Cyclohexane, 1-ethenyl-1-methyl-2,4-bis(1-methylethenyl)-, [1S-(1α,2β,4β)]-

Formula: C₁₅H₂₄
Molecular weight: 204.3511
IUPAC Standard InChI: InChI=1S/C15H24/c1-7-15(6)9-8-13(11(2)3)10-14(15)12(4)5/h7,13-14H,1-2,4,8-10H2,3,5-6H3/t13-,14+,15-/m1/s1
IUPAC Standard InChIKey: OPFTUNCRGUEPRZ-QLFBSQMISA-N
CAS Registry Number: 515-13-9
Chemical structure:
This structure is also available as a 2d Mol file
Stereoisomers:
Other names: Cyclohexane, 2,4-diisopropenyl-1-methyl-1-vinyl-, (1S,2R,4R)- (-)-; β-Elemene, (-)-; (-)-β-Elemene; β-Elemen; levo-β-Elemene; β-Elemene; β-Elemene enantiomer; 2,4-Diisopropenyl-1-methyl-1-vinylcyclohexane, [1S-(1α,2β,4β)]-; 2,4-Diisopropenyl-1-methyl-1-vinylcyclohexane; 1S-1α,2β,4β-1-Ethenyl-1-methyl-2,4-bis-(1-methylethenyl)cyclohexane; Cyclohexane, 1-ethenyl-1-methyl-2,4-bis(1-methylethenyl)-, (1S,2S,4R)-; beta elemene
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Information on this page:
Other data available:
- Mass spectrum (electron ionization)
- Gas Chromatography
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Normal alkane RI, non-polar column, temperature ramp

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-5 MS	DB-5	RTX-1	HP-5 MS	HP-5 MS
Column length (m)	30.	30.	60.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.22	0.25	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	80.	40.
T_end (C)	240.	240.	230.	240.	250.
Heat rate (K/min)	3.	3.	2.	4.	3.
Initial hold (min)				3.	1.
Final hold (min)			5.	10.	3.
I	1397.	1390.	1389.	1380.	1390.
Reference	Pinheiro, de Queiros, et al., 2013	Rodriques, Amorim, et al., 2013	Bendiabdellah, El Amine Dib, et al., 2012	Dutra, Pittella, et al., 2012	Jian-Yu, Zhu, et al., 2012
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	Polydimethyl siloxane with 5 % Ph	DP-5	HP-5 MS	HP-5 MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium		Helium
Substrate
Column diameter (mm)	0.25		0.25	0.25	0.25
Phase thickness (μm)	0.25		0.25	0.25	0.25
T_start (C)	35.	80.	80.	60.	50.
T_end (C)	300.	200.	300.	300.	250.
Heat rate (K/min)	3.	5.	4.	15.	7.
Initial hold (min)	5.		1.	2.	1.
Final hold (min)	15.	25.	40.	10.	5.
I	1397.	1390.	1398.	1421.	1393.
Reference	Kotowska, Zalikowski, et al., 2012	Priya, Prathapan, et al., 2012	Vijayakumar, Duraipandiyan, et al., 2012	Xu, Han, et al., 2012	Zouari, Ayadi, et al., 2012
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	DB-5	SE-30 MS	CP-Sil 5 CB
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Nitrogen
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.26
T_start (C)	60.	60.	60.	50.	45.
T_end (C)	240.	240.	240.	250.	280.
Heat rate (K/min)	3.	3.	3.	5.	3.
Initial hold (min)		2.		5.
Final hold (min)				10.	22.
I	1391.	1390.	1391.	1390.	1391.
Reference	Bertoli, Lepnardi, et al., 2011	Kahriman, Tosun, et al., 2011	Karimi, Farmani, et al., 2011	Menichini, Tundis, et al., 2011	Mothana, Hasson, et al., 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	ZB-5	HP-5	DB-5	HP-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Nitrogen	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	50.	50.	60.	60.
T_end (C)	200.	300.	250.	240.	240.
Heat rate (K/min)	5.	50.	2.	3.	3.
Initial hold (min)	5.	5.		2.
Final hold (min)	5.	5.
I	1418.	1391.	1391.	1390.	1390.
Reference	Vazquez, Demmel, et al., 2011	Bi Kouame, Bedi, et al., 2010	Ho, Wang, et al., 2010	Kahriman, Tosun, et al., 2010	Magalhaes, Lima, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5 MS	DB-1	BP-1	HP-5	HP-5 MS
Column length (m)	60.	25.		30.	30.
Carrier gas	Helium	Nitrogen	Nitrogen	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25		0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	40.	60.	60.	40.	60.
T_end (C)	250.	250.	220.	260.	220.
Heat rate (K/min)	5.	4.	5.	4.	5.
Initial hold (min)	15.	1.	10.		10.
Final hold (min)	15.	10.	30.	5.
I	1385.	1392.	1389.	1396.	1393.
Reference	Mesa-Arango, Betancur-Galvis, et al., 2010	Mirjalili, Salehi, et al., 2010	Mishra, Chaudhary, et al., 2010	Miyazawa, Kawauchi, et al., 2010	Ogunwande, Flamini, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5 MS	HP-5	HP-5 MS	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Hydrogen	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	100.	70.	70.	60.
T_end (C)	220.	220.	290.	290.	240.
Heat rate (K/min)	5.	2.	5.	5.	3.
Initial hold (min)	10.
Final hold (min)				10.
I	1394.	1387.	1398.	1393.	1393.
Reference	Ogunwande, Flamini, et al., 2010	Pripdeevech, Chumpolsri, et al., 2010	Radulovic, Dordevic, et al., 2010	Radulovic, Dordevic, et al., 2010, 2	Scherer, Wagner, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5 MS	CP Sil 5 CB	DB-1	OV-101	OV-101
Column length (m)	30.	25.	30.	50.	50.
Carrier gas	Helium		Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.15	0.25	0.25	0.25
T_start (C)	60.	50.	50.	70.	70.
T_end (C)	240.	230.	220.	220.	220.
Heat rate (K/min)	3.	3.	4.	2.	2.
Initial hold (min)			2.
Final hold (min)			2.
I	1387.	1391.	1386.	1391.	1394.
Reference	Silva, Pott, et al., 2010	Usman, Zubair, et al., 2010	Xu, Tang, et al., 2010	Benites, Moiteiro, et al., 2009	Benites, Moiteiro, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-54	DB-5	SPB-5	DB-5	HP-5 MS
Column length (m)	30.	30.	60.	30.	30.
Carrier gas	Helium	Helium	Nitrogen	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.35	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	35.	60.	50.	35.
T_end (C)	260.	220.	230.	250.	195.
Heat rate (K/min)	2.	3.	4.	5.	2.
Initial hold (min)	5.			2.	5.
Final hold (min)	999.	40.	40.		30.
I	1387.	1391.	1403.	1391.	1387.
Reference	Dayisoylu and Alma, 2009	El-Massry, El-Ghorab, et al., 2009	Gauvin-Bialecki and Marodon, 2009	Ho, Wang, et al., 2009	Kim and Chung, 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5 MS	HP-5	DB-5	VF-1 MS	HP-5
Column length (m)	30.	30.	30.	30.	25.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.20
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.33
T_start (C)	50.	50.	70.	60.	60.
T_end (C)	250.	280.	240.	280.	240.
Heat rate (K/min)	2.	5.	5.	4.	3.
Initial hold (min)	5.	2.		5.
Final hold (min)		5.		10.	7.
I	1388.	1391.	1383.	1391.	1393.
Reference	Koba, Sanda, et al., 2009	Lago, Favero, et al., 2009	Lawal and Oyedelji, 2009	Marchesini, Prada, et al., 2009	Maridass, 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	RTX-1	BP-1	DB-5	DB-5 MS
Column length (m)	60.	60.	50.	30.	30.
Carrier gas	Helium	Helium	Helium	Nitrogen	Helium
Substrate
Column diameter (mm)	0.22	0.22	0.22	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	40.	50.
T_end (C)	230.	230.	220.	230.	220.
Heat rate (K/min)	2.	2.	2.	2.	3.
Initial hold (min)					2.
Final hold (min)	30.	30.	20.		70.
I	1385.	1389.	1391.	1391.	1385.
Reference	Museli, Pau, et al., 2009	Museli, Pau, et al., 2009	Ottavioli, Bighelli, et al., 2009	Scrivanti, Anton, et al., 2009	Shimizu, Imayoshi, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5 MS	HP-5MS	HP-5 MS	HP-5 MS	HP-5 MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	50.	60.	50.	70.
T_end (C)	250.	240.	300.	280.	210.
Heat rate (K/min)	4.	5.	15.	4.	5.
Initial hold (min)	2.		2.		1.
Final hold (min)	2.		10.		5.
I	1391.	1391.	1421.	1394.	1397.
Reference	Su, Wang, et al., 2009	Wannes, Mhamdi, et al., 2009	Xu, Han, et al., 2009	Zhao, Zeng, et al., 2009	Bouwmeester, de Kraker, et al., 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-52	HP-5	HP-5	HP-5	SLB-5 MS
Column length (m)	50.	30.	30.	30.	30.
Carrier gas	Helium	N2	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	100.	50.
T_end (C)	280.	220.	300.	240.	250.
Heat rate (K/min)	3.	5.	3.	5.	3.
Initial hold (min)		10.		2.	2.
Final hold (min)	20.		30.	5.	10.
I	1396.	1392.	1387.	1391.	1391.
Reference	Djarri, Medjroubi, et al., 2008	Flamini, Tebano, et al., 2008	Isidorov, Lech, et al., 2008	Lago, Romoff, et al., 2008	Lo Presti, Sciarrone, et al., 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	ZB-1	DB-5	DB-5 MS	RTX-1	Elite-1
Column length (m)	30.	60.	30.	60.	30.
Carrier gas	Nitrogen	Nitrogen	Helium	He	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.22	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	45.	60.	50.	60.	60.
T_end (C)	230.	250.	300.	230.	246.
Heat rate (K/min)	3.	5.	5.	2.	3.
Initial hold (min)			5.
Final hold (min)		10.	5.	35.
I	1387.	1400.	1383.	1387.	1388.
Reference	Mierendorff, Stahl-Biskup, et al., 2008	Mosayebi, Amin, et al., 2008	Noudogbessi, Yedomonhan, et al., 2008	Paolini, Tomi, et al., 2008	Raj, Baby, et al., 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BPX-5	RTX-5	HP-5	HP-5	HP-5 MS
Column length (m)	7.5	20.	25.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.10	0.18	0.25	0.25	0.25
Phase thickness (μm)	10.	0.20	0.25	0.32	0.25
T_start (C)	60.	50.	60.	60.	50.
T_end (C)	240.	280.	240.	250.	230.
Heat rate (K/min)	3.	4.	4.	5.	3.
Initial hold (min)		1.	2.	30.	10.
Final hold (min)					10.
I	1395.	1403.	1390.	1392.	1389.
Reference	Shellie, 2008	Skalicka-Wozniak, Los, et al., 2008	Verdian-rizi, 2008	Yassa and Akhani, 2008	Adams, Beauchamp, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5MS	CP Sil 5 CB	HP-5MS	DB-5
Column length (m)	50.	30.	30.	30.	30.
Carrier gas	Nitrogen	He	N2	He	He
Substrate
Column diameter (mm)	0.20	0.25	0.32	0.25	0.26
Phase thickness (μm)	0.32	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	220.	240.	300.	280.	240.
Heat rate (K/min)	5.	3.	4.	3.	3.
Initial hold (min)	3.
Final hold (min)	5.
I	1388.	1390.	1392.	1383.	1387.
Reference	Amiri, 2007	Andrade, Oliveira, et al., 2007	Baran, von Reuss, et al., 2007	Basta, Pavlovic, et al., 2007	Bos, Woerdenbag, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	DB-5MS	RTX-5 MS	DB-5	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	He	He	Helium	Helium
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.26	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.26
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	280.	240.	200.	290.	240.
Heat rate (K/min)	4.	3.	2.	3.	4.
Initial hold (min)	5.		2.		2.
Final hold (min)			10.		20.
I	1390.	1390.	1385.	1387.	1396.
Reference	Capetanos, Saroglou, et al., 2007	Da Silva J.K.R., Sousa P.J.C., et al., 2007	Edris, Chizzola, et al., 2007	Elfami, Bos, et al., 2007	Farsam, Amanlou, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	Col-Elite 5MS	HP-1	HP-101	BP-1
Column length (m)	30.	30.	30.	25.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.2
T_start (C)	60.	30.	60.	70.	60.
T_end (C)	250.	246.	240.	200.	220.
Heat rate (K/min)	2.	3.	2.	3.	5.
Initial hold (min)	8.			2.
Final hold (min)	15.		20.		6.
I	1387.	1399.	1376.	1359.	1389.
Reference	Ferhat, Tigrine-Kordjani, et al., 2007	Gudaityte and Venskutonis R.P., 2007	Hachicha, Skanji, et al., 2007	Jerkovic, Mastelic, et al., 2007	Kiran, Devi, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-30	HP-5	DB-5	ZB-5	DB-1
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He		Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	40.	60.	60.	50.
T_end (C)	250.	250.	240.	220.	260.
Heat rate (K/min)	5.	5.	2.	4.	2.5
Initial hold (min)	5.	5.		5.	1.
Final hold (min)	10.	10.		20.	20.
I	1379.	1387.	1383.	1386.	1377.
Reference	Loizzo, Tundis, et al., 2007	Loizzo, Tundis, et al., 2007	Miyazawa and Tamura, 2007	Mohottalage, Tabacchi, et al., 2007	Monser-Esfahani, Karamkhani, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	DB-1	HP-5 MS	SPB-5
Column length (m)	30.	25.	30.	25.	30.
Carrier gas	Helium	H2		Helium	He
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.33	0.15	0.25	0.25
T_start (C)	60.	60.	60.	100.	50.
T_end (C)	220.	240.	220.	280.	250.
Heat rate (K/min)	4.	3.	3.	4.	2.
Initial hold (min)				3.
Final hold (min)				5.
I	1393.	1392.	1380.	1396.	1394.
Reference	Morteza-Semnani, Saeedi, et al., 2007	Oliveira, Leitão, et al., 2007	Ouattara, Koudou, et al., 2007	Phutdhawong, Kawaree, et al., 2007	Raal, Orav, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BPX-5	BPX-5	HP-5	DB-5	DB-5
Column length (m)	50.	50.	30.	30.	30.
Carrier gas	He	He	Helium
Substrate
Column diameter (mm)	0.22	0.22	0.25	0.25	0.25
Phase thickness (μm)		1.	0.25	0.25	0.25
T_start (C)	50.	50.	40.	40.	40.
T_end (C)	300.	300.	260.	210.	250.
Heat rate (K/min)	4.	4.	4.	2.	2.
Initial hold (min)	1.	1.
Final hold (min)	10.	10.		33.	33.
I	1420.	1420.	1387.	1389.	1389.
Reference	Rali, Wossa, et al., 2007	Rali, Wossa, et al., 2007, 2	Ristic, Krivokuca-Dokic, et al., 2007	Sylvestre, Longtin, et al., 2007	Sylvestre, Pichette, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5	HP-5MS	DB-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.32	0.25	0.25	0.25
T_start (C)	60.	60.	40.	60.	60.
T_end (C)	280.	250.	260.	300.	300.
Heat rate (K/min)	3.	5.	4.	3.	3.
Initial hold (min)		30.
Final hold (min)
I	1391.	1392.	1388.0	1381.	1385.
Reference	Vagionas, Graikou, et al., 2007	Yassa and Akhani, 2007	Zizovic, Stamenic, et al., 2007	Apel, Sobral, et al., 2006	Apel, Sobral, et al., 2006, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	BP-1	BP-1	HP-5MS
Column length (m)	30.	60.	50.	50.	30.
Carrier gas	He	He	He		He
Substrate
Column diameter (mm)	0.25	0.25	0.22	0.22	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	60.	60.	60.
T_end (C)	265.	250.	220.	220.	280.
Heat rate (K/min)	2.5	3.	2.	2.	3.
Initial hold (min)	1.
Final hold (min)	20.		20.	20.
I	1392.	1397.	1384.	1388.	1391.
Reference	Bazargani, Almasirad, et al., 2006	Bertrand, Comte, et al., 2006	Boti, Muselli, et al., 2006	Boti, Yao, et al., 2006	Bozin, Mimicá-Dukic, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-1	HP-1	HP-1	HP-1	HP-1
Column length (m)	50.	50.	50.	50.	50.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.2	0.2	0.2	0.2	0.2
Phase thickness (μm)	0.33	0.33	0.33	0.5	0.33
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	250.	250.	250.	250.	250.
Heat rate (K/min)	2.	2.	2.	2.	2.
Initial hold (min)	4.	4.	4.		4.
Final hold (min)	30.	30.	30.	120.	30.
I	1386.	1383.	1387.	1385.	1385.
Reference	Castel, Fernandez, et al., 2006	Castel, Fernandez, et al., 2006	Castel, Fernandez, et al., 2006	Castel, Fernandez, et al., 2006, 2	Castel, Fernandez, et al., 2006, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-1	DB-5	HP-5	DB-5	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	N2	He
Substrate
Column diameter (mm)	0.20	0.25	0.32	0.32	0.25
Phase thickness (μm)	0.20	0.25	0.25	0.25	0.25
T_start (C)	70.	70.	60.	60.	60.
T_end (C)	220.	230.	246.	230.	280.
Heat rate (K/min)	3.	2.	3.	3.	4.
Initial hold (min)		2.
Final hold (min)	15.	20.		15.
I	1382.	1393.	1390.	1391.	1388.
Reference	Cavaleiro, Pinto, et al., 2006	Choi, 2006	Coronel, Cerda-Garcia-Rojas, et al., 2006	Damjanovic, Skala, et al., 2006	Ebrahim Sajjadi and Mehregan, 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	BP-1	HP-1	HP-5	DB-5
Column length (m)	30.	50.	50.	30.	30.
Carrier gas	Helium	He	He	He
Substrate
Column diameter (mm)	0.26	0.22	0.2	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.33	0.25	0.25
T_start (C)	60.	60.	60.	50.	40.
T_end (C)	290.	220.	250.	300.	210.
Heat rate (K/min)	3.	2.	2.	5.	2.
Initial hold (min)				5.	2.
Final hold (min)		20.	60.	5.	33.
I	1387.	1388.	1394.	1389.	1389.
Reference	Elfami, Komar, et al., 2006	Fanciullino, Tomi, et al., 2006	Fernandez, Pintaric, et al., 2006	Figuérédo, Cabassu, et al., 2006	Garneau F.X., Collin G., et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	BP-1	RTX-1	DB-1
Column length (m)	30.	30.		30.	60.
Carrier gas	He	Helium	Helium	He
Substrate
Column diameter (mm)	0.25	0.25		0.32	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	50.	60.	60.	60.	70.
T_end (C)	250.	260.	220.	300.	230.
Heat rate (K/min)	3.	3.	5.	4.	2.
Initial hold (min)					2.
Final hold (min)	10.		6.		20.
I	1391.	1391.	1389.	1396.	1416.
Reference	Havlik, Kokoska, et al., 2006	Javidnia, Miri, et al., 2006	Kiran, Bhavani, et al., 2006	Kula, Izydorczyk, et al., 2006	Lan Phi N.T., Nishiyama C., et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	CP Sil 5 CB	CP Sil 5 CB	5 % Phenyl methyl siloxane	DB-5
Column length (m)	50.	30.	30.	30.	30.
Carrier gas	He	N2	N2	Helium	Helium
Substrate
Column diameter (mm)	0.22	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	50.	60.	50.
T_end (C)	220.	300.	200.	280.	250.
Heat rate (K/min)	2.	4.	5.	3.	3.
Initial hold (min)					5.
Final hold (min)	20.			30.
I	1387.	1382.	1391.	1363.	1391.
Reference	Lesueur, Ban, et al., 2006	Lis and Milczarek, 2006	Martin, Joseph, et al., 2006	Marongiu, Piras, et al., 2006	Mirza, Navaei, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	DB-5	NB-30
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He		He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	50.	50.
T_end (C)	220.	220.	220.	265.	250.
Heat rate (K/min)	4.	4.	4.	2.5	2.
Initial hold (min)		5.	5.	0.5
Final hold (min)
I	1394.	1393.	1393.	1394.	1388.
Reference	Morteza-Semnani, Akbarzadeh, et al., 2006	Morteza-Semnani K., Akbarzadeh M., et al., 2006	Morteza-Semnani K., Saeedi M., et al., 2006	Nickavar B., Kamalinejad M., et al., 2006	Orav, Raal, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	DB-5	DB-5	DB-5
Column length (m)	25.	30.	30.	30.	30.
Carrier gas	N2	He	Hydrogen	Hydrogen	Hydrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.15	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	70.	70.	70.
T_end (C)	200.	220.	280.	280.	280.
Heat rate (K/min)	4.	5.	4.	4.	4.
Initial hold (min)	3.	10.	4.	4.	4.
Final hold (min)
I	1400.	1383.	1392.	1391.	1391.
Reference	Ouamba, Ouabonzi, et al., 2006	Pintore G., Chessa M., et al., 2006	Pino, Marbot, et al., 2006	Pino, Marbot, et al., 2006	Pino, Marbot, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5	DB-5	DB-5	DB-5
Column length (m)	30.	25.	30.	30.	30.
Carrier gas	He	H2	He	He	He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	280.	240.	200.	200.	260.
Heat rate (K/min)	3.	3.	2.	2.	5.
Initial hold (min)
Final hold (min)			60.	60.
I	1354.	1394.	1391.	1392.	1399.
Reference	Pitarokili, Tzakou, et al., 2006	Potzernheim, Bizzo, et al., 2006	Rout, Naik, et al., 2006	Rout, Naik, et al., 2006	Sabulal, Dan, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	DB-1	CP Sil 5 CB	SPB-1
Column length (m)	60.	30.	60.	25.	50.
Carrier gas	He	He	Helium	H2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.2
Phase thickness (μm)		0.25	0.25		0.33
T_start (C)	40.	40.	60.	50.	50.
T_end (C)	250.	260.	250.	230.	220.
Heat rate (K/min)	4.	2.	5.	3.	4.
Initial hold (min)		5.			1.
Final hold (min)		20.	10.		10.
I	1385.	1387.	1389.	1392.	1384.
Reference	Sefidkon, Jamzad, et al., 2006	Senatore, Landolfi, et al., 2006	Sonboli, Mirjalili, et al., 2006	Tesso, König, et al., 2006	Wong, Lim, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-30	HP-5MS	DB-5	DB-5	DB-5
Column length (m)	30.	30.	50.	30.	30.
Carrier gas	He	He		He	He
Substrate
Column diameter (mm)		0.25	0.3	0.25	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	90.	60.	60.	60.	60.
T_end (C)	220.	275.	240.	240.	240.
Heat rate (K/min)	7.	4.	2.	3.	3.
Initial hold (min)	2.
Final hold (min)
I	1391.	1391.	1390.	1393.	1393.
Reference	Ahuja, Bakshi, et al., 2005	Asadipour, Mehrabani, et al., 2005	Chagonda and Chalchat, 2005	Chaverri and Cicció, 2005	Chaverri and Cicció, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-1	CP Sil 8 CB	DB-1	DB-5
Column length (m)	25.	30.	30.	60.	30.
Carrier gas	He	He	He	N2	He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.33	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	80.	60.	60.
T_end (C)	240.	250.	200.	250.	300.
Heat rate (K/min)	3.	5.	3.	5.	3.
Initial hold (min)		5.	5.		3.
Final hold (min)	7.	15.	5.	10.
I	1387.	1345.	1389.	1400.	1384.
Reference	Duarte, Figueira, et al., 2005	Facundo, Pinto, et al., 2005	Facey, Porter, et al., 2005	Fakhari A.R., Sonboli A., et al., 2005	Ferraz, Limberger, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5MS	HP-5MS	CP Sil 5 CB	HP-5
Column length (m)	30.	25.	30.	30.	25.
Carrier gas	He	He	He	N2	H2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25		0.25	0.25	0.52
T_start (C)	60.	50.	60.	60.	40.
T_end (C)	200.	250.	300.	250.	240.
Heat rate (K/min)	4.	3.	3.	5.	4.
Initial hold (min)	30.	3.
Final hold (min)		10.		10.
I	1386.	1390.	1390.	1397.	1389.
Reference	Gauvin and Smadja, 2005	Ghasemi Y., Faridi P., et al., 2005	Grombone-Guaratini, Silva-Brandão, et al., 2005	Jassbi, Mehrdad, et al., 2005	Jovanovic, Kitic, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	DB-5	DB-5MS	DB-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He		Helium	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	35.	35.	60.	60.
T_end (C)	265.	280.	280.	280.	280.
Heat rate (K/min)	2.5	4.	4.	3.	3.
Initial hold (min)	1.	2.	2.	30.	30.
Final hold (min)	20.
I	1373.	1396.	1396.	1367.	1368.
Reference	Khanavi, Ghasemian, et al., 2005	Kowalski and Wolski, 2005	Kowalski, 2005	Marongiu, Piras, et al., 2005	Marongiu, Piras, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	HP-5	DB-1	DB-1
Column length (m)	30.	30.	30.	50.	50.
Carrier gas	He	He	He	N2	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25		0.25	0.25	0.25
T_start (C)	60.	40.	70.	95.	95.
T_end (C)	220.	220.	240.	240.	240.
Heat rate (K/min)	4.	4.	5.	4.	4.
Initial hold (min)	4.	1.
Final hold (min)
I	1393.	1388.	1401.	1387.	1387.
Reference	Morteza-Semnani and Saeedi, 2005	de Oliveira, Dias, et al., 2005	Oyedeji, Yani, et al., 2005	Palá-Paúl, Pérez-Alonso, et al., 2005	Pala-Paul, Perez-Alonso, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-5 MS	HP-5MS	CP Sil 5 CB	HP-5MS	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He		He	He	He
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.25		0.25	0.25	0.25
T_start (C)	50.	60.	40.	60.	60.
T_end (C)	280.	280.	220.	280.	275.
Heat rate (K/min)	8.	3.	4.	4.	4.
Initial hold (min)	2.		1.
Final hold (min)	2.
I	1401.	1391.	1403.	1390.	1392.
Reference	Pellati, Benvenuti, et al., 2005	Petrakis, Roussis, et al., 2005	Rohloff and Bones, 2005	Sajjadi S.E. and Eskandari B., 2005	Sajjadi and Ghannadi, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5MS	DB-5MS	DB-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	60.	60.	60.
T_end (C)	265.	280.	240.	300.	300.
Heat rate (K/min)	2.5	3.	3.	3.	3.
Initial hold (min)	1.	5.
Final hold (min)	20.
I	1376.	1392.	1391.	1385.	1385.
Reference	Sarkhail, Amin, et al., 2005	Setzer, Noletto, et al., 2005	da Silva, Andrade, et al., 2005	Simoes-Pires C.A., Debenedetti S., et al., 2005	Simoes-Pires C.A., Debenedetti S., et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	RTX-1	RTX-5	HP-5 MS	DB-5
Column length (m)	30.	60.	30.	30.	30.
Carrier gas	He	He		He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.50	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	280.	25.	220.	260.	280.
Heat rate (K/min)	3.	5.	3.	3.	3.
Initial hold (min)
Final hold (min)		10.		20.
I	1392.	1392.	1392.	1393.	1361.
Reference	Slavkovska, Couladis, et al., 2005	Sonboli, Salehi, et al., 2005	Szafranek, Chrapkowska, et al., 2005	Topçu, Barla, et al., 2005	Tzakou and Constantinidis, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	HP-5MS	SPB-1	HP-5
Column length (m)	50.	50.	30.	50.	30.
Carrier gas	N2			He	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.2	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.33	0.25
T_start (C)	90.	60.	40.	50.	40.
T_end (C)	240.	240.	220.	220.	250.
Heat rate (K/min)	4.	3.	3.	4.	5.
Initial hold (min)			5.	3.	2.
Final hold (min)			10.	30.	5.
I	1372.	1370.	1403.	1387.	1386.
Reference	Velasco-Negueruela, Pérez-Alonso, et al., 2005	Velasco-Negueruela, Pérez-Alonso, et al., 2005, 2	Vichi, Riu-Aumatell, et al., 2005	Wong, Lee, et al., 2005	N/A
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	SPB-5	DB-5	DB-5
Column length (m)	30.	30.	60.	30.	25.
Carrier gas	He	N2	He	N2	Nitrogen
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25	1.	0.25	0.25
T_start (C)	90.	50.	60.	40.	60.
T_end (C)	220.	200.	200.	230.	240.
Heat rate (K/min)	7.	5.	4.	2.	3.
Initial hold (min)	2.
Final hold (min)	5.		30.
I	1390.	1394.	1401.	1394.	1391.
Reference	Agnihotri, Thappa, et al., 2004	Fekam Boyom, Fotio, et al., 2004	Gauvin, Ravaomanarivo, et al., 2004	González, Guerra, et al., 2004	JAvidnia, Mojab, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	SE-54	DB-5	DB-5MS	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	N2	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	300.	260.	300.	240.	300.
Heat rate (K/min)	4.	2.	3.	3.	3.
Initial hold (min)		5.
Final hold (min)
I	1390.	1386.	1378.	1375.	1403.
Reference	Kalemba and Thiem, 2004	Kilic, Hafizoglu, et al., 2004	Lago, de Ávila, et al., 2004	paz Lima, Silva, et al., 2004	Limberger, Sobral, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	DB-5MS	HP-5MS	DB-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	N2	He	He		Helium
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.15
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	300.	280.	275.	220.	240.
Heat rate (K/min)	4.	3.	4.	3.	2.
Initial hold (min)				3.
Final hold (min)		30.			999.
I	1386.	1358.	1393.	1385.	1386.
Reference	Lis, Boczek, et al., 2004	Marongiu, Porcedda, et al., 2004	Mehrabani, Asadipour, et al., 2004	Mevy, Bessiere, et al., 2004	Miyazawa, Fuhita, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	NB-30	NB-30	DB-1
Column length (m)	50.	60.	50.	50.	50.
Carrier gas	Helium	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.2	0.22
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	60.	50.	50.	50.	70.
T_end (C)	240.	270.	250.	250.	220.
Heat rate (K/min)	2.	4.	2.	2.	4.
Initial hold (min)
Final hold (min)	999.
I	1386.	1388.	1386.	1388.	1390.
Reference	Miyazawa, Fujita, et al., 2004	Nik, Mirza, et al., 2004	Orav, Stulova, et al., 2004	Orav, Stulova, et al., 2004	Palá-Paúl, García-Jiménez, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	NB-30	HP-5MS	DB-1	HP-1
Column length (m)	50.	50.	30.	30.	30.
Carrier gas	N2	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.20	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.33
T_start (C)	95.	50.	60.	50.	40.
T_end (C)	240.	250.	280.	265.	260.
Heat rate (K/min)	4.	2.	4.	2.5	2.
Initial hold (min)				1.	5.
Final hold (min)				20.	20.
I	1385.	1385.	1390.	1376.	1362.
Reference	Palá-Paúl, Velasco-Negueruela, et al., 2004	Raal, Paaver, et al., 2004	Sajjadi and Shahpiri, 2004	Sarkhail, Amin, et al., 2004	Senatore, Napolitano, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-5	CP Sil 5 CB	DB-5	CP Sil 8 CB
Column length (m)	25.	30.	20.	30.	30.
Carrier gas	H2		He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.52	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	100.	60.	50.
T_end (C)	240.	300.	270.	300.	200.
Heat rate (K/min)	4.	3.	8.	3.	5.
Initial hold (min)			2.		5.
Final hold (min)
I	1391.	1380.	1391.	1391.	1394.
Reference	Simic, Sokovic, et al., 2004	Suyenaga, Apel, et al., 2004	Thappa, Bakshi, et al., 2004	Tirillini, Pellegrino, et al., 2004	Wang, Guo, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	RTX-5Sil	DB-5	HP-5MS	HP-1
Column length (m)	30.	30.	60.	30.	30.
Carrier gas	N2	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	60.	70.	50.	60.	70.
T_end (C)	220.	200.	220.	220.	200.
Heat rate (K/min)	5.	4.	3.	5.	10.
Initial hold (min)	10.			20.
Final hold (min)		10.		20.
I	1402.	1389.	1398.	1399.	1394.
Reference	Bertoli, Menichini, et al., 2003	Dudai, Larkov, et al., 2003	Edris and Farrag, 2003	Feizbaksh, Saber Tehrani, et al., 2003	Fekam Boyom, Amvam Zollo, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-1	HP-5MS	RSL-200	RSL-200
Column length (m)	30.	50.	30.	30.	30.
Carrier gas	N2	He	He	H2	H2
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.32	0.32
Phase thickness (μm)	0.25	0.5	0.25	0.25	0.25
T_start (C)	50.	60.	60.	40.	40.
T_end (C)	200.	220.	280.	280.	280.
Heat rate (K/min)	5.	2.	4.	6.	6.
Initial hold (min)				5.	5.
Final hold (min)		45.		5.	5.
I	1374.	1394.	1391.	1390.	1399.
Reference	Fekam Boyom, Ngouana, et al., 2003	Fernandez, Lizzani-Cuvelier, et al., 2003	Ghasemi, Asghari, et al., 2003	Jirovetz, Buchbauer, et al., 2003	Jirovetz, Buchbauer, et al., 2003, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	DB-5	DB-5	ZB-1
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	N2	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	80.	60.	60.	45.
T_end (C)	250.	250.	280.	280.	230.
Heat rate (K/min)	3.	4.	3.	3.	3.
Initial hold (min)
Final hold (min)			30.	30.
I	1403.	1368.	1383.	1382.	1387.
Reference	Limberger, Simões-Pires, et al., 2003	Mahalwal and Ali, 2003	Marongiu, Porcedda, et al., 2003	Marongiu, Porcedda, et al., 2003	Mierendorff, Stahl-Biskup, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5	DB-5	CP Sil 5 CB	DB-5
Column length (m)	60.	30.	30.	25.	30.
Carrier gas	He	Helium	He	H2	H2
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25		0.25	0.15	0.25
T_start (C)	50.	70.	60.	50.	60.
T_end (C)	270.	210.	275.	230.	280.
Heat rate (K/min)	4.	2.	4.	3.	4.
Initial hold (min)			5.		10.
Final hold (min)		60.			40.
I	1384.	1387.	1391.	1376.	1392.
Reference	Mirza and Nik, 2003	Mookdasanit, Tamura, et al., 2003	Morteza-Semnani and Saeedi, 2003	Oyedeji, Ekundayo, et al., 2003	Pino, Marbot, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	HP-5	DB-1	DB-5
Column length (m)	30.	30.	30.	60.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	75.	60.	60.	50.	60.
T_end (C)	220.	280.	280.	280.	240.
Heat rate (K/min)	3.	4.	4.	4.	3.
Initial hold (min)	4.
Final hold (min)
I	1389.	1390.	1388.	1386.	1392.
Reference	Priestap, van Baren, et al., 2003	Sajjadi and Mehregan, 2003	Sajjadi and Mehregan, 2003, 2	Shahmir, Ahmadi, et al., 2003	da Silva, Luz, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5MS	HP-5	HP-5	DB-5	DB-5
Column length (m)	30.	25.	25.	30.	30.
Carrier gas	He	Helium	Helium	He	He
Substrate
Column diameter (mm)	0.25	0.32	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.53	0.53	0.25	0.25
T_start (C)	60.	40.	40.	60.	60.
T_end (C)	240.	280.	280.	240.	240.
Heat rate (K/min)	3.	4.	4.	3.	3.
Initial hold (min)
Final hold (min)
I	1392.	1388.	1391.	1390.	1394.
Reference	Taveira, de Lima, et al., 2003	Velickovic, Ristic, et al., 2003	Velickovic, Ristic, et al., 2003	Zoghbi, Andrade, et al., 2003	Zoghbi, Andrade, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	OV-101	DB-5	HP-1
Column length (m)	25.	30.	25.	30.	30.
Carrier gas	N2	He		He	He
Substrate
Column diameter (mm)	0.25	0.249	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	50.	60.	50.	60.	70.
T_end (C)	250.	300.	200.	280.	220.
Heat rate (K/min)	4.	3.	5.	3.	3.
Initial hold (min)
Final hold (min)	10.	5.		30.	15.
I	1392.	1391.	1394.	1383.	1382.
Reference	Zrira, Elamrani, et al., 2003	Bos, Koulman, et al., 2002	Boyom, Keumedjio, et al., 2002	Caredda, Marongiu, et al., 2002	Cavaleiro, Salgueiro, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	5 % Phenyl methyl siloxane	DB-5MS	DB-5MS	BP-1	DB-1
Column length (m)	30.	30.	30.	25.	30.
Carrier gas	He	He	He	N2	H2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.50	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	75.	60.	60.	60.	40.
T_end (C)	200.	280.	280.	220.	245.
Heat rate (K/min)	3.	3.	3.	5.	3.
Initial hold (min)	4.				20.
Final hold (min)	8.			10.
I	1391.	1392.	1392.	1390.	1387.
Reference	Cicció and Gómez-Laurito, 2002	Congiu, Falconieri, et al., 2002	Congiu, Falconieri, et al., 2002	Das, Ram, et al., 2002	Gancel, Ollé, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	MDN-5	RSL-200	RSL-200	DB-1	DB-5
Column length (m)	30.	30.	30.	25.	30.
Carrier gas		H2	H2	He	He
Substrate
Column diameter (mm)	0.25	0.32	0.32	0.23	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.20	0.25
T_start (C)	40.	40.	50.	50.	60.
T_end (C)	280.	280.	280.	200.	240.
Heat rate (K/min)	8.	6.	6.	3.	3.
Initial hold (min)	3.	5.	5.	3.
Final hold (min)		5.	5.	30.
I	1389.	1391.	1401.	1394.	1390.
Reference	Jelén, 2002	Jirovetz, Buchbauer, et al., 2002	Jirovetz, Ngassoum, et al., 2002	Khallouki, Younos, et al., 2002	Kobaisy, Tellez, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	OV-101	DB-5	HP-5	DB-5
Column length (m)	30.	25.	30.	30.	25.
Carrier gas	He	He	He		N2
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.23
Phase thickness (μm)	0.25		0.25	0.25	0.15
T_start (C)	35.	50.	60.	60.	50.
T_end (C)	280.	200.	250.	275.	250.
Heat rate (K/min)	3.	5.	3.	4.	3.
Initial hold (min)	2.			4.
Final hold (min)	15.
I	1395.	1394.	1385.	1385.	1387.
Reference	Krauze-Baranowska, Mardarowicz, et al., 2002	Kuiate, Bessière, et al., 2002	Limberger, Simões-Pires, et al., 2002	Lockwood, Asghari, et al., 2002	Mahmout, Bessière, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5MS	DB-1	HP-1	DB-5
Column length (m)	30.	30.	30.	50.	25.
Carrier gas	He	He	He	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	90.	60.
T_end (C)	240.	240.	250.	220.	220.
Heat rate (K/min)	3.	3.	4.	3.	3.
Initial hold (min)			10.
Final hold (min)
I	1394.	1395.	1397.	1388.	1393.
Reference	Maia, da Silva, et al., 2002	Maia, Zoghbi, et al., 2002	Norouzi-Arasi, Yavari, et al., 2002	Priestap, van Baren, et al., 2002	Schwob, Bessière, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	DB-1	DB-5MS	DB-5
Column length (m)	60.	60.	50.	30.	30.
Carrier gas	He	He	N2	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	40.	40.	60.	60.	60.
T_end (C)	250.	280.	240.	270.	240.
Heat rate (K/min)	4.	4.	3.	3.	3.
Initial hold (min)		5.
Final hold (min)
I	1380.	1384.	1368.	1392.	1393.
Reference	Sefidkon, Dabiri, et al., 2002	Sefidkon, 2002	Velasco-Negueruela, Pérez-Alonso, et al., 2002	Zoghbi, Andrade, et al., 2002	Zoghbi, Andrade, et al., 2002, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	Optima-5	RTX-1	BP-1	CBP-1
Column length (m)	60.	30.	30.	50.	25.
Carrier gas	N2	He	N2	He	Nitrogen
Substrate
Column diameter (mm)	0.248	0.2	0.25	0.22	0.25
Phase thickness (μm)	0.25		0.25	0.25	0.25
T_start (C)	60.	50.	60.	60.	50.
T_end (C)	220.	250.	300.	230.	210.
Heat rate (K/min)	3.	3.	4.	2.	3.
Initial hold (min)	5.	3.			2.
Final hold (min)	22.			35.
I	1382.	1396.	1387.	1388.	1382.
Reference	Bailac, Dellacasa, et al., 2001	Jacquemond-Collet, Bessière, et al., 2001	Kalemba, Marschall, et al., 2001	Lota, de Rocca Serra, et al., 2001	Ly, Yamauchi, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5MS	DB-5MS	DB-1	DB-5	DB-1
Column length (m)	30.	30.	60.	30.	30.
Carrier gas	He	He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	60.	80.
T_end (C)	240.	240.	270.	270.	225.
Heat rate (K/min)	3.	3.	4.	3.	4.
Initial hold (min)
Final hold (min)	30.	30.
I	1343.	1353.	1384.	1394.	1376.
Reference	Marongiu, Porcedda, et al., 2001	Marongiu, Porcedda, et al., 2001	Mirza, Ahmadi, et al., 2001	Palmeira, Conserva, et al., 2001	Palá-Paúl, Pérez-Alonso, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	OV-101	CP Sil 5 CB	DB-1	CP Sil 5 CB
Column length (m)	30.	50.	25.	60.	25.
Carrier gas	He	N2		N2	He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.25	0.25
Phase thickness (μm)			0.15	0.25	0.4
T_start (C)	60.	80.	50.	60.	60.
T_end (C)	240.	200.	230.	220.	260.
Heat rate (K/min)	3.	2.	3.	3.	5.
Initial hold (min)				5.	40.
Final hold (min)				22.
I	1390.5	1385.	1392.	1392.	1385.
Reference	Santos, Moreira, et al., 2001	Yang, 2001	Asekun and Ekundayo, 2000	Bailac, Dellacasa, et al., 2000	Baser, Özek, et al., 2000
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	SPB-1	DB-1	RSL-200	DB-1
Column length (m)	33.	30.	30.	60.	25.
Carrier gas	N2	He		H2	Nitrogen
Substrate
Column diameter (mm)	0.25	0.2	0.32	0.32	0.50
Phase thickness (μm)	0.50	0.2	0.25	0.25	0.25
T_start (C)	50.	80.	45.	40.	60.
T_end (C)	135.	300.	300.	250.	220.
Heat rate (K/min)	20.	5.	15.	6.	5.
Initial hold (min)	2.	3.	2.
Final hold (min)			5.
I	1404.	1391.	1380.	1400.	1389.
Reference	Feger, Brandauer, et al., 2000	Fraternale, Giamperi, et al., 2000	Hedin, McKibben, et al., 2000	Jirovetz, Puschmann, et al., 2000	Mallavarapu, Rao, et al., 2000
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-1	DB-5	HP-5	OV-101	CP Sil 5 CB
Column length (m)	60.	30.	30.	50.	25.
Carrier gas	He	N2	He	Nitrogen	H2
Substrate
Column diameter (mm)	0.25	0.22	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25		0.15
T_start (C)	60.	70.	40.	40.	50.
T_end (C)	200.	230.	240.	200.	320.
Heat rate (K/min)	4.	4.	3.	2.	3.
Initial hold (min)	5.	2.	5.	10.
Final hold (min)	25.	20.
I	1399.	1384.	1395.	1390.	1381.
Reference	Meccia, Rojas, et al., 2000	Mitiku, Sawamura, et al., 2000	Novak, Novak, et al., 2000	Tamura, Boonbumrung, et al., 2000	Asekun and Ekundayo, 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	Ultra-2	DB-1	CBP-1	OV-1
Column length (m)	25.	50.	25.	25.	25.
Carrier gas	N2		He	He	H2
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.3	0.25
Phase thickness (μm)			0.25		0.25
T_start (C)	50.	32.	50.	60.	40.
T_end (C)	200.	250.	290.	240.	220.
Heat rate (K/min)	5.	4.	4.	4.	3.
Initial hold (min)		5.			5.
Final hold (min)					5.
I	1391.	1386.	1391.	1394.	1374.
Reference	Ayedoun, Adéoti, et al., 1999	Khalilov L.M., Khalilova A.Z., et al., 1999	Koulman, 1999	Labuckas, Zygadlo, et al., 1999	Oberhofer, Nikiforov, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	BP-1	CP Sil 5 CB	DB-5	DB-5MS
Column length (m)	50.	25.	25.	30.	30.
Carrier gas	He	N2	He	He	He
Substrate
Column diameter (mm)	0.25	0.5	0.25	0.25	0.25
Phase thickness (μm)	0.25		0.39	0.25	0.25
T_start (C)	70.	60.	60.	60.	60.
T_end (C)	240.	220.	220.	240.	240.
Heat rate (K/min)	4.	5.	5.	3.	3.
Initial hold (min)			5.
Final hold (min)		10.	20.
I	1377.	1389.	1390.	1391.	1392.
Reference	Palá-Paúl, Pérez-Alonso, et al., 1999	Rao, Bhattacharya, et al., 1999	Rustaiyan, Masoudi, et al., 1999	Tellez, Canel, et al., 1999	Zoghbi, Andrade, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	SPB-5	DB-5	DB-5	DB-5
Column length (m)	50.	50.	30.	30.	30.
Carrier gas	He	He	He	He	Helium
Substrate
Column diameter (mm)	0.22	0.32	0.25	0.25	0.25
Phase thickness (μm)	1.	0.25	0.25	0.25	0.25
T_start (C)	100.	60.	60.	60.	60.
T_end (C)	220.	240.	240.	240.	240.
Heat rate (K/min)	1.	3.	3.	3.	3.
Initial hold (min)	1.
Final hold (min)		20.
I	1381.	1397.	1392.	1393.	1392.
Reference	Camciuc, Bessière, et al., 1998	Doneanu and Anitescu, 1998	El-Sakhawy, El-Tantawy, et al., 1998	Maia, Zohhbi, et al., 1998	Santos, Andrade, et al., 1998
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-1	OV-101	CP Sil 5 CB	CP Sil 5 CB	CP Sil 5 CB
Column length (m)	60.	25.	25.	25.	25.
Carrier gas	He		N2	N2	He
Substrate
Column diameter (mm)	0.25	0.32	0.32	0.32	0.25
Phase thickness (μm)	0.25		0.25	0.25	0.25
T_start (C)	50.	50.	50.	50.	60.
T_end (C)	280.	200.	290.	290.	300.
Heat rate (K/min)	4.	5.	4.	4.	6.
Initial hold (min)	5.
Final hold (min)
I	1407.	1391.	1379.	1379.	1379.
Reference	Stashenko, Cervantes, et al., 1998	Zollo, Biyiti, et al., 1998	Bos, Woerdenbag, et al., 1997	Bos, Woerdenbag, et al., 1997	Bos, Woerdenbag, et al., 1997, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	OV-1	SPB-Sulfur	DB-1	DB-5
Column length (m)	30.	30.	30.		30.
Carrier gas	He		He		He
Substrate
Column diameter (mm)	0.25	0.32	0.32		0.25
Phase thickness (μm)	0.25	0.25	4.
T_start (C)	65.	40.	45.	80.	60.
T_end (C)	300.	270.	240.	220.	240.
Heat rate (K/min)	4.	2.	5.	6.	4.
Initial hold (min)	2.	4.	13.
Final hold (min)			5.
I	1398.	1379.	1422.	1388.	1393.
Reference	Elias, Simoneit, et al., 1997	Kökdil, Tanker, et al., 1997	Mariaca, Berger, et al., 1997	Salgueiro, Vila, et al., 1997	Zunino, Novillo-Newton, et al., 1997
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CBP-1	HP-1	OV-101	DB-5	OV-101
Column length (m)	25.	23.	50.	30.	50.
Carrier gas	He	He	N2		He
Substrate
Column diameter (mm)	0.22	0.32	0.25	0.25	0.25
Phase thickness (μm)		0.17	0.17	0.25
T_start (C)	60.	60.	50.	60.	50.
T_end (C)	240.	250.	220.	300.	250.
Heat rate (K/min)	5.	5.	5.	4.	2.
Initial hold (min)		3.		2.
Final hold (min)		30.		5.
I	1394.	1385.	1402.	1391.0	1383.
Reference	Zygadlo, Ariza-Espinar, et al., 1997	Ayedoun, Adeoti, et al., 1996	Chacko, Jayalekshmy, et al., 1996	Gawdzik, Mardarowicz, et al., 1996	Orav, Kailas, et al., 1996
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	BP-1	DB-1	HP-1	SPB-1
Column length (m)	25.	25.	60.	25.	50.
Carrier gas	N2	N2	He	Helium	He
Substrate
Column diameter (mm)	0.50	0.50	0.32	0.32	0.2
Phase thickness (μm)			0.50	0.25	0.33
T_start (C)	60.	60.	50.	60.	40.
T_end (C)	220.	220.	250.	220.	200.
Heat rate (K/min)	5.	5.	8.	4.	3.
Initial hold (min)			1.	2.	3.
Final hold (min)			6.	20.	30.
I	1388.	1390.	1392.	1384.	1385.
Reference	Rajeswara, Kaul, et al., 1996	Rajeswara, Kaul, et al., 1996	Sagrero-Nieves and Bartley, 1996	Thanh, Dung, et al., 1996	Wong and Lai, 1996
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-1	DB-5	Methyl Silicone	Methyl Silicone
Column length (m)		60.	60.	50.	50.
Carrier gas			Helium	N2	N2
Substrate
Column diameter (mm)		0.32	0.32	0.25	0.25
Phase thickness (μm)		0.50		0.17	0.17
T_start (C)	35.	50.	60.	80.	80.
T_end (C)	200.	225.	220.	200.	200.
Heat rate (K/min)	6.	2.	3.	2.	3.
Initial hold (min)	2.
Final hold (min)
I	1416.	1394.	1400.	1400.	1403.
Reference	Larsen and Frisvad, 1995	Sagrero-Nieves, Bartley, et al., 1994	Everaerts, Roisin, et al., 1993	Gopalakrishnan, Menon, et al., 1993	Gopalakrishnan, Menon, et al., 1993
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 8 CB	OV-101	OV-101	DB-1	OV-101
Column length (m)	25.	50.	50.	60.	50.
Carrier gas		N2	N2		N2
Substrate
Column diameter (mm)	0.20	0.25	0.25	0.32	0.25
Phase thickness (μm)
T_start (C)	60.	80.	80.	50.	80.
T_end (C)	230.	200.	200.	250.	200.
Heat rate (K/min)	3.	2.	2.	4.	2.
Initial hold (min)	10.			0.1
Final hold (min)				5.
I	1396.	1388.	1390.	1386.	1385.
Reference	Jantan and Goh, 1990	Yang and Sugisawa, 1990	Yang and Sugisawa, 1990	Binder and Flath, 1989	Sugisawa, Yang, et al., 1989
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	OV-1	OV-101	OV-101	OV-1
Column length (m)	50.	50.	45.	50.	40.
Carrier gas	N2	He	He		He
Substrate
Column diameter (mm)	0.25	0.20	0.25	0.30	0.5
Phase thickness (μm)		0.20			0.75
T_start (C)	80.	30.	100.	40.	30.
T_end (C)	200.	220.	180.	230.	220.
Heat rate (K/min)	2.	2.	3.	3.5	3.
Initial hold (min)				5.
Final hold (min)
I	1388.	1385.	1411.	1386.	1384.
Reference	Sugisawa, Yang, et al., 1989	de Pooter, Nicolai, et al., 1988	Wu, Zhao, et al., 1987	Nykanen, 1986	de Pooter, de Buyck, et al., 1986
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary
Active phase	OV-101
Column length (m)	30.
Carrier gas	He
Substrate
Column diameter (mm)	0.5
Phase thickness (μm)	0.8
T_start (C)	40.
T_end (C)	220.
Heat rate (K/min)	2.
Initial hold (min)
Final hold (min)
I	1383.
Reference	De Pooter and Schamp, 1986
Comment	MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

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Xu, Han, et al., 2009
Xu, L.-L.; Han, T.; Wu, J.-Z.; Zhang, Q.-Y.; Zhang, H.; Huang, B.-K.; Rahman, K., Comparative research of chemical constituents, antifungal and antitumor properties of ether extracts of Panax ginseng and its endophytic fungus, Phytomedicine: Int. J. Phytotherapy Phytopharmacology, 2009, 16, 6-7, 609-616, https://doi.org/10.1016/j.phymed.2009.03.014 . [all data]

Zhao, Zeng, et al., 2009
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Jelén, H.H., Volatile sesquiterpene hydrocarbons characteristic for Penicillium roqueforti strains producing PR toxin, J. Agric. Food Chem., 2002, 50, 22, 6569-6574, https://doi.org/10.1021/jf020311o . [all data]

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Priestap, H.A.; van Baren, C.M.; Lira, P.D.L.; Prado, H.J.; Neugebauer, M.; Mayer, R.; Bandoni, A.L., Essential oils from aerial parts of Aristolochia gibertii Hook., Flavour Fragr. J., 2002, 17, 1, 69-71, https://doi.org/10.1002/ffj.1044 . [all data]

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Ly, T.N.; Yamauchi, R.; KAto, K., Volatile components of the essential oils in Galanga (Alpina officinarum Hance) from Vietnam, Food Sci. Technol. Res., 2001, 7, 4, 303-306, https://doi.org/10.3136/fstr.7.303 . [all data]

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Asekun and Ekundayo, 2000
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Bailac, Dellacasa, et al., 2000
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Baser, Özek, et al., 2000
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Khalilov L.M., Khalilova A.Z., et al., 1999
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Tellez, Canel, et al., 1999
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Camciuc, Bessière, et al., 1998
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Maia, Zohhbi, et al., 1998
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Bos, Woerdenbag, et al., 1997, 2
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Elias, Simoneit, et al., 1997
Elias, V.O.; Simoneit, B.R.T.; Cardoso, J.N., Analysis of volatile sesquiterpenoids in environmental and geological samples, J. Hi. Res. Chromatogr., 1997, 20, 6, 305-309, https://doi.org/10.1002/jhrc.1240200602 . [all data]

Kökdil, Tanker, et al., 1997
Kökdil, G.; Tanker, M.; Kurucu, S.; Topcu, G., Essential oil analysis of Nepeta cilicia Boiss., Flavour Fragr. J., 1997, 12, 2, 99-101, https://doi.org/10.1002/(SICI)1099-1026(199703)12:2<99::AID-FFJ619>3.0.CO;2-# . [all data]

Mariaca, Berger, et al., 1997
Mariaca, R.G.; Berger, T.F.H.; Gauch, R.; Imhof, M.I.; Jeangros, B.; Bosset, J.O., Occurrence of volatile mono- and sesquiterpenoids in highland and lowland plant species as possible precursors for flavor compounds in milk and dairy products, J. Agric. Food Chem., 1997, 45, 11, 4423-4434, https://doi.org/10.1021/jf970216t . [all data]

Salgueiro, Vila, et al., 1997
Salgueiro, L.R.; Vila, R.; Tomi, F.; Figueiredo, A.C.; Barroso, J.G.; Cañigueral, S.; Casanova, J.; da Cunha, A.P.; Adzet, T., Variability of essential oils of Thymus caespititius from Portugal, Phytochemistry, 1997, 45, 2, 307-311, https://doi.org/10.1016/S0031-9422(96)00872-2 . [all data]

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Zygadlo, J.A.; Ariza-Espinar, L.; Velasco-Negueruela, A.; Perez-Alonso, M.J., Volatile constituents of Stevia achalensis hieronymus, Flavour Fragr. J., 1997, 12, 4, 297-299, https://doi.org/10.1002/(SICI)1099-1026(199707)12:4<297::AID-FFJ625>3.0.CO;2-2 . [all data]

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Chacko, Jayalekshmy, et al., 1996
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Gawdzik, Mardarowicz, et al., 1996
Gawdzik, J.; Mardarowicz, M.; Suprynowicz, Z.; Kawka, S.; Wolski, T., Supercritical fluid extraction of essential oils from the fruits of Archangelica off. Hoffm. and their characterization by GC/MS, J. Hi. Res. Chromatogr., 1996, 19, 4, 237-240, https://doi.org/10.1002/jhrc.1240190416 . [all data]

Orav, Kailas, et al., 1996
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Binder and Flath, 1989
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Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References

Symbols used in this document:

T_end Final temperature

T_start Initial temperature
Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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