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Bicyclosesquiphellandrene


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-51488.Stashenko, Jaramillo, et al., 200450. m/0.2 mm/0.2 «mu»m, He, 35. C @ 15. min, 3. K/min, 250. C @ 40. min
CapillaryMS51470.Shao, Marriott, et al., 200325. m/0.25 mm/0.25 «mu»m, 3. K/min; Tstart: 40. C; Tend: 180. C
CapillaryBP-11489.Rezzi, Cavaleiro, et al., 200150. m/0.22 mm/0.25 «mu»m, 2. K/min, 220. C @ 20. min; Tstart: 60. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-5MS1498.7Andriamaharavo, 201430. m/0.25 mm/0.25 «mu»m, He; Program: 60C (1 min) => 5 C/min => 210C => 10 C/min => 280C (15 min)

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryCP Sil 5 CB1493.Ayoub, Al-Azizi, et al., 2006He, 10. K/min; Column length: 25. m; Tstart: 80. C; Tend: 270. C
CapillaryHP-51491.Figuérédo, Cabassu, et al., 200630. m/0.25 mm/0.25 «mu»m, He, 50. C @ 5. min, 5. K/min, 300. C @ 5. min
CapillaryBPX-51495.Dickschat, Martens, et al., 200525. m/0.22 mm/0.25 «mu»m, He, 50. C @ 5. min, 5. K/min; Tend: 320. C
CapillaryCP Sil 5 CB1490.Olawore, Ogunwande, et al., 200525. m/0.25 mm/0.15 «mu»m, 3. K/min; Tstart: 50. C; Tend: 230. C
CapillaryHP-51489.Stashenko, Jaramillo, et al., 200360. m/0.25 mm/0.25 «mu»m, 40. C @ 15. min, 5. K/min; Tend: 250. C
CapillaryHP-51489.Stashenko, Jaramillo, et al., 200360. m/0.25 mm/0.25 «mu»m, 40. C @ 15. min, 5. K/min; Tend: 250. C
CapillaryHP-51490.Stashenko, Jaramillo, et al., 200360. m/0.25 mm/0.25 «mu»m, 40. C @ 15. min, 5. K/min; Tend: 250. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-51481.Parker, Pollnitz, et al., 200730. m/0.25 mm/0.25 «mu»m, He; Program: 50C(1min) => 3C/min => 250C(10min) => 20C/min => 280C (5min)
CapillaryHP-5MS1521.Yu, Huang, et al., 200730. m/0.25 mm/0.25 «mu»m, He; Program: 40C(3min) => 6C/min => 160C => 10C/min => 300C (10min)
CapillaryDB-51471.Hamm, Bleton, et al., 200430. m/0.25 mm/0.25 «mu»m, He; Program: 40C(1min) => 9C/min => 130C => 2C/min => 230C

Normal alkane RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-Innowax1760.Stashenko, Jaramillo, et al., 200350. m/0.2 mm/0.2 «mu»m, 50. C @ 5. min, 4. K/min; Tend: 220. C
CapillaryHP-Innowax1760.Stashenko, Jaramillo, et al., 200350. m/0.2 mm/0.2 «mu»m, 50. C @ 5. min, 4. K/min; Tend: 220. C
CapillaryHP-Innowax1760.Stashenko, Jaramillo, et al., 200350. m/0.2 mm/0.2 «mu»m, 50. C @ 5. min, 4. K/min; Tend: 220. C
CapillaryDB-Wax1706.Christoph, 200160. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 45. C; Tend: 240. C
CapillaryDB-Wax1748.Molleken U., Sinnwell V., et al., 199830. m/0.25 mm/0.25 «mu»m, N2, 3. K/min; Tstart: 45. C; Tend: 220. C

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Stashenko, Jaramillo, et al., 2004
Stashenko, E.E.; Jaramillo, B.E.; Martínez, J.R., Comparison of different extraction methods for the analysis of volatile secondary metabolites of Lippia alba (Mill.) N.E. Brown, grown in Colombia, and evaluation of its in vitro antioxidant activity, J. Chromatogr. A, 2004, 1025, 1, 93-103, https://doi.org/10.1016/j.chroma.2003.10.058 . [all data]

Shao, Marriott, et al., 2003
Shao, Y.; Marriott, P.; Shellie, R.; Hügel, H., Solid-phase micro-extraction-comprehensive two-dimensional gas chromatography of ginger (Zingiber officinale) volatiles, Flavour Fragr. J., 2003, 18, 1, 5-12, https://doi.org/10.1002/ffj.1133 . [all data]

Rezzi, Cavaleiro, et al., 2001
Rezzi, S.; Cavaleiro, C.; Bighelli, A.; Salgueiro, L.; da Cunha, A.P.; Casanova, J., Intraspecific chemical variability of the leaf essential oil of Juniperus phoenicea subsp. turbinata from Corsica, Biochem. Syst. Ecol., 2001, 29, 2, 179-188, https://doi.org/10.1016/S0305-1978(00)00044-2 . [all data]

Andriamaharavo, 2014
Andriamaharavo, N.R., Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2014. [all data]

Ayoub, Al-Azizi, et al., 2006
Ayoub, N.; Al-Azizi, M.; König, W.; Kubeczka, K.-H., Essential oils and a novel polyacetylene from Eryngium yuccifolium Michaux. (Apiaceae), Flavour Fragr. J., 2006, 21, 6, 864-868, https://doi.org/10.1002/ffj.1631 . [all data]

Figuérédo, Cabassu, et al., 2006
Figuérédo, G.; Cabassu, P.; Chalchat, J.-C.; Pasquier, B., Studies of Mediterranean oregano populations. VIII. Chemical composition of essential oils of oreganos of various origins, Flavour Fragr. J., 2006, 21, 1, 134-139, https://doi.org/10.1002/ffj.1543 . [all data]

Dickschat, Martens, et al., 2005
Dickschat, J.S.; Martens, T.; Brinkhoff, T.; Simon, M.; Schulz, S., Volatiles released by a Streptomyces species isolated from the North Sea, Chemistry and Biodiversity, 2005, 2, 7, 837-865, https://doi.org/10.1002/cbdv.200590062 . [all data]

Olawore, Ogunwande, et al., 2005
Olawore, N.O.; Ogunwande, I.A.; Ekundayo, O.; Adeleke, K.A., Chemical composition of the leaf and fruit essential oils of Murraya paniculata (L.) Jack. (Syn. Murraya exotica Linn.), Flavour Fragr. J., 2005, 20, 1, 54-56, https://doi.org/10.1002/ffj.1365 . [all data]

Stashenko, Jaramillo, et al., 2003
Stashenko, E.E.; Jaramillo, B.E.; Martínez, J.R., Comparación de la composición química y de la actividad antioxidante in vitro de los metabolitos secundarios volátiles de plantas de la familia verbenaceae, Rev. Acad. Colomb. Cienc. Exactas Fis. Nat., 2003, 27, 105, 579-597. [all data]

Parker, Pollnitz, et al., 2007
Parker, M.; Pollnitz, A.P.; Cozzolino, D.; Leigh Francis, I.; Herderich, M.J., Identification and Quantification of a Marker Compound for 'Pepper' Aroma and Flavor in Shiraz Grape Berries by Combination of Chemometrics and Gas Chromatography-Mass Spectrometry, J. Agric. Food Chem., 2007, 55, 15, 5948-5955, https://doi.org/10.1021/jf0705320 . [all data]

Yu, Huang, et al., 2007
Yu, Y.; Huang, T.; Yang, B.; Liu, X.; Duan, G., Development of gas chromatography-mass spectrometry with microwave distillation and simultaneous solid-phase microextraction for rapid determination of volatile constituents in ginger, J. Pharm. Biomed. Anal., 2007, 43, 1, 24-31, https://doi.org/10.1016/j.jpba.2006.06.037 . [all data]

Hamm, Bleton, et al., 2004
Hamm, S.; Bleton, J.; Tchapla, A., Headspace solid phase microextraction for screening for the presence of resins in Egyptian archaeological samples, J. Sep. Sci., 2004, 27, 3, 235-243, https://doi.org/10.1002/jssc.200301611 . [all data]

Christoph, 2001
Christoph, F., Chemische Zuzammensetzung und antimikrobielle Eigenschaften der ätherischen Öle von Leptospermum scoparium J. R. et G. Forst. und anderer Teebaumöle der Gattungen Kunzea, Leptospermum und Melaleuca unter besonderer Berücksichtigung von Handelsölen, Dissertation, University of Hamburg, Germany, 2001, 196. [all data]

Molleken U., Sinnwell V., et al., 1998
Molleken U.; Sinnwell V.; Kubeczka K.H., TThe essential oil composition of fruits from Smyrnium perfoliatum, Phytochemistry, 1998, 47, 6, 1079-1083, https://doi.org/10.1016/S0031-9422(98)80076-9 . [all data]


Notes

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