(-)-β-Bourbonene

Formula: C₁₅H₂₄
Molecular weight: 204.3511
IUPAC Standard InChI: InChI=1S/C15H24/c1-9(2)11-7-8-15(4)12-6-5-10(3)13(12)14(11)15/h9,11-14H,3,5-8H2,1-2,4H3/t11-,12?,13?,14?,15-/m1/s1
IUPAC Standard InChIKey: YIRAHEODBQONHI-XTLGRWLVSA-N
CAS Registry Number: 5208-59-3
Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript.
Stereoisomers:
Other names: Cyclobuta[1,2:3,4]dicyclopentene, decahydro-3a-methyl-6-methylene-1-(1-methylethyl)-, [1S-(1α,3aα,3bβ,6aβ,6bα)]-; β-Bourbonene; Cyclobuta[1,2:3,4]dicyclopentene, 1,2,3,3a,3bβ,4,5,6,6aβ,6bα-decahydro-1α-isopropyl-3aα-methyl-6-methylene-; Cyclobuta[1,2:3,4]dicyclopentene, decahydro-3a-methyl-6-methylene-1-(1-methylethyl)-, (1α,3aα,3bβ,6aβ,6bα)-; [1S-[1α,3aα,3bβ,6aβ,6bα]]-Cyclobuta[1,2:3,4]dicyclopentene-decahydro-3a-methyl-6-methylene-1-[1-methylethyl]; (1S,3aS,3bR,6aS,6bR)-1-Isopropyl-3a-methyl-6-methylenedecahydrocyclobuta[1,2:3,4]di[5]annulene; β-bourbenene; Cyclobuta[1,2:3,4]dicyclopentene, decahydro-3a-methyl-6-methylene-1-(1-methylethyl)-, (1S,3aS,3bR,6aS,6bR)-; beta-bourbonene
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Information on this page:
Other data available:
- Mass spectrum (electron ionization)
- Gas Chromatography
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Normal alkane RI, non-polar column, temperature ramp

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	DB-5	HP-5	HP-5	HP-5
Column length (m)	60.	30.	25.	25.	25.
Carrier gas	Helium	Helium	Hydrogen	Hydrogen	Hydrogen
Substrate
Column diameter (mm)	0.22	0.25	0.32	0.32	0.32
Phase thickness (μm)	0.25	0.25	0.52	0.52	0.52
T_start (C)	60.	100.	40.	40.	40.
T_end (C)	230.	260.	280.	280.	280.
Heat rate (K/min)	2.	10.	4.	4.	4.
Initial hold (min)		1.
Final hold (min)	5.	10.	10.	10.	10.
I	1379.	1393.	1378.	1378.	1378.
Reference	Bendiabdellah, El Amine Dib, et al., 2012	Boukhris, Bouaziz, et al., 2012	Velickovic, Ristic, et al., 2012	Velickovic, Ristic, et al., 2012	Velickovic, Ristic, et al., 2012
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DP-5	DP-5	HP-5 MS	HP-5	HP-5 MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	80.	80.	50.	60.	50.
T_end (C)	300.	300.	250.	240.	180.
Heat rate (K/min)	4.	4.	7.	3.	2.
Initial hold (min)	1.	1.	1.
Final hold (min)	40.	40.	5.
I	1339.	1339.	1388.	1388.	1372.
Reference	Vijayakumar, Duraipandiyan, et al., 2012	Vijayakumar, Duraipandiyan, et al., 2012	Zouari, Ayadi, et al., 2012	Bertoli, Lepnardi, et al., 2011	Hammami, Kamoun, et al., 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5 MS	HP-5	RTX-1	HP-5
Column length (m)	30.	30.	30.	60.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.252	0.22	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	30.	60.	60.	60.
T_end (C)	240.	250.	240.	230.	240.
Heat rate (K/min)	3.	5.	3.	2.	3.
Initial hold (min)		3.			2.
Final hold (min)		10.		30.
I	1384.	1429.	1381.	1386.	1386.
Reference	Karimi, Farmani, et al., 2011	Zarai, Kadri, et al., 2011	Cavar, Maksimovic, et al., 2010	Dib, Djabou, et al., 2010	Kahriman, Tosun, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-1	DB-5	DB-5 MS	SPB-1	HP-5 MS
Column length (m)	30.	30.	60.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.20	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.20	0.25
T_start (C)	50.	60.	40.	70.	60.
T_end (C)	250.	240.	250.	220.	220.
Heat rate (K/min)	5.	3.	5.	3.	5.
Initial hold (min)	3.		15.		10.
Final hold (min)	15.		15.	15.
I	1375.	1383.	1391.	1375.	1385.
Reference	Lazarevic, Palic, et al., 2010	Magalhaes, Lima, et al., 2010	Mesa-Arango, Betancur-Galvis, et al., 2010	Neves, Rosa, et al., 2010	Ogunwande, Flamini, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5	HP-5 MS	DB-1	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Hydrogen	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	100.	70.	70.	50.	60.
T_end (C)	220.	290.	290.	220.	240.
Heat rate (K/min)	2.	5.	5.	4.	3.
Initial hold (min)				2.
Final hold (min)			10.	2.
I	1380.	1392.	1388.	1378.	1388.
Reference	Pripdeevech, Chumpolsri, et al., 2010	Radulovic, Dordevic, et al., 2010	Radulovic, Dordevic, et al., 2010, 2	Xu, Tang, et al., 2010	Alim, Goze, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	SE-54	DB-5	SPB-5	DB-5
Column length (m)	50.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Nitrogen	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.53	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.50	0.25
T_start (C)	70.	60.	35.	50.	50.
T_end (C)	220.	260.	220.	210.	250.
Heat rate (K/min)	2.	2.	3.	3.	5.
Initial hold (min)		5.		5.	2.
Final hold (min)		999.	40.	45.
I	1391.	1379.	1384.	1393.	1388.
Reference	Benites, Moiteiro, et al., 2009	Dayisoylu and Alma, 2009	El-Massry, El-Ghorab, et al., 2009	Gilani, Shah, et al., 2009	Ho, Wang, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	RTX-1	RTX-1	DB-5	DB-5
Column length (m)	25.	60.	60.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Nitrogen
Substrate
Column diameter (mm)	0.20	0.22	0.22	0.25	0.25
Phase thickness (μm)	0.33	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	45.	40.
T_end (C)	240.	230.	230.	250.	250.
Heat rate (K/min)	3.	2.	2.	3.	3.
Initial hold (min)				3.	1.
Final hold (min)	7.	30.	30.	5.	10.
I	1385.	1379.	1386.	1392.	1393.
Reference	Maridass, 2009	Museli, Pau, et al., 2009	Museli, Pau, et al., 2009	Porto, Decorti, et al., 2009	Rahimi-Nasrabadi, Gholivand, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5 MS	HP-5 MS	SE-52	HP-5
Column length (m)	30.	30.	30.	50.	30.
Carrier gas	Nitrogen	Helium	Helium	Helium	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	40.	50.	60.	60.
T_end (C)	230.	250.	280.	280.	220.
Heat rate (K/min)	2.	4.	4.	3.	5.
Initial hold (min)		2.			10.
Final hold (min)		2.		20.
I	1388.	1388.	1387.	1392.	1386.
Reference	Scrivanti, Anton, et al., 2009	Su, Wang, et al., 2009	Zhao, Zeng, et al., 2009	Djarri, Medjroubi, et al., 2008	Flamini, Tebano, et al., 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SLB-5 MS	RTX-1	RTX-5	HP-5	DB-5
Column length (m)	30.	60.	20.	30.	50.
Carrier gas	Helium	He	Helium	Helium	Nitrogen
Substrate
Column diameter (mm)	0.25	0.22	0.18	0.25	0.20
Phase thickness (μm)	0.25	0.25	0.20	0.32	0.32
T_start (C)	50.	60.	50.	60.	60.
T_end (C)	250.	230.	280.	250.	220.
Heat rate (K/min)	3.	2.	4.	5.	5.
Initial hold (min)	2.		1.	30.	3.
Final hold (min)	10.	35.			5.
I	1385.	1388.	1398.	1385.	1380.
Reference	Lo Presti, Sciarrone, et al., 2008	Paolini, Tomi, et al., 2008	Skalicka-Wozniak, Los, et al., 2008	Yassa and Akhani, 2008	Amiri, 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5 MS	HP-5	DB-5	ZP-5
Column length (m)	30.	30.	30.	30.	60.
Carrier gas	He	Helium	N2	Helium	He
Substrate
Column diameter (mm)	0.26	0.32	0.25	0.26	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	60.	40.
T_end (C)	240.	280.	240.	290.	260.
Heat rate (K/min)	3.	4.	5.	3.	6.
Initial hold (min)		5.	1.		7.
Final hold (min)			4.		1.
I	1379.	1384.	1384.	1379.	1407.
Reference	Bos, Woerdenbag, et al., 2007	Capetanos, Saroglou, et al., 2007	Cheraif, Ben Jannet, et al., 2007	Elfami, Bos, et al., 2007	Füssel, Dötterl, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	Col-Elite 5MS	BP-1	ZB-5	DB-1
Column length (m)	60.	30.		30.	30.
Carrier gas	Nitrogen	He	He		Helium
Substrate
Column diameter (mm)	0.25	0.25		0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	60.	30.	60.	60.	50.
T_end (C)	250.	246.	220.	220.	260.
Heat rate (K/min)	4.	3.	5.	4.	2.5
Initial hold (min)	1.			5.	1.
Final hold (min)	10.		6.	20.	20.
I	1393.	1391.	1386.	1381.	1370.
Reference	Ghasempour, Shirinpour, et al., 2007	Gudaityte and Venskutonis R.P., 2007	Kiran, Devi, et al., 2007	Mohottalage, Tabacchi, et al., 2007	Monser-Esfahani, Karamkhani, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	SPB-1	DB-1	DB-1	DB-5
Column length (m)	30.	30.	60.	60.	30.
Carrier gas	Helium	He	Nitrogen	Nitrogen
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.2	0.25	0.25	0.25
T_start (C)	60.	70.	60.	60.	40.
T_end (C)	220.	220.	250.	250.	210.
Heat rate (K/min)	4.	3.	4.	5.	2.
Initial hold (min)			1.
Final hold (min)		15.	10.	10.	33.
I	1389.	1378.	1393.	1391.	1382.
Reference	Morteza-Semnani, Saeedi, et al., 2007	Pinto, Salgueiro, et al., 2007	Reza, Ebrahim, et al., 2007	Sonboli, Kanani, et al., 2007	Sylvestre, Longtin, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Elite-5MS	HP-5MS	HP-5 MS	HP-5	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	Helium		He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.5	0.25	0.25	0.25	0.32
T_start (C)	40.	60.	60.	40.	60.
T_end (C)	280.	280.	280.	240.	250.
Heat rate (K/min)	4.	3.	3.	5.	5.
Initial hold (min)	5.			3.	30.
Final hold (min)	10.			10.
I	1387.	1346.	1388.	1339.	1385.
Reference	Tava, Pecetti, et al., 2007	Tzakou, Bazos, et al., 2007	Vagionas, Graikou, et al., 2007	Wenguang, Wenlai, et al., 2007	Yassa and Akhani, 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	CP Sil 5 CB	HP-1	HP-1	HP-5MS
Column length (m)	30.	25.	50.	50.	30.
Carrier gas	He	He	He	He
Substrate
Column diameter (mm)	0.25		0.2	0.2	0.25
Phase thickness (μm)	0.25		0.5	0.33	0.25
T_start (C)	60.	80.	60.	60.	60.
T_end (C)	300.	270.	250.	250.	280.
Heat rate (K/min)	3.	10.	2.	2.	4.
Initial hold (min)				4.
Final hold (min)			120.	30.
I	1374.	1384.	1387.	1387.	1381.
Reference	Apel, Sobral, et al., 2006	Ayoub, Al-Azizi, et al., 2006	Castel, Fernandez, et al., 2006	Castel, Fernandez, et al., 2006	Ebrahim Sajjadi and Mehregan, 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	DB-1	DB-5	DB-1
Column length (m)	30.	30.	60.	30.	60.
Carrier gas	Helium	He	He	He	He
Substrate
Column diameter (mm)	0.26	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	60.	60.	60.
T_end (C)	290.	300.	240.	240.	240.
Heat rate (K/min)	3.	5.	5.	5.	5.
Initial hold (min)		5.	2.	2.	2.
Final hold (min)		5.
I	1379.	1384.	1386.	1384.	1386.
Reference	Elfami, Komar, et al., 2006	Figuérédo, Cabassu, et al., 2006	Gohari, Hadjiakhoondi, et al., 2006	Gohari, Hadjiakhoondi, et al., 2006	Gohari A.R., Hadjiakhoondi A., et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	BP-1	HP-5	CP Sil 5 CB	5 % Phenyl methyl siloxane
Column length (m)	30.		30.	30.	30.
Carrier gas	He	Helium	Helium	N2	Helium
Substrate
Column diameter (mm)	0.25		0.32	0.32	0.25
Phase thickness (μm)	0.25		0.25	0.25	0.25
T_start (C)	60.	60.	60.	50.	60.
T_end (C)	240.	220.	260.	300.	280.
Heat rate (K/min)	5.	5.	5.	4.	3.
Initial hold (min)	2.		2.
Final hold (min)		6.	13.		30.
I	1384.	1386.	1387.	1374.	1357.
Reference	Gohari A.R., Hadjiakhoondi A., et al., 2006	Kiran, Bhavani, et al., 2006	Kucuk, Gulec, et al., 2006	Lis and Milczarek, 2006	Marongiu, Piras, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	DB-5	DB-5	NB-30	DB-5
Column length (m)	25.	30.	30.	30.	25.
Carrier gas	He	He	He	He	N2
Substrate
Column diameter (mm)	0.3	0.25	0.25	0.2	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.15
T_start (C)	70.	60.	60.	50.	50.
T_end (C)	220.	220.	220.	250.	200.
Heat rate (K/min)	4.	4.	4.	2.	4.
Initial hold (min)	2.		5.		3.
Final hold (min)	10.
I	1403.	1390.	1393.	1381.	1390.
Reference	Moody, Gundidza, et al., 2006	Morteza-Semnani, Akbarzadeh, et al., 2006	Morteza-Semnani K., Akbarzadeh M., et al., 2006	Orav, Raal, et al., 2006	Ouamba, Ouabonzi, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5MS	HP-5	DB-5	DB-5
Column length (m)	50.	30.	30.	30.	30.
Carrier gas	N2	He	He	Hydrogen	Hydrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	95.	40.	60.	70.	70.
T_end (C)	240.	260.	220.	280.	280.
Heat rate (K/min)	4.	4.	5.	4.	4.
Initial hold (min)			10.	4.	4.
Final hold (min)
I	1386.	1388.	1373.	1384.	1384.
Reference	Pala-Paul J., Perez-Alonso M.J., et al., 2006	Petrovic, Ristic, et al., 2006	Pintore G., Chessa M., et al., 2006	Pino, Marbot, et al., 2006	Pino, Marbot, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	DB-1	SPB-5	Methyl Silicone	SPB-5
Column length (m)	30.	60.		25.	60.
Carrier gas	He	He	He	N2	He
Substrate
Column diameter (mm)	0.25	0.25		0.3	0.32
Phase thickness (μm)	0.25			0.15	1.
T_start (C)	60.	40.	50.	50.	40.
T_end (C)	280.	250.	250.	210.	230.
Heat rate (K/min)	3.	4.	5.	2.	3.
Initial hold (min)			3.	5.	5.
Final hold (min)			15.		2.
I	1351.	1379.	1383.	1397.	1418.
Reference	Pitarokili, Tzakou, et al., 2006	Sefidkon, Jamzad, et al., 2006	Stojanovic, Palic, et al., 2006	Tonzibo, Coffy, et al., 2006	Tornambe, Cornu, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	DB-5	DB-5	DB-5	DB-5
Column length (m)	30.	30.	50.	25.	30.
Carrier gas	He	He			He
Substrate
Column diameter (mm)	0.25	0.249	0.3	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.15	0.25
T_start (C)	60.	60.	60.	40.	60.
T_end (C)	280.	290.	240.	220.	240.
Heat rate (K/min)	3.	3.	2.	3.	3.
Initial hold (min)				5.
Final hold (min)
I	1363.	1384.	1382.	1382.	1384.
Reference	Basta, Tzakou, et al., 2005	Bos, Stojanova, et al., 2005	Chagonda and Chalchat, 2005	Chagonda and Chalchat, 2005, 2	Chaverri and Cicció, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	Methyl Silicone	SPB-5	HP-5	CP Sil 8 CB
Column length (m)	30.	60.	60.	25.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.3	0.32	0.2	0.25
Phase thickness (μm)	0.25		1.	0.33	0.25
T_start (C)	60.	50.	40.	60.	80.
T_end (C)	240.	240.	230.	240.	200.
Heat rate (K/min)	3.	3.	3.	3.	3.
Initial hold (min)			5.		5.
Final hold (min)				7.	5.
I	1384.	1382.	1418.	1385.	1382.
Reference	Chaverri and Cicció, 2005	Chalchat and Özcan, 2005	Cornu, Kondjoyan, et al., 2005	Duarte, Figueira, et al., 2005	Facey, Porter, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	DB-1	DB-1	DB-5
Column length (m)	30.	25.	30.	30.	30.
Carrier gas	He	H2	He	He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.52	0.25	0.25	0.25
T_start (C)	50.	40.	50.	50.	35.
T_end (C)	300.	240.	265.	265.	280.
Heat rate (K/min)	5.	4.	2.5	2.5	4.
Initial hold (min)	5.		1.	1.	2.
Final hold (min)	5.		20.	30.
I	1384.	1380.	1366.	1370.	1389.
Reference	Figuérédo, Cabassu, et al., 2005	Jovanovic, Kitic, et al., 2005	Khanavi, Ghasemian, et al., 2005	Khalighi-Sigaroodi, Hadijiakhoondi, et al., 2005	Kowalski and Wolski, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5MS	DB-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	35.	60.	60.	60.	60.
T_end (C)	280.	230.	280.	220.	220.
Heat rate (K/min)	4.	3.	3.	4.	4.
Initial hold (min)	2.		30.	5.	4.
Final hold (min)
I	1389.	1379.	1360.	1388.	1388.
Reference	Kowalski, 2005	Limberger, Sobral, et al., 2005	Marongiu, Piras, et al., 2005	Morteza-Semnani, Akbarzadeh, et al., 2005	Morteza-Semnani and Saeedi, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	HP-5	DB-1	HP-5MS
Column length (m)	30.	30.	30.	50.	30.
Carrier gas	He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	70.	95.	60.
T_end (C)	220.	250.	240.	240.	280.
Heat rate (K/min)	4.	3.	5.	4.	3.
Initial hold (min)	4.	5.
Final hold (min)
I	1389.	1382.	1394.	1376.	1388.
Reference	Morteza-Semnani and Saeedi, 2005, 2	Najafpour Navaei, Mirza, et al., 2005	Oyedeji, Yani, et al., 2005	Pala-Paul, Perez-Alonso, et al., 2005	Petrakis, Roussis, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5MS	HP-5MS	DB-5	DB-1
Column length (m)	30.	30.	30.	30.	60.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	280.	275.	280.	220.	250.
Heat rate (K/min)	4.	4.	4.	3.	5.
Initial hold (min)				4.
Final hold (min)					10.
I	1382.	1385.	1380.	1385.	1391.
Reference	Sajjadi S.E. and Eskandari B., 2005	Sajjadi and Ghannadi, 2005	Sajjadi, 2005	Salehi, Sefidkon, et al., 2005	Salehi, Sonboli, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	PE-5	DB-5	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	H2	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25		0.25	0.25	0.25
T_start (C)	50.	40.	60.	60.	60.
T_end (C)	265.	240.	230.	230.	280.
Heat rate (K/min)	2.5	4.	5.	3.	3.
Initial hold (min)	1.		2.
Final hold (min)	20.		4.	20.
I	1368.	1383.	1378.	1388.	1382.
Reference	Sarkhail, Amin, et al., 2005	Sefidkon and Jamzad, 2005	Singh, Raina, et al., 2005	Skoula and Grayer, 2005	Slavkovska, Couladis, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5 MS	DB-5	DB-1	HP-5
Column length (m)	60.	30.	30.	50.	30.
Carrier gas	He	He	He	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.50	0.25	0.25	0.32
T_start (C)	60.	60.	60.	90.	60.
T_end (C)	250.	260.	280.	240.	250.
Heat rate (K/min)	5.	3.	3.	4.	5.
Initial hold (min)					3.
Final hold (min)	10.	20.
I	1389.	1398.	1352.	1366.	1356.
Reference	Sonboli, Salehi, et al., 2005	Topçu, Barla, et al., 2005	Tzakou and Constantinidis, 2005	Velasco-Negueruela, Pérez-Alonso, et al., 2005	Aghel, Yamini, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	RTX-1	DB-5	DB-5	HP-5MS
Column length (m)	25.	30.	30.	30.	30.
Carrier gas	Nitrogen	N2	He		He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	40.	60.
T_end (C)	240.	300.	300.	210.	280.
Heat rate (K/min)	3.	4.	3.	2.	3.
Initial hold (min)				2.
Final hold (min)				33.
I	1382.	1386.	1381.	1383.	1381.
Reference	JAvidnia, Mojab, et al., 2004	Kalemba and Thiem, 2004	Limberger, Sobral, et al., 2004	Lopez Arze, Collin, et al., 2004	Malencic, Couladis, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	DB-1	DB-1	NB-30	DB-1
Column length (m)	30.	60.	50.	50.	30.
Carrier gas	He	He	N2	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.20	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	95.	50.	50.
T_end (C)	275.	270.	240.	250.	265.
Heat rate (K/min)	4.	4.	4.	2.	2.5
Initial hold (min)					1.
Final hold (min)					20.
I	1387.	1384.	1371.	1383.	1368.
Reference	Mehrabani, Asadipour, et al., 2004	Nik, Mirza, et al., 2004	Palá-Paúl, Velasco-Negueruela, et al., 2004	Raal, Paaver, et al., 2004	Sarkhail, Amin, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	BPX-5	HP-5MS	HP-5MS
Column length (m)	60.	30.	25.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.22	0.25	0.25
Phase thickness (μm)	0.25	0.25	1.	0.25	0.25
T_start (C)	40.	60.	60.	60.	60.
T_end (C)	280.	300.	250.	280.	220.
Heat rate (K/min)	4.	3.	3.	3.	5.
Initial hold (min)	5.		5.		20.
Final hold (min)			10.		20.
I	1380.	1388.	1405.	1382.	1393.
Reference	Sefidkon and Shaabani, 2004	Tirillini, Pellegrino, et al., 2004	Vilaseca, Guy, et al., 2004	Couladis, Özcan, et al., 2003	Feizbaksh, Saber Tehrani, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5MS	HP-5MS	HP-5	RSL-200
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	N2	He	He	He	H2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	60.	60.	40.
T_end (C)	200.	275.	280.	275.	280.
Heat rate (K/min)	5.	4.	4.	4.	6.
Initial hold (min)					5.
Final hold (min)					5.
I	1372.	1384.	1384.	1386.	1386.
Reference	Fekam Boyom, Ngouana, et al., 2003	Ghannadi, Aghazari, et al., 2003	Ghasemi, Asghari, et al., 2003	Ghannadi and Zolfaghari, 2003	Jirovetz, Buchbauer, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RSL-200	DB-5	CP Sil 5 CB	DB-5MS	DB-5
Column length (m)	30.	50.	25.	30.	50.
Carrier gas	H2	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.2	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.39	0.25	0.25
T_start (C)	40.	50.	60.	60.	50.
T_end (C)	280.	220.	220.	240.	220.
Heat rate (K/min)	6.	3.	5.	3.	3.
Initial hold (min)	5.	2.			2.
Final hold (min)	5.	10.
I	1386.	1394.	1380.	1386.	1390.
Reference	Jirovetz, Buchbauer, et al., 2003, 2	Juteau, Jerkovic, et al., 2003	Khanavi, Hadjiakhoondi, et al., 2003	Maia, Taveira, et al., 2003	Masotti, Juteau, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	DB-5	DB-1	HP-5
Column length (m)	60.	60.	30.	50.	30.
Carrier gas	He	He	He	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	50.	60.	95.	60.
T_end (C)	270.	270.	275.	240.	280.
Heat rate (K/min)	4.	4.	4.	4.	3.
Initial hold (min)			5.
Final hold (min)
I	1380.	1385.	1384.	1377.	1365.
Reference	Mirza and Nik, 2003	Mirza, Nik, et al., 2003	Morteza-Semnani and Saeedi, 2003	Perez-Alonso, Velasco-Negueruela, et al., 2003	Pitarokili, Tzakou, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	HP-5	HP-5	HP-5
Column length (m)	30.	60.	30.	30.	60.
Carrier gas	He	He	He	He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	75.	40.	60.	60.	40.
T_end (C)	220.	220.	280.	280.	250.
Heat rate (K/min)	3.	4.	4.	4.	5.
Initial hold (min)	4.				15.
Final hold (min)
I	1380.	1406.	1382.	1381.	1384.
Reference	Priestap, van Baren, et al., 2003	Rasooli and Mirmostafa, 2003	Sajjadi and Mehregan, 2003	Sajjadi and Mehregan, 2003, 2	Stashenko, Jaramillo, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	Cross-Linked Methylsilicone	HP-5	HP-5
Column length (m)	60.	60.	25.	25.	25.
Carrier gas			He	H2	H2
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.32	0.32
Phase thickness (μm)	0.25	0.25	0.33	0.53	0.53
T_start (C)	40.	40.	70.	40.	40.
T_end (C)	250.	250.	250.	280.	280.
Heat rate (K/min)	5.	5.	4.	4.	4.
Initial hold (min)	15.	15.
Final hold (min)
I	1384.	1384.	1366.	1379.	1388.
Reference	Stashenko, Jaramillo, et al., 2003	Stashenko, Jaramillo, et al., 2003	Velasco-Negueruela, Pérez-Alonso, et al., 2003	Velickovic, Randjelovic, et al., 2003	Velickovic, Randjelovic, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	HP-5	HP-5	DB-5
Column length (m)	25.	25.	25.	25.	30.
Carrier gas	Helium	Helium	Helium	Helium	He
Substrate
Column diameter (mm)	0.32	0.32	0.32	0.32	0.25
Phase thickness (μm)	0.53	0.53	0.53	0.53	0.25
T_start (C)	40.	40.	40.	40.	60.
T_end (C)	280.	280.	280.	280.	240.
Heat rate (K/min)	4.	4.	4.	4.	3.
Initial hold (min)
Final hold (min)
I	1381.	1381.	1382.	1388.	1383.
Reference	Velickovic, Ristic, et al., 2003	Velickovic, Ristic, et al., 2003	Velickovic, Ristic, et al., 2003	Velickovic, Ristic, et al., 2003	Zoghbi, Andrade, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	DB-5	5 % Phenyl methyl siloxane	BP-1	DB-5
Column length (m)	25.	30.	30.	25.	30.
Carrier gas	N2	He	He	N2	He
Substrate
Column diameter (mm)	0.25	0.249	0.25	0.50	0.25
Phase thickness (μm)	0.4	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	75.	60.	60.
T_end (C)	260.	300.	200.	220.	240.
Heat rate (K/min)	5.	3.	3.	5.	3.
Initial hold (min)			4.
Final hold (min)	40.	5.	8.	10.
I	1374.	1383.	1385.	1386.	1386.
Reference	Azaz. D., Demirci, et al., 2002	Bos, Koulman, et al., 2002	Cicció and Gómez-Laurito, 2002	Das, Ram, et al., 2002	Flamini, Ertugrul, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	PTE-5	SE-30	DB-5	DB-5
Column length (m)	30.	60.	50.	30.	30.
Carrier gas	H2	H2	He	He	He
Substrate
Column diameter (mm)	0.32	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.30	0.25	0.25	0.25
T_start (C)	40.	60.	70.	60.	35.
T_end (C)	245.	285.	240.	240.	280.
Heat rate (K/min)	3.	4.3	4.	3.	3.
Initial hold (min)	20.				2.
Final hold (min)					15.
I	1370.	1384.	1386.	1385.	1390.
Reference	Gancel, Ollé, et al., 2002	Gudzic, Djokovic, et al., 2002	Iñigo, Palá-Paúl, et al., 2002	Kobaisy, Tellez, et al., 2002	Krauze-Baranowska, Mardarowicz, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	DB-5	DB-5MS	DB-1	HP-1
Column length (m)	25.	30.	30.	30.	50.
Carrier gas	He	He	He	He	N2
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	50.	60.	60.	60.	90.
T_end (C)	200.	250.	240.	250.	220.
Heat rate (K/min)	5.	3.	3.	4.	3.
Initial hold (min)				10.
Final hold (min)
I	1389.	1379.	1385.	1391.	1379.
Reference	Kuiate, Bessière, et al., 2002	Limberger, Simões-Pires, et al., 2002	Maia, Zoghbi, et al., 2002	Norouzi-Arasi, Yavari, et al., 2002	Priestap, van Baren, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	DB-1	DB-1	HP-5
Column length (m)	25.	60.	60.	50.	30.
Carrier gas	He	He	He	N2	H2
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.25	0.25
Phase thickness (μm)			0.25	0.25	0.25
T_start (C)	60.	40.	40.	60.	40.
T_end (C)	220.	250.	280.	240.	280.
Heat rate (K/min)	3.	4.	4.	3.	4.
Initial hold (min)			5.
Final hold (min)
I	1385.	1377.	1381.	1361.	1384.
Reference	Schwob, Bessière, et al., 2002	Sefidkon, Dabiri, et al., 2002	Sefidkon, 2002	Velasco-Negueruela, Pérez-Alonso, et al., 2002	Velickovic, Randjelovic, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5MS	SPB-5	DB-1	DB-1	HP-5
Column length (m)	30.	60.	60.	60.	30.
Carrier gas	He	He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25		0.25	0.25	0.25
T_start (C)	60.	40.	40.	40.	60.
T_end (C)	270.	220.	280.	280.	220.
Heat rate (K/min)	3.	3.	4.	4.	5.
Initial hold (min)		5.	5.	5.	10.
Final hold (min)		15.
I	1386.	1385.	1377.	1377.	1384.
Reference	Zoghbi, Andrade, et al., 2002	Cornu, Carnat, et al., 2001	Dabiri and Sefidkon, 2001	Dabiri and Sefidkon, 2001	Flamini, Cioni, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	BP-1	Optima-5	RTX-1	DB-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	N2	N2	He	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	60.	60.	50.	60.	60.
T_end (C)	220.	220.	250.	300.	240.
Heat rate (K/min)	5.	5.	3.	4.	3.
Initial hold (min)	10.		3.
Final hold (min)					30.
I	1386.	1387.	1390.	1387.	1345.
Reference	Gallori, Flamini, et al., 2001	Gupta, Mallavarapu, et al., 2001	Jacquemond-Collet, Bessière, et al., 2001	Kalemba, Marschall, et al., 2001	Marongiu, Porcedda, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	DB-5	DB-5	CP Sil 5 CB
Column length (m)	60.	30.	30.	30.	25.
Carrier gas	He	N2	H2	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.4
T_start (C)	50.	80.	60.	60.	60.
T_end (C)	270.	225.	285.	240.	260.
Heat rate (K/min)	4.	4.	3.	3.	5.
Initial hold (min)					40.
Final hold (min)
I	1380.	1372.	1383.5	1384.	1380.
Reference	Mirza, Ahmadi, et al., 2001	Palá-Paúl, Pérez-Alonso, et al., 2001	Santos-Gomes and Fernandes-Ferreira, 2001	Tellez M., Estell R., et al., 2001	Baser, Özek, et al., 2000
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-1	DB-5	RTX-1	Ultra-2	DB-1
Column length (m)	60.	30.	30.	50.	25.
Carrier gas	He	He	N2		He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25		0.25
T_start (C)	60.	60.	60.	32.	50.
T_end (C)	200.	240.	300.	250.	290.
Heat rate (K/min)	4.	3.	4.	4.	4.
Initial hold (min)	5.			5.
Final hold (min)	25.
I	1389.	1385.	1386.	1375.	1383.
Reference	Meccia, Rojas, et al., 2000	Tellez, Dayan, et al., 2000	Kalemba, 1999	Khalilov L.M., Khalilova A.Z., et al., 1999	Koulman, 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	OV-1	SE-30	DB-1	DB-5
Column length (m)	50.	25.	30.	60.	30.
Carrier gas	N2	H2	Helium	He	He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.20	0.25	0.25
T_start (C)	80.	40.	60.	40.	40.
T_end (C)	200.	220.	200.	280.	220.
Heat rate (K/min)	1.	3.	3.	4.	4.
Initial hold (min)		5.	4.	5.	5.
Final hold (min)	20.	5.
I	1385.	1372.	1430.	1389.	1380.
Reference	Menon, Chacko, et al., 1999	Oberhofer, Nikiforov, et al., 1999	Prikhod'ko, Klyuev, et al., 1999	Sefidkon, Dabiri, et al., 1999	Sefidkon and Khajavi, 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	SPB-5	OV-101	DB-5	OV-1
Column length (m)	60.	60.	25.	30.	30.
Carrier gas	He	He		He	He
Substrate
Column diameter (mm)	0.25	0.32	0.32	0.25	0.32
Phase thickness (μm)	0.25	1.		0.25	0.25
T_start (C)	50.	40.	50.	65.	40.
T_end (C)	220.	200.	200.	300.	270.
Heat rate (K/min)	4.	3.	5.	4.	2.
Initial hold (min)		5.		2.	4.
Final hold (min)		2.
I	1390.	1415.	1386.	1382.	1367.
Reference	Sefidkon and Mirza, 1999	Viallon C., Verdier-Metz I., et al., 1999	Zollo, Biyiti, et al., 1998	Elias, Simoneit, et al., 1997	Kökdil, Kurucu, et al., 1997
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-1	DB-1	DB-5	CBP-1	DB-5
Column length (m)	30.		30.	25.	30.
Carrier gas			Helium	He
Substrate
Column diameter (mm)	0.32		0.25	0.22	0.25
Phase thickness (μm)	0.25		0.25		0.25
T_start (C)	40.	80.	60.	60.	60.
T_end (C)	270.	220.	240.	240.	300.
Heat rate (K/min)	2.	6.	3.	5.	4.
Initial hold (min)	4.				2.
Final hold (min)					5.
I	1365.	1379.	1385.	1380.	1383.9
Reference	Kökdil, Tanker, et al., 1997	Salgueiro, Vila, et al., 1997	Tellez, Estell, et al., 1997	Zygadlo, Ariza-Espinar, et al., 1997	Gawdzik, Mardarowicz, et al., 1996
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	BP-1	DB-1	HP-1	HP-101
Column length (m)	50.	25.	60.	25.	50.
Carrier gas	He	N2	He	Helium	H2
Substrate
Column diameter (mm)	0.25	0.50	0.32	0.32	0.32
Phase thickness (μm)			0.50	0.25	0.3
T_start (C)	50.	60.	50.	60.	65.
T_end (C)	250.	220.	250.	220.	300.
Heat rate (K/min)	2.	5.	8.	4.	2.
Initial hold (min)			1.	2.	5.
Final hold (min)			6.	20.
I	1396.	1382.	1405.	1377.	1377.
Reference	Orav, Kailas, et al., 1996	Rajeswara, Kaul, et al., 1996	Sagrero-Nieves and Bartley, 1996	Thanh, Dung, et al., 1996	Demarne and van der Walt, 1993
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Methyl Silicone	DB-1	DB-1	DB-1	OV-1
Column length (m)	25.		60.	60.	50.
Carrier gas					He
Substrate
Column diameter (mm)	0.50		0.32	0.32	0.20
Phase thickness (μm)					0.20
T_start (C)	60.	50.	50.	50.	30.
T_end (C)	220.	230.	230.	250.	220.
Heat rate (K/min)	5.	4.	4.	4.	2.
Initial hold (min)				0.1
Final hold (min)		10.	10.	5.
I	1378.	1381.	1381.	1380.	1380.
Reference	Mallavarapu, Ramesh, et al., 1993	Binder, Turner, et al., 1990	Binder, Turner, et al., 1990, 2	Binder and Flath, 1989	de Pooter, Nicolai, et al., 1988
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-30	OV-101	OV-101	OV-101	OV-101
Column length (m)	30.	50.	50.	50.	30.
Carrier gas					He
Substrate
Column diameter (mm)		0.30	0.30	0.30	0.5
Phase thickness (μm)					0.8
T_start (C)	50.	40.	40.	40.	40.
T_end (C)	240.	230.	230.	230.	220.
Heat rate (K/min)	4.	3.5	3.5	3.5	2.
Initial hold (min)	2.	5.	5.	5.
Final hold (min)	10.
I	1382.	1381.	1396.	1398.	1378.
Reference	Ramaswami, Briscese, et al., 1988	Nykanen, 1986	Nykanen, 1986	Nykanen, 1986	De Pooter and Schamp, 1986
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	SE-30	SE-30+Igepal	SE-30+Igepal
Column length (m)	30.	30.	100.	100.
Carrier gas	He
Substrate
Column diameter (mm)	0.5		0.25	0.25
Phase thickness (μm)	0.8
T_start (C)	40.	50.	70.	70.
T_end (C)	220.	240.	170.	170.
Heat rate (K/min)	2.	4.	1.	1.
Initial hold (min)		2.
Final hold (min)		10.
I	1378.	1382.	1406.	1417.
Reference	De Pooter and Schamp, 1986	Ramaswami, Briscese, et al., 1986	Shibamoto and Jennings, 1977	Shibamoto and Jennings, 1977
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

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Monser-Esfahani, Karamkhani, et al., 2007
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Morteza-Semnani, Saeedi, et al., 2007
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Pinto, Salgueiro, et al., 2007
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Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References

Symbols used in this document:

T_end Final temperature

T_start Initial temperature
Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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