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Bicyclo[3.1.0]hexan-2-ol, 2-methyl-5-(1-methylethyl)-


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-5MS1096.Baranauskiene, Venskutonis, et al., 200330. m/0.25 mm/0.25 «mu»m, He, 50. C @ 2. min, 4. K/min, 280. C @ 10. min
CapillaryCP Sil 5 CB1053.Ogunwande, Olawore, et al., 200325. m/0.25 mm/0.15 «mu»m, H2, 3. K/min; Tstart: 50. C; Tend: 230. C
CapillaryDB-51068.Viña and Murillo, 200330. m/0.25 mm/0.25 «mu»m, He, 50. C @ 5. min, 0.5 K/min, 250. C @ 10. min
CapillaryBP-11114.Ekundayo, Laakso, et al., 1988H2, 65. C @ 2. min, 5. K/min; Column length: 50. m; Column diameter: 0.33 mm; Tend: 220. C

Kovats' RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryBP-11096.Khan, Verma, et al., 200630. m/0.32 mm/0.25 «mu»m, N2; Program: 60C => 5C/min => 220C (5min) => 3C/min => 245C(5min)

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillarySPB-11051.Antunes, Sevinate-Pinto, et al., 200430. m/0.25 mm/0.25 «mu»m, He, 3. K/min, 220. C @ 15. min; Tstart: 70. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryBPX-51082.Cardeal, da Silva, et al., 200630. m/0.25 mm/0.25 «mu»m; Program: 35C(5min) => 3C/min => 210C => 40C/min => 240C (4min)
CapillarySE-521068.Lorenzo, Paz, et al., 200230. m/0.32 mm/0.42 «mu»m, H2; Program: 60C(8min) => 3C/min => 180C => 20C/min => 250C(10min)

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryCP-Sil 5 CB1109.Mothana, Hasson, et al., 201130. m/0.25 mm/0.26 «mu»m, Nitrogen, 3. K/min, 280. C @ 22. min; Tstart: 45. C
CapillaryHP-5MS1095.Bozin B., Mlmica-Dukic N., et al., 200730. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryCP Sil 5 CB1090.Hymete, Rohloff, et al., 200630. m/0.25 mm/0.25 «mu»m, 3. K/min, 220. C @ 3. min; Tstart: 40. C
CapillaryHP-5MS1033.Pitarokili, Tzakou, et al., 200630. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryDB-51068.Bos, Stojanova, et al., 200530. m/0.249 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 290. C
CapillaryRSL-2001070.Jirovetz, Buchbauer, et al., 200530. m/0.25 mm/0.25 «mu»m, 40. C @ 2. min, 6. K/min, 280. C @ 10. min
CapillarySE-541094.Kilic, Hafizoglu, et al., 200430. m/0.25 mm/0.25 «mu»m, He, 60. C @ 5. min, 2. K/min; Tend: 260. C
CapillarySE-541125.Kilic, Hafizoglu, et al., 200430. m/0.053 mm/1.5 «mu»m, He, 5. K/min; Tstart: 100. C; Tend: 250. C
CapillaryDB-51070.Rohloff, Mordal, et al., 200430. m/0.25 mm/0.25 «mu»m, He, 2.5 K/min, 220. C @ 6. min; Tstart: 35. C
CapillaryRTX-5Sil1102.Dudai, Larkov, et al., 200330. m/0.25 mm/0.25 «mu»m, He, 4. K/min, 200. C @ 10. min; Tstart: 70. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-11040.Silva, Matos, et al., 200330. m/0.25 mm/0.1 «mu»m, He; Program: 35C => 4C/min => 180C => 10C/min => 250C
CapillaryDB-51077.Sanda, Koba, et al., 199830. m/0.25 mm/0.25 «mu»m, N2; Program: 45C(5min) => 2C/min => 200C => 5C/min => 250C

Normal alkane RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryCP-Wax 52CB1469.Hymete, Rohloff, et al., 200630. m/0.32 mm/0.25 «mu»m, He, 60. C @ 7. min, 3.3 K/min, 220. C @ 3. min

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Baranauskiene, Venskutonis, et al., 2003
Baranauskiene, R.; Venskutonis, P.R.; Viskelis, P.; Dambrauskiene, E., Influence of nitrogen fertilizers on the yield and composition of thyme (Thymus vulgaris), J. Agric. Food Chem., 2003, 51, 26, 7751-7758, https://doi.org/10.1021/jf0303316 . [all data]

Ogunwande, Olawore, et al., 2003
Ogunwande, I.A.; Olawore, N.O.; Kasali, A.A.; König, W.A., Chemical composition of the leaf volatile oils of Callitris intratropica R.T. Baker H.G. Smith from Nigeria, Flavour Fragr. J., 2003, 18, 5, 387-389, https://doi.org/10.1002/ffj.1214 . [all data]

Viña and Murillo, 2003
Viña, A.; Murillo, E., Essential oil composition from twelve varieties of basil (Ocimum spp) grown in Columbia, J. Braz. Chem. Soc., 2003, 14, 5, 744-749, https://doi.org/10.1590/S0103-50532003000500008 . [all data]

Ekundayo, Laakso, et al., 1988
Ekundayo, O.; Laakso, I.; Adegbola, R.-M.; Oguntimein, B.; Sofowora, A.; Hiltunen, R., Essential oil constituents of Ashanti pepper (Piper guineense) fruits (berries), J. Agric. Food Chem., 1988, 36, 5, 880-882, https://doi.org/10.1021/jf00083a001 . [all data]

Khan, Verma, et al., 2006
Khan, M.; Verma, S.C.; Srivastava, S.K.; Shawl, A.S.; Syamsundar, K.V.; Khanuja, S.P.S.; Kumar, T., Essential oil composition of Taxus wallichiana Zucc. from the Northern Himalayan region of India, Flavour Fragr. J., 2006, 21, 5, 772-775, https://doi.org/10.1002/ffj.1682 . [all data]

Antunes, Sevinate-Pinto, et al., 2004
Antunes, T.; Sevinate-Pinto, I.; Barroso, J.G.; Cavaleiro, C.; Salgueiro, L.R., Micromorphology of trichomes and composition of essential oil of Teucrium capitatum, Flavour Fragr. J., 2004, 19, 4, 336-340, https://doi.org/10.1002/ffj.1310 . [all data]

Cardeal, da Silva, et al., 2006
Cardeal, Z.L.; da Silva, M.D.R.G.; Marriott, P.J., Comprehensive two-dimensional gas chromatography/mass spectrometric analysis of pepper volatiles, Rapid Commun. Mass Spectrom., 2006, 20, 19, 2823-2836, https://doi.org/10.1002/rcm.2665 . [all data]

Lorenzo, Paz, et al., 2002
Lorenzo, D.; Paz, D.; Dellacassa, E.; Davies, P.; Vila, R.; Cañigueral, S., Essential oils of Mentha pulegium and Mentha rotundifolia from Uruguay, Braz. Arch. Biol. Technol., 2002, 45, 4, 519-524, https://doi.org/10.1590/S1516-89132002000600016 . [all data]

Mothana, Hasson, et al., 2011
Mothana, R.A.A.; Hasson, S.S.; Schultze, W.; Mowitz, A.; Lindequist, U., Phytochemical composition and in vitro antimicrobial and antioxidant activities of essential oils of three endemic Soqotraen Boswellia species, Food Chem., 2011, 126, 3, 1149-1154, https://doi.org/10.1016/j.foodchem.2010.11.150 . [all data]

Bozin B., Mlmica-Dukic N., et al., 2007
Bozin B.; Mlmica-Dukic N.; Samojlik I.; Jovin E., Antimicrobial and antioxidant properties of rosemary and sage (Rosmarinus officinalis L. and Salvia officinalis L., lamiaceae) essential oils, J. Agric. Food Chem., 2007, 55, 19, 7879-7885, https://doi.org/10.1021/jf0715323 . [all data]

Hymete, Rohloff, et al., 2006
Hymete, A.; Rohloff, J.; Iversen, T.-H., Essential oil from seeds and husks of Aframomum corrorima from Ethiopia, Flavour Fragr. J., 2006, 21, 4, 642-644, https://doi.org/10.1002/ffj.1634 . [all data]

Pitarokili, Tzakou, et al., 2006
Pitarokili, D.; Tzakou, O.; Loukis, A., Essential oil composition of Salvia verticillata, S. verbenaca, S. glutinosa and S. candidissima growing wild in Greece, Flavour Fragr. J., 2006, 21, 4, 670-673, https://doi.org/10.1002/ffj.1647 . [all data]

Bos, Stojanova, et al., 2005
Bos, R.; Stojanova, A.; Woerdenbag, H.J.; Koulman, A.; Quax, W.J., Volatile components of the aerial parts of Artemisia pontica L. grown in Bulgaria, Flavour Fragr. J., 2005, 20, 2, 145-148, https://doi.org/10.1002/ffj.1399 . [all data]

Jirovetz, Buchbauer, et al., 2005
Jirovetz, L.; Buchbauer, G.; Stoyanova, A.; Georgiev, E.V.; Damianova, S.T., Composition, quality control and antimicrobial activity of the essential oil of cumin (Cuminum cyminumL.) seeds from Bulgaria that had been stored for up to 36 years, Int. J. Food Sci. Technol., 2005, 40, 3, 305-310, https://doi.org/10.1111/j.1365-2621.2004.00915.x . [all data]

Kilic, Hafizoglu, et al., 2004
Kilic, A.; Hafizoglu, H.; Kollmannsberger, H.; Nitz, S., Volatile constituents and key odorants in leaves, buds, flowers, and fruits of Laurus nobilis L., J. Agric. Food Chem., 2004, 52, 6, 1601-1606, https://doi.org/10.1021/jf0306237 . [all data]

Rohloff, Mordal, et al., 2004
Rohloff, J.; Mordal, R.; Dragland, S., Chemotypical variation of tansy (Tanacetum vulgare L.) from 40 different locations in Norway, J. Agric. Food Chem., 2004, 52, 6, 1742-1748, https://doi.org/10.1021/jf0352430 . [all data]

Dudai, Larkov, et al., 2003
Dudai, N.; Larkov, O.; Chaimovitsh, D.; Lewinsohn, E.; Freiman, L.; Ravid, U., Essential oil compounds of Origanum dayi Post, Flavour Fragr. J., 2003, 18, 4, 334-337, https://doi.org/10.1002/ffj.1237 . [all data]

Silva, Matos, et al., 2003
Silva, M.G.V.; Matos, F.J.A.; Machado, M.I.L.; Craveiro, A.A., Essential oils of Ociumum basilicum L., O. basilicum. var. minimum L. and O. basilicum. var. purpurascens Benth. grown in north-eastern Brazil, Flavour Fragr. J., 2003, 18, 1, 13-14, https://doi.org/10.1002/ffj.1134 . [all data]

Sanda, Koba, et al., 1998
Sanda, K.; Koba, K.; Nambo, P.; Gaset, A., Chemical investigation of Ocimum species growing in Togo, Flavour Fragr. J., 1998, 13, 4, 226-232, https://doi.org/10.1002/(SICI)1099-1026(1998070)13:4<226::AID-FFJ717>3.0.CO;2-H . [all data]


Notes

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