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Butyl sulfide

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Kovats' RI, non-polar column, isothermal

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryPacked
Active phase DB-5DB-5DB-5DB-5Apiezon M
Column length (m) 30.30.30.30.2.1
Carrier gas     He or N2
Substrate     Chromosorb W, AW-DMCS
Column diameter (mm) 0.250.250.250.25 
Phase thickness (mum) 0.10.10.10.1 
Temperature (C) 100.120.60.80.130.
I 1084.41088.51078.11081.31081.
ReferenceMiller and Bruno, 2003Miller and Bruno, 2003Miller and Bruno, 2003Miller and Bruno, 2003Garbuzov, Misharina, et al., 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPackedCapillary
Active phase SE-30SE-30Apiezon MApiezon MApiezon L
Column length (m) 1.82.2.12.1 
Carrier gas N2 N2N2 
Substrate Chromaton N-AWHMDSChromosorb W AW (80-100 mesh)Chromosorb WChromosorb W 
Column diameter (mm)      
Phase thickness (mum)      
Temperature (C) 80.110.130.130.120.
I 1059.1077.1081.1082.1084.
ReferenceZotov, Golovkin, et al., 1981Möckel and Zolg, 1977Golovnya, Garbuzov, et al., 1976Golovnya and Garbuzov, 1974Agr, Tesaric, et al., 1973
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SqualaneSqualaneSqualaneSqualaneApiezon L
Column length (m)   50.50.100.
Carrier gas   N2N2N2
Substrate   Celite 545Celite 545 
Column diameter (mm)   0.30.30.3
Phase thickness (mum)      
Temperature (C) 120.86.120.86.120.
I 1070.1064.1070.1064.1084.
ReferenceAgr, Tesaric, et al., 1973Agr, Tesaric, et al., 1973Agrawal, Tesarík, et al., 1972Agrawal, Tesarík, et al., 1972Agrawal, Tesarík, et al., 1972
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryPackedPackedPackedPacked
Active phase E-301DC-200SE-30Apiezon LApiezon L
Column length (m)  1.51.5  
Carrier gas      
Substrate      
Column diameter (mm)      
Phase thickness (mum)      
Temperature (C) 150.120.130.110.130.
I 1077.1081.1081.1082.1086.
ReferenceKudryavtseva, Fatalieva, et al., 1972Golovnya and Arsen'ev, 1970Golovnya and Arsen'ev, 1970Martinu and Janák, 1970Martinu and Janák, 1970
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPackedPacked
Active phase Apiezon LSqualaneSqualaneSqualaneSqualane
Column length (m)  2.1.21.21.2
Carrier gas  H2/N2=3/1ArArAr
Substrate  CeliteCeliteCeliteCelite
Column diameter (mm)      
Phase thickness (mum)      
Temperature (C) 150.100.100.65.78.
I 1092.1060.01062.1056.1057.
ReferenceMartinu and Janák, 1970Evans and Smith, 1967Adlard, Evans, et al., 1965Adlard, Evans, et al., 1965Adlard, Evans, et al., 1965
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPackedPacked
Active phase SqualaneSqualaneSqualaneSqualaneSqualane
Column length (m) 1.51.51.51.51.5
Carrier gas ArArArMixtureMixture
Substrate CeliteCeliteCeliteCeliteCelite
Column diameter (mm)      
Phase thickness (mum)      
Temperature (C) 100.65.78.100.65.
I 1058.1053.1056.1060.1055.
ReferenceAdlard, Evans, et al., 1965Adlard, Evans, et al., 1965Adlard, Evans, et al., 1965Adlard, Evans, et al., 1965Adlard, Evans, et al., 1965
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPackedPacked
Active phase SqualaneSqualaneSqualaneSqualaneSqualane
Column length (m) 1.50.90.90.91.
Carrier gas MixtureN2N2N2He
Substrate CeliteCeliteCeliteCeliteCelite
Column diameter (mm)      
Phase thickness (mum)      
Temperature (C) 78.100.65.78.100.
I 1057.1079.1072.1075.1060.
ReferenceAdlard, Evans, et al., 1965Adlard, Evans, et al., 1965Adlard, Evans, et al., 1965Adlard, Evans, et al., 1965Adlard, Evans, et al., 1965
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPackedPacked
Active phase SqualaneSqualaneSqualaneSqualaneSqualane
Column length (m) 1.1.4.4.4.
Carrier gas HeHeN2N2N2
Substrate CeliteCeliteSterchamolSterchamolSterchamol
Column diameter (mm)      
Phase thickness (mum)      
Temperature (C) 65.78.100.65.78.
I 1055.1057.1066.1060.1062.
ReferenceAdlard, Evans, et al., 1965Adlard, Evans, et al., 1965Adlard, Evans, et al., 1965Adlard, Evans, et al., 1965Adlard, Evans, et al., 1965
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPackedPacked
Active phase SqualaneSqualaneSqualaneSqualaneSqualane
Column length (m) 0.90.90.9  
Carrier gas H2H2H2  
Substrate CeliteCeliteCelite  
Column diameter (mm)      
Phase thickness (mum)      
Temperature (C) 100.65.78.100.65.
I 1056.1050.1053.1061.1056.
ReferenceAdlard, Evans, et al., 1965Adlard, Evans, et al., 1965Adlard, Evans, et al., 1965Adlard, Evans, et al., 1965Adlard, Evans, et al., 1965
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Packed
Active phase Squalane
Column length (m)  
Carrier gas  
Substrate  
Column diameter (mm)  
Phase thickness (mum)  
Temperature (C) 78.
I 1058.
ReferenceAdlard, Evans, et al., 1965
Comment MSDC-RI

References

Go To: Top, Kovats' RI, non-polar column, isothermal, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Miller and Bruno, 2003
Miller, K.E.; Bruno, T.J., Isothermal Kováts retention indices of sulfur compounds on a poly(5% diphenyl-95% dimethylsiloxane) stationary phase, J. Chromatogr. A, 2003, 1007, 1-2, 117-125, https://doi.org/10.1016/S0021-9673(03)00958-0 . [all data]

Garbuzov, Misharina, et al., 1985
Garbuzov, V.G.; Misharina, T.A.; Aerov, A.F.; Golovnya, R.V., Gas chromatographic retention indices for sulphur(II)-containing organic substances, J. Anal. Chem. USSR (Engl. Transl.), 1985, 40, 4, 576-586. [all data]

Zotov, Golovkin, et al., 1981
Zotov, L.N.; Golovkin, G.V.; Golovnya, R.V., GC Behaviour of Symmetrical n-Dialkyl Sulphides under Isothermal and Temperature Programming Conditions, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1981, 4, 1, 6-10, https://doi.org/10.1002/jhrc.1240040103 . [all data]

Möckel and Zolg, 1977
Möckel, H.J.; Zolg, M., Retentionsindices n-aliphatischer Schwefelverbindungen, Z. Anal. Chem., 1977, 285, 1, 45-46, https://doi.org/10.1007/BF00446017 . [all data]

Golovnya, Garbuzov, et al., 1976
Golovnya, R.V.; Garbuzov, V.G.; Misharina, T.A., Gas chromatographic characteristics of sulfur compounds. 2. Normal sulfides, Izv. Akad. Nauk Kaz. SSR Ser. Khim., 1976, 10, 2266-2270. [all data]

Golovnya and Garbuzov, 1974
Golovnya, R.V.; Garbuzov, V.G., Effect of heteroatom in aliphatic sulfur- and oxygen-containing compounds on the values of the retention indices in gas chromatography, Izv. Akad. Nauk SSSR Ser. Khim., 1974, 7, 1519-1521. [all data]

Agr, Tesaric, et al., 1973
Agr, X.X.; Tesaric, K.; Janak, J., Will be entered later, J. Chromatogr., 1973, 95, 207-215. [all data]

Agrawal, Tesarík, et al., 1972
Agrawal, B.B.; Tesarík, K.; Janák, J., Gas chromatographic characterization of sulphur compounds in the 93-162° gasoline cut from Romashkino crude oil using Kováts retention indices, J. Chromatogr., 1972, 65, 1, 207-215, https://doi.org/10.1016/S0021-9673(00)86933-2 . [all data]

Kudryavtseva, Fatalieva, et al., 1972
Kudryavtseva, N.A.; Fatalieva, A.A.; Lulova, N.I.; Vinogradova, I.E., Methods of assessing fuel and oil quality. Use of gas chromatography to identify components of decomposition products from Sul'fol antiscuff additive, Chem. Technol. Fuels Oils (Engl. Transl.), 1972, 8, 10, 786-790, https://doi.org/10.1007/BF00717079 . [all data]

Golovnya and Arsen'ev, 1970
Golovnya, R.V.; Arsen'ev, Y.N., Gas-chromatographic method for the analysis of n-mercaptans and symmetrical n-sulfides and n-disulfides, Bull. Acad. Sci. USSR, Div. Chem. Sci. (Engl. Transl.), 1970, 6, 4, 1316-1318, https://doi.org/10.1007/BF00852683 . [all data]

Martinu and Janák, 1970
Martinu, V.; Janák, J., Gas-liquid chromatographic retention data of some aliphatic and alicyclic sulphides, J. Chromatogr., 1970, 52, 69-75, https://doi.org/10.1016/S0021-9673(01)96545-8 . [all data]

Evans and Smith, 1967
Evans, M.B.; Smith, J.F., Gas chromatography in qualitative analysis. IV. An investigation of the changes in relative rentention data accompanying the oxidation of apolar stationary phases, J. Chromatogr., 1967, 28, 277-284, https://doi.org/10.1016/S0021-9673(01)85968-9 . [all data]

Adlard, Evans, et al., 1965
Adlard, E.R.; Evans, M.B.; Butlin, A.G.; Evans, R.S.; Hill, R.; Huber, J.F.K.; Littlewood, A.B.; McCambley, W.G.; Smith, J.F.; Swanton, W.T.; Swoboda, P.A.T., Recommendations of the data sub-committee for the publication of retention data, J. Gas Chromatogr., 1965, 3, 9, 298-302, https://doi.org/10.1093/chromsci/3.9.298 . [all data]


Notes

Go To: Top, Kovats' RI, non-polar column, isothermal, References