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Bicyclo[3.1.1]hept-2-ene-2-methanol, 6,6-dimethyl-


Van Den Dool and Kratz RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSCP-Sil PONA GBHP-5DB-5HP-5MS
Column length (m) 30.100.25.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.140.60.60.60.
Tend (C) 250.230.240.240.280.
Heat rate (K/min) 2.5.4.3.3.
Initial hold (min) 8.10.2.  
Final hold (min) 30.25.   
I 1198.1191.1204.1193.1196.
ReferenceBenkaci-Ali, Baaliouamer, et al., 2007Cunicao, Lopes, et al., 2007Dehghan, Solaimanian, et al., 2007Flamini, Cioni, et al., 2007Kundakovic, Fokialakis, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1Equity-5DB-5HP-5MSZB-5
Column length (m) 50.60.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.250.250.250.25
Phase thickness (mum) 0.251.0.250.250.25
Tstart (C) 60.40.60.60.50.
Tend (C) 220.260.260.280.250.
Heat rate (K/min) 2.5.5.4.3.
Initial hold (min)  1. 5. 
Final hold (min) 20.15.   
I 1174.1237.1202.1192.1195.
ReferenceLesueur, de Rocca Serra, et al., 2007Rocha, Coelho, et al., 2007Sabulal, Dan, et al., 2007Saroglou, Marin, et al., 2007Simoniatto, Bonani, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5BP-1BP-15 % Phenyl methyl siloxane
Column length (m) 30.30.50.50.25.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.220.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 80.60.60.60.60.
Tend (C) 300.240.220.220.280.
Heat rate (K/min) 4.3.2.2.3.
Initial hold (min)      
Final hold (min)   20.20.20.
I 1202.91193.1176.1177.1196.
ReferenceZeng, Zhao, et al., 2007Block, Flamini, et al., 2006Boti, Bighelli, et al., 2006Bousmaha, Boti, et al., 2006Djarri, Medjroubi, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5BP-1SPB-1
Column length (m) 30.30.50.50.30.
Carrier gas N2N2N2HeHe
Substrate      
Column diameter (mm) 0.320.250.20.220.2
Phase thickness (mum) 0.250.250.320.250.2
Tstart (C) 60.60.60.60.70.
Tend (C) 240.240.220.220.220.
Heat rate (K/min) 3.3.5.2.3.
Initial hold (min) 3.3.3.  
Final hold (min) 5.3.5.20.15.
I 1196.1194.1194.1180.1176.
ReferenceDob, Dahmane, et al., 2006Dob, Dahmane, et al., 2006, 2Esmaeili, Nematollahi, et al., 2006Gonny, Cavaleiro, et al., 2006Salgueiro L.R., Pinto E., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSDB-5HP-5RTX-1
Column length (m) 30.30.30.30.60.
Carrier gas HeH2H2N2 
Substrate      
Column diameter (mm) 0.250.250.250.250.22
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.50.35.60.60.
Tend (C) 280.285.270.220.220.
Heat rate (K/min) 4.4.35.5.2.
Initial hold (min) 5.  10. 
Final hold (min)   20. 20.
I 1196.1194.1194.1195.1181.
ReferenceSaroglou, Dorizas, et al., 2006Vujisic L., Vuckovic I., et al., 2006Alves, Pinto, et al., 2005Cioni, Flamini, et al., 2005Cozzani, Muselli, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1HP-5MSHP-5MSHP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas N2 HeHeHe
Substrate      
Column diameter (mm) 0.320.320.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.50.80.80.80.
Tend (C) 260.250.290.290.290.
Heat rate (K/min) 2.2.2.4.6.
Initial hold (min) 3.8.   
Final hold (min) 5.    
I 1168.1178.1199.41201.31202.1
ReferenceDob T., Berramdane T., et al., 2005Dob, Dahmane, et al., 2005Zhao, Liang, et al., 2005Zhao, Liang, et al., 2005Zhao, Liang, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-54SPB-1SPB-1HP-5BP-1
Column length (m) 30.30.30.30.50.
Carrier gas HeHeHe  
Substrate      
Column diameter (mm) 0.250.250.20.250.22
Phase thickness (mum) 0.250.250.20.250.25
Tstart (C) 60.70.70.60.60.
Tend (C) 260.220.220.220.220.
Heat rate (K/min) 2.3.3.5.2.
Initial hold (min) 5.  10. 
Final hold (min)  15.15. 20.
I 1191.1176.1177.1195.1179.
ReferenceAlma, Nitz, et al., 2004Antunes, Sevinate-Pinto, et al., 2004Cavaleiro, Salgueiro, et al., 2004Ceccarini, Macchia, et al., 2004Gonny, Bradesi, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5DB-5HP-5MSDB-1
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.25 0.250.250.25
Tstart (C) 60.60.60.60.50.
Tend (C) 280.260.260.280.265.
Heat rate (K/min) 4.3.3.4.2.5
Initial hold (min) 5.  5. 
Final hold (min)      
I 1194.1193.1194.1203.1173.
ReferenceGrujic-Jovanovic, Skaltsa, et al., 2004Javidnia, Miri, et al., 2004Javidnia, Miri, et al., 2004, 2Karioti, Hadjipavlou-Litina, et al., 2004Ramezani, Behravan, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-5OV-1SPB-1
Column length (m) 30.50.25.25.30.
Carrier gas HeHeN2H2He
Substrate      
Column diameter (mm) 0.250.20.250.250.2
Phase thickness (mum) 0.250.20.250.30.2
Tstart (C) 60.40.75.50.70.
Tend (C) 275.250.210.200.220.
Heat rate (K/min) 4.3.3.3.3.
Initial hold (min)  15.10.1. 
Final hold (min)  40.1.20.15.
I 1195.1194.1198.1173.1176.
ReferenceRamezani, Khaje-Karamoddin, et al., 2004Stashenko, Jaramillo, et al., 2004bin Ahmad and bin Jantan, 2003Bicchi, Rubiolo, et al., 2003Cavaleiro, Salgueiro, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1DB-5HP-5MSHP-5MSHP-5
Column length (m) 60.25.60.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.250.250.250.25
Phase thickness (mum) 0.25 0.250.250.25
Tstart (C) 60.60.40.50.60.
Tend (C) 230.260.310.250.280.
Heat rate (K/min) 2.4.3.3.4.
Initial hold (min)   1. 5.
Final hold (min) 45. 20.  
I 1179.1197.1202.1194.1194.
ReferenceCavalli, Tomi, et al., 2003Javidnia, Miri, et al., 2003Lalel, Singh, et al., 2003Salido, Altarejos, et al., 2003Skaltsa, Demetzos, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5SE-52DB-5
Column length (m) 30.30.30.25.30.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (mum) 0.250.250.250.150.25
Tstart (C) 60.60.60.45.60.
Tend (C) 280.280.280.200.260.
Heat rate (K/min) 3.3.3.3.4.
Initial hold (min)    5. 
Final hold (min)    20. 
I 1196.1196.1196.1160.1194.
ReferenceTsiri, Kretsi, et al., 2003Tsiri, Kretsi, et al., 2003Tzakou, Couladis, et al., 2003Duru, Cakir, et al., 2002Javidnia, Miri, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5CP Sil 5 CBDB-1RTX-5RTX-5
Column length (m) 30.25.50.30.30.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.220.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 45.60.60.45.45.
Tend (C) 300.280.220.250.250.
Heat rate (K/min) 3.4.2.3.3.
Initial hold (min) 6.6. 6.6.
Final hold (min) 10. 20.  
I 1199.1182.1181.1194.1204.
ReferenceMondello, Zappia, et al., 2002Pino, Marbot, et al., 2002Pintore, Usai, et al., 2002Shellie, Mondello, et al., 2002Shellie, Mondello, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5MSHP-101HP-101
Column length (m) 30.30.30.25.25.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.20.2
Phase thickness (mum) 0.250.250.250.20.2
Tstart (C) 60.60.60.70.70.
Tend (C) 280.380.280.200.200.
Heat rate (K/min) 3.3.4.3.3.
Initial hold (min) 5. 5.2.2.
Final hold (min)    10.10.
I 1196.1194.1194.1196.1195.
ReferenceAligiannis, Kalpoutzakis, et al., 2001Couladis, Tsortanidou, et al., 2001Skaltsa, Mavrommati, et al., 2001Milos and Radonic, 2000Milos and Radonic, 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBBP-1DB-1CP Sil 5 CBOV-1
Column length (m) 50.50.30.25.25.
Carrier gas H2He He 
Substrate      
Column diameter (mm) 0.220.220.250.250.25
Phase thickness (mum) 0.130.250.25 0.3
Tstart (C) 40.60.50.60.50.
Tend (C) 300.220.220.260.200.
Heat rate (K/min) 4.2.3.5.3.
Initial hold (min)   3. 1.
Final hold (min) 10.20.  20.
I 1182.1177.1190.1183.1174.
ReferencePfeifhofer, 2000Mazzoni, Tomi, et al., 1999Muselli, Hoi, et al., 1999Weyerstahl, Marschall, et al., 1999Bicchi, Rubiolo, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1DB-5DB-1DB-1DB-1
Column length (m) 50.30.30.30.60.
Carrier gas HeHeN2N2He
Substrate      
Column diameter (mm) 0.220.260.320.320.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.50.150.150.40.
Tend (C) 230.225.280.280.280.
Heat rate (K/min) 2.2.3.3.2.
Initial hold (min)     3.
Final hold (min) 35.20.  10.
I 1179.1192.1183.1185.1194.
ReferenceMariotti, Tomi, et al., 1997Sagrero-Nieves, Bartley, et al., 1997Coen, Engel, et al., 1995Coen, Engel, et al., 1995Adedeji, Hartman, et al., 1992
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Benkaci-Ali, Baaliouamer, et al., 2007
Benkaci-Ali, F.; Baaliouamer, A.; Meklati, B.Y.; Chemat, F., Chemical composition of seed essential oils from Algerian Nigella sativa extracted by microwave and hydrodistillation, Flavour Fragr. J., 2007, 22, 2, 148-153, https://doi.org/10.1002/ffj.1773 . [all data]

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Dehghan, Solaimanian, et al., 2007
Dehghan, G.; Solaimanian, R.; Shahverdi, A.R.; Amin, G.; Abdollahi, M.; Shafiee, A., Chemical composition and antimicrobial activity of essential oil of Ferula szovitsiana D.C., Flavour Fragr. J., 2007, 22, 3, 224-227, https://doi.org/10.1002/ffj.1789 . [all data]

Flamini, Cioni, et al., 2007
Flamini, G.; Cioni, P.L.; Morelli, I.; Bader, A., Essential oils of the aerial parts of three Salvia species from Jordan: Salvia lanigera, S. spinosa and S. syriaca, Food Chem., 2007, 100, 2, 732-735, https://doi.org/10.1016/j.foodchem.2005.10.032 . [all data]

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Kundakovic, T.; Fokialakis, N.; Kovacevic, N.; Chinou, I., Essential oil composition of Achillea lingulata and A. umbellata, Flavour Fragr. J., 2007, 22, 3, 184-187, https://doi.org/10.1002/ffj.1778 . [all data]

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Rocha, S.M.; Coelho, E.; Zrostlikova, J.; Delgadillo, I.; Coimbra b, M.A., Comprehensive two-dimensional gas chromatography with time-of-flight mass spectrometry of monoterpenoids as a powerful tool for grape origin traceability, J. Chromatogr. A, 2007, 1161, 1-2, 292-299, https://doi.org/10.1016/j.chroma.2007.05.093 . [all data]

Sabulal, Dan, et al., 2007
Sabulal, B.; Dan, M.; John, A.; Kurup, R.; Chandrika, S.P.; George, V., Phenylbutanoid-rich rhizome oil of Zingiber neesanum from Western Ghats, southern India, Flavour Fragr. J., 2007, 22, 6, 521-524, https://doi.org/10.1002/ffj.1834 . [all data]

Saroglou, Marin, et al., 2007
Saroglou, V.; Marin, P.D.; Rancic, A.; Veljic, M.; Skaltsa, H., Composition and antimicrobial activity of the essential oil of six Hypericum species from Serbia, Biochem. Syst. Ecol., 2007, 35, 3, 146-152, https://doi.org/10.1016/j.bse.2006.09.009 . [all data]

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Saroglou, Dorizas, et al., 2006
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Alves, R.J.V.; Pinto, A.C.; da Costa, A.V.M.; Rezende, C.M., Zizyphus mauritiana Lam. (Rhamnaceae) and the chemical composition of its floral fecal odor, J. Braz. Chem. Soc., 2005, 16, 3B, 654-656, https://doi.org/10.1590/S0103-50532005000400027 . [all data]

Cioni, Flamini, et al., 2005
Cioni, P.L.; Flamini, G.; Caponi, C.; Ceccarini, L.; Morelli, I., Analysis of volatile fraction, fixed oil and tegumental waxes of the seeds of two different cultivars of Helianthus annuus, Food Chem., 2005, 90, 4, 713-717, https://doi.org/10.1016/j.foodchem.2004.04.031 . [all data]

Cozzani, Muselli, et al., 2005
Cozzani, S.; Muselli, A.; Desjobert, J.-M.; Bernardini, A.-F.; Tomi, F.; Casanova, J., Chemical composition of essential oil of Teucrium polium subsp. capitatum (L.) from Corsica, Flavour Fragr. J., 2005, 20, 4, 436-441, https://doi.org/10.1002/ffj.1463 . [all data]

Dob T., Berramdane T., et al., 2005
Dob T.; Berramdane T.; Chelghoum C., Analysis of essential oil from the needles of Pinus pinaster growing in Algeria, Chem. Nat. Compd. (Engl. Transl.), 2005, 41, 5, 545-548, https://doi.org/10.1007/s10600-005-0202-z . [all data]

Dob, Dahmane, et al., 2005
Dob, T.; Dahmane, D.; Berramdane, T.; Chelghoum, C., Chemical composition of the essential oil of Artemisia campestris L. from Algeria, Pharm. Biol., 2005, 43, 6, 512-514, https://doi.org/10.1080/13880200500220664 . [all data]

Zhao, Liang, et al., 2005
Zhao, C.-X.; Liang, Y.-Z.; Fang, H.-Z.; Li, X.-N., Temperature-programmed retention indices for gas chromatography-mass spectroscopy analysis of plant essential oils, J. Chromatogr. A, 2005, 1096, 1-2, 76-85, https://doi.org/10.1016/j.chroma.2005.09.067 . [all data]

Alma, Nitz, et al., 2004
Alma, M.H.; Nitz, S.; Kollmannsberger, H.; Digrak, M.; Efe, F.T.; Yilmaz, N., Chemical composition and antimicrobial activity of the essential oils from the gum of Turkish Pistachio (Pistacia vera L.), J. Agric. Food Chem., 2004, 52, 12, 3911-3914, https://doi.org/10.1021/jf040014e . [all data]

Antunes, Sevinate-Pinto, et al., 2004
Antunes, T.; Sevinate-Pinto, I.; Barroso, J.G.; Cavaleiro, C.; Salgueiro, L.R., Micromorphology of trichomes and composition of essential oil of Teucrium capitatum, Flavour Fragr. J., 2004, 19, 4, 336-340, https://doi.org/10.1002/ffj.1310 . [all data]

Cavaleiro, Salgueiro, et al., 2004
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Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References