Methamphetamine


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
PackedApiezon L120.1187.Donike and Stratmann, 1976Chromosorb W

Kovats' RI, polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
PackedPEG-20M120.1562.Donike and Stratmann, 1976Chromosorb W

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-5 MS1188.Taniguchi, Yamamoto, et al., 201030. m/0.25 mm/0.25 μm, Helium, 60. C @ 2. min, 20. K/min, 250. C @ 3. min

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryOV-1, SE-30, Methyl silicone, SP-2100, OV-101, DB-1, etc.1161.Waggott and Davies, 1984Hydrogen; Column length: 50. m; Column diameter: 0.32 mm; Program: not specified

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Donike and Stratmann, 1976
Donike, M.; Stratmann, D., Gas-chromatographische identifizierung von stimulantien der phenyläthylaminreihe mit hilfe der retnetions-indices, Z. Anal. Chem., 1976, 279, 2, 129-131, https://doi.org/10.1007/BF00440798 . [all data]

Taniguchi, Yamamoto, et al., 2010
Taniguchi, M.; Yamamoto, Y.; Nishi, K., A technique combining trifluoroacetyl derivatization and gas chromatography - mass spectrometry to distinguish methamphetamine and its 4-substituted analogues, J. Mass Spectrom., 2010, 45, 12, 1473-1476, https://doi.org/10.1002/jms.1851 . [all data]

Waggott and Davies, 1984
Waggott, A.; Davies, I.W., Identification of organic pollutants using linear temperature programmed retention indices (LTPRIs) - Part II, 1984, retrieved from http://dwi.defra.gov.uk/research/completed-research/reports/dwi0383.pdf. [all data]


Notes

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