al., 2004Flamini, Cioni, et al., 2004Grujic-Jovanovic, Skaltsa, et al., 2004Javidnia, Miri, et al., 2004Javidnia, Miri, et al., 2004, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSDB-1DB-5HP-5MS
Column length (m) 30.30.60.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.40.60.50.
Tend (C) 280.300.280.275.250.
Heat rate (K/min) 4.5.4.4.3.
Initial hold (min) 5.5.5.  
Final hold (min)      
I 1139.1140.1119.1143.1143.
ReferenceKarioti, Hadjipavlou-Litina, et al., 2004Mumm, Tiemann, et al., 2004Omidbaigi, Sefidkon, et al., 2004Ramezani, Khaje-Karamoddin, et al., 2004Salido, Valenzuela, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5RTX-1HP-5HP-5
Column length (m) 25.30.60.30.30.
Carrier gas N2HeHeN2N2
Substrate      
Column diameter (mm) 0.250.250.220.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 75.60.60.60.60.
Tend (C) 210.240.230.220.220.
Heat rate (K/min) 3.3.2.5.5.
Initial hold (min) 10.  10.10.
Final hold (min) 1.30.45.  
I 1139.1141.1124.1140.1141.
Referencebin Ahmad and bin Jantan, 2003Bader, Caponi, et al., 2003Cavalli, Tomi, et al., 2003Emilio Tomei, Manganelli, et al., 2003Flamini, Luigi Cioni, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5HP-5HP-5HP-5
Column length (m) 25.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 260.240.280.280.280.
Heat rate (K/min) 4.3.4.3.3.
Initial hold (min)   5.  
Final hold (min)      
I 1140.1141.1134.1139.1139.
ReferenceJavidnia, Miri, et al., 2003Macchioni, Cioni, et al., 2003Skaltsa, Demetzos, et al., 2003Tsiri, Kretsi, et al., 2003Tsiri, Kretsi, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5CP Sil 5 CBDB-1RTX-5
Column length (m) 30.30.25.50.30.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.220.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.45.
Tend (C) 280.260.280.220.250.
Heat rate (K/min) 3.4.4.2.3.
Initial hold (min)   6. 6.
Final hold (min)    20. 
I 1138.1139.1122.1130.1139.
ReferenceTzakou, Couladis, et al., 2003Javidnia, Miri, et al., 2002Pino, Marbot, et al., 2002Pintore, Usai, et al., 2002Shellie, Mondello, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5HP-5HP-5HP-5MSBP-1
Column length (m) 30.30.30.30.50.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.22
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 45.60.60.60.60.
Tend (C) 250.260.380.280.220.
Heat rate (K/min) 3.3.3.3.2.
Initial hold (min) 6.  5. 
Final hold (min)  10.  20.
I 1146.1136.1142.1139.1125.
ReferenceShellie, Mondello, et al., 2002Couladis, Baziou, et al., 2001Couladis, Tsortanidou, et al., 2001Giamakis, Kretsi, et al., 2001Rezzi, Cavaleiro, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSBP-1DB-1CP Sil 5 CB
Column length (m) 30.30.50.30.25.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.250.250.220.250.25
Phase thickness (μm) 0.250.250.250.25 
Tstart (C) 50.60.60.50.60.
Tend (C) 250.280.220.220.260.
Heat rate (K/min) 3.4.2.3.5.
Initial hold (min)  5. 3. 
Final hold (min)   20.  
I 1143.1134.1123.1121.1126.
ReferenceSalido, Altarejos, et al., 2001Skaltsa, Mavrommati, et al., 2001Mazzoni, Tomi, et al., 1999Muselli, Hoi, et al., 1999Weyerstahl, Marschall, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase BP-1BP-1
Column length (m) 50.50.
Carrier gas HeHe
Substrate   
Column diameter (mm) 0.220.22
Phase thickness (μm) 0.250.25
Tstart (C) 60.60.
Tend (C) 230.230.
Heat rate (K/min) 2.2.
Initial hold (min)   
Final hold (min) 35.35.
I 1117.1122.
ReferenceMariotti, Costa, et al., 1997Mariotti, Tomi, et al., 1997
Comment MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Antunes, Sevinate-Pinto, et al., 2004
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Grujic-Jovanovic, Skaltsa, et al., 2004
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Javidnia, Miri, et al., 2004
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Javidnia, Miri, et al., 2004, 2
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Karioti, Hadjipavlou-Litina, et al., 2004
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Mumm, Tiemann, et al., 2004
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Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References