Globulol

Formula: C₁₅H₂₆O
Molecular weight: 222.3663
IUPAC Standard InChI: InChI=1S/C15H26O/c1-9-5-6-10-12(9)13-11(14(13,2)3)7-8-15(10,4)16/h9-13,16H,5-8H2,1-4H3/t9?,10-,11-,12-,13-,15-/m0/s1
IUPAC Standard InChIKey: AYXPYQRXGNDJFU-UFMLLKMHSA-N
CAS Registry Number: 51371-47-2
Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript.
Species with the same structure:
- (-)-Globulol
Stereoisomers:
Other names: 1,1,4,7-Tetramethyldecahydro-1H-cyclopropa[e]azulen-4-ol, (1aα,4α,4aα,7α,7aβ,7bα)-; (.+/-.)-Globulol; Glubulol
Information on this page:
Other data available:
- Mass spectrum (electron ionization)
- Gas Chromatography
Options:
- Switch to calorie-based units

Normal alkane RI, non-polar column, temperature ramp

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5 MS	HP-5 MS	HP-5	HP-5 MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium		Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	60.	60.	50.
T_end (C)	240.	180.	300.	240.	180.
Heat rate (K/min)	3.	2.	15.	3.	2.
Initial hold (min)			2.
Final hold (min)			10.
I	1585.	1590.	1591.	1585.	1581.
Reference	Rodriques, Amorim, et al., 2013	Phungpanya, Thongpoon, et al., 2012	Xu, Han, et al., 2012	Bertoli, Lepnardi, et al., 2011	Hammami, Kamoun, et al., 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-1	HP-5	DB-5	DB-5
Column length (m)	30.	25.	30.	30.	30.
Carrier gas	Helium	Nitrogen	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.252	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	35.	50.
T_end (C)	240.	250.	240.	220.	250.
Heat rate (K/min)	3.	4.	3.	3.	5.
Initial hold (min)		1.	5.		2.
Final hold (min)		10.		40.
I	1588.	1593.	1603.	1569.	1585.
Reference	Cavar, Maksimovic, et al., 2010	Mirjalili, Salehi, et al., 2010	Monsef-Esfahani, Miri, et al., 2010	El-Massry, El-Ghorab, et al., 2009	Ho, Wang, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	5 % Phenyl methyl siloxane	HP-5 MS	HP-5	DB-5
Column length (m)	30.	60.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	70.	90.	60.	50.	100.
T_end (C)	240.	225.	300.	280.	300.
Heat rate (K/min)	5.	3.	15.	9.	20.
Initial hold (min)			2.	3.	2.
Final hold (min)		3.	10.	3.	10.
I	1623.	1591.	1591.	1585.	1585.
Reference	Lawal and Oyedelji, 2009	Retta, Gattuso, et al., 2009	Xu, Han, et al., 2009	Aicha, Ines, et al., 2008	Khokra, Prakash, et al., 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	VF-5MS	HP-5	DB-5 MS	HP-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.26
Phase thickness (μm)	0.25	0.25	0.25	0.32	0.25
T_start (C)	240.	100.	50.	60.	60.
T_end (C)	320.	240.	300.	250.	240.
Heat rate (K/min)	20.	5.	5.	5.	3.
Initial hold (min)	1.	2.	5.	30.
Final hold (min)		5.	5.
I	1595.	1583.	1580.	1580.	1583.
Reference	Kowalski, 2008	Lago, Romoff, et al., 2008	Noudogbessi, Yedomonhan, et al., 2008	Yassa and Akhani, 2008	Bos, Woerdenbag, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	ZB-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	He	He		Helium
Substrate
Column diameter (mm)	0.26	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	35.	60.	60.	60.
T_end (C)	290.	220.	300.	220.	300.
Heat rate (K/min)	3.	3.	3.	4.	3.
Initial hold (min)				5.
Final hold (min)		40.		20.
I	1583.	1579.	1579.	1583.	1557.
Reference	Elfami, Bos, et al., 2007	El-Ghorab A., El-Massry K.F., et al., 2007	Limberger, Scopel, et al., 2007	Mohottalage, Tabacchi, et al., 2007	Moreno, Lima, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-1	DB-5	DB-5	HP-5 MS	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He		Helium	He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.2	0.25	0.25	0.25	0.25
T_start (C)	70.	60.	40.	60.	40.
T_end (C)	220.	320.	250.	280.	260.
Heat rate (K/min)	3.	10.	2.	3.	4.
Initial hold (min)
Final hold (min)	15.	4.	33.
I	1563.	1599.	1579.	1584.	1588.0
Reference	Pinto, Salgueiro, et al., 2007	Smelcerovic, Spiteller, et al., 2007	Sylvestre, Pichette, et al., 2007	Tsokou, Georgopoulos, et al., 2007	Zizovic, Stamenic, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	AT-5	DB-1	DB-5
Column length (m)	30.	30.	60.	60.	30.
Carrier gas	He		He	Nitrogen	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.26
Phase thickness (μm)	0.25	0.25	0.25		0.25
T_start (C)	60.	60.	60.	40.	60.
T_end (C)	300.	300.	200.	200.	290.
Heat rate (K/min)	3.	3.	4.	2.	3.
Initial hold (min)				1.
Final hold (min)			20.	9.
I	1575.	1581.	1580.	1576.	1583.
Reference	Apel, Sobral, et al., 2006	Apel, Sobral, et al., 2006, 2	Borges, Rojas, et al., 2006	Chen, Sheu, et al., 2006	Elfami, Komar, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	CP Sil 5 CB	DB-5MS	5 % Phenyl methyl siloxane	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	N2	He	Helium	He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	50.	60.	60.	60.
T_end (C)	300.	300.	280.	280.	220.
Heat rate (K/min)	5.	4.	3.	3.	4.
Initial hold (min)	5.
Final hold (min)	5.		30.	30.
I	1587.	1588.	1552.	1552.	1588.
Reference	Figuérédo, Cabassu, et al., 2006	Lis and Milczarek, 2006	Maronigiu, Piras, et al., 2006	Marongiu, Piras, et al., 2006	Morteza-Semnani, Akbarzadeh, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	HP-5	DB-5	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	Hydrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	60.	70.	50.
T_end (C)	220.	250.	220.	280.	250.
Heat rate (K/min)	4.	4.	5.	4.	10.
Initial hold (min)	5.		10.	4.	5.
Final hold (min)
I	1589.	1592.	1579.	1582.	1598.
Reference	Morteza-Semnani K., Akbarzadeh M., et al., 2006	Najafpour Navaei, Mirza, et al., 2006	Pintore G., Chessa M., et al., 2006	Pino, Marbot, et al., 2006	Robinson, 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	HP-5	SPB-1
Column length (m)	30.	30.	30.	25.	50.
Carrier gas	He	He	N2	H2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.52	0.33
T_start (C)	60.	60.	60.	50.	50.
T_end (C)	200.	260.	240.	280.	220.
Heat rate (K/min)	2.	5.	4.	2.5	4.
Initial hold (min)				5.	1.
Final hold (min)	60.				10.
I	1582.	1610.	1584.	1586.	1568.
Reference	Rout, Naik, et al., 2006	Sabulal, Dan, et al., 2006	Trilles, Bombarda, et al., 2006	Wang, Kong, et al., 2006	Wong, Lim, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-30	DB-5	DB-5	DB-5	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)		0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	90.	60.	60.	60.	60.
T_end (C)	220.	240.	240.	300.	30.
Heat rate (K/min)	7.	3.	3.	3.	4.
Initial hold (min)	2.			3.	3.
Final hold (min)					15.
I	1583.	1584.	1587.	1581.	1584.
Reference	Ahuja, Bakshi, et al., 2005	Chaverri and Cicció, 2005	Chaverri and Cicció, 2005	Ferraz, Limberger, et al., 2005	Ferretti, Maggi, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-1	DB-5	DB-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	Helium	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	50.	50.	60.	35.	60.
T_end (C)	300.	265.	240.	280.	230.
Heat rate (K/min)	5.	2.5	3.	4.	3.
Initial hold (min)	5.	1.		2.
Final hold (min)	5.	20.
I	1587.	1570.	1578.	1611.	1575.
Reference	Figuérédo, Cabassu, et al., 2005	Khanavi, Ghasemian, et al., 2005	Khayyat and Karimi, 2005	Kowalski, 2005	Limberger, Sobral, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	DB-1	HP-5MS	DB-5	DB-5
Column length (m)	25.	50.	30.	30.	30.
Carrier gas		N2		He	He
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.25	0.25
Phase thickness (μm)	0.15	0.25			0.25
T_start (C)	50.	95.	60.	40.	40.
T_end (C)	230.	240.	280.	240.	260.
Heat rate (K/min)	3.	4.	3.	4.	2.
Initial hold (min)					5.
Final hold (min)					20.
I	1586.	1583.	1585.	1582.	1584.
Reference	Ogunwande, Olawore, et al., 2005	Pala-Paul, Perez-Alonso, et al., 2005	Petrakis, Roussis, et al., 2005	Sefidkon and Jamzad, 2005	Senatore, Apostolides Arnold, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	HP-5MS	CP Sil 8 CB
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	300.	300.	300.	280.	290.
Heat rate (K/min)	3.	3.	3.	3.	3.
Initial hold (min)					5.
Final hold (min)
I	1578.	1579.	1580.	1591.	1579.
Reference	Simoes-Pires C.A., Debenedetti S., et al., 2005	Simoes-Pires C.A., Debenedetti S., et al., 2005	Simoes-Pires C.A., Debenedetti S., et al., 2005	Slavkovska, Couladis, et al., 2005	Suárez, Vásquez, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	DB-1	DB-5	DB-5	DB-5
Column length (m)	30.	30.	25.	60.	30.
Carrier gas	N2	N2	Nitrogen	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	50.	60.	40.	60.
T_end (C)	200.	200.	240.	280.	300.
Heat rate (K/min)	5.	5.	3.	4.	3.
Initial hold (min)				4.
Final hold (min)
I	1599.	1582.	1583.	1583.	1571.
Reference	Agnaniet, Menut, et al., 2004	Fekam Boyom, Fotio, et al., 2004	JAvidnia, Mojab, et al., 2004	Kalvandi, Sefidkon, et al., 2004	Lago, de Ávila, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5MS	DB-5	RTX-1	DB-5	DB-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	N2		He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	40.	60.
T_end (C)	240.	300.	300.	210.	280.
Heat rate (K/min)	3.	3.	4.	2.	3.
Initial hold (min)				2.
Final hold (min)				33.	30.
I	1584.	1577.	1590.	1586.	1557.
Reference	paz Lima, Silva, et al., 2004	Limberger, Sobral, et al., 2004	Lis, Boczek, et al., 2004	Lopez Arze, Collin, et al., 2004	Marongiu, Porcedda, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	HP-1	DB-5	DB-5
Column length (m)	60.	30.	30.	30.	30.
Carrier gas	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.33	0.25	0.25
T_start (C)	50.	50.	40.	40.	60.
T_end (C)	270.	265.	260.	250.	300.
Heat rate (K/min)	4.	2.5	2.	2.	3.
Initial hold (min)		1.	5.	5.
Final hold (min)		20.	20.	20.
I	1591.	1572.	1588.	1586.	1574.
Reference	Nik, Mirza, et al., 2004	Sarkhail, Amin, et al., 2004	Senatore, Napolitano, et al., 2004	Senatore, Rigano, et al., 2004	Suyenaga, Apel, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-1	Methyl Silicone	RSL-200	RSL-200
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	N2	He	H2	H2
Substrate
Column diameter (mm)	0.32	0.25	0.32	0.32	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	100.	50.	60.	40.	40.
T_end (C)	240.	200.	250.	280.	280.
Heat rate (K/min)	5.	5.	2.	6.	6.
Initial hold (min)	2.		2.	5.	5.
Final hold (min)	5.		5.	5.	5.
I	1592.	1574.	1568.	1570.	1588.
Reference	Chaves, Lago, et al., 2003	Fekam Boyom, Ngouana, et al., 2003	Jayaprakasha, Rao, et al., 2003	Jirovetz, Buchbauer, et al., 2003	Jirovetz, Buchbauer, et al., 2003, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	DB-5	DB-5	DB-5	DB-5
Column length (m)	25.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	35.	60.	60.	60.	60.
T_end (C)	280.	280.	250.	280.	280.
Heat rate (K/min)	5.	5.	3.	3.	3.
Initial hold (min)	2.5
Final hold (min)				30.	30.
I	1566.	1575.	1585.	1569.	1568.
Reference	Kanjilal, Kotoky, et al., 2003	Lago, de Ávila, et al., 2003	Limberger, Simões-Pires, et al., 2003	Marongiu, Porcedda, et al., 2003	Marongiu, Porcedda, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-1	DB-1	DB-5
Column length (m)	30.	30.	60.	60.	30.
Carrier gas	H2	H2	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	40.	60.
T_end (C)	280.	280.	250.	260.	240.
Heat rate (K/min)	4.	4.	4.	4.	3.
Initial hold (min)	10.	10.		5.
Final hold (min)	40.	40.
I	1583.	1583.	1590.	1576.	1585.
Reference	Pino, Marbot, et al., 2003	Pino, Marbot, et al., 2003	Pourmortazavi, Sefidkon, et al., 2003	Sefidkon, Naderi Nik, et al., 2003	da Silva, Luz, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	PTE-5	SE-30	CP Sil 8 CB
Column length (m)	30.	30.	60.	50.	30.
Carrier gas	N2	N2	H2	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.30	0.25	0.25
T_start (C)	50.	50.	60.	70.	50.
T_end (C)	250.	250.	285.	240.	220.
Heat rate (K/min)	4.	4.	4.3	4.	3.
Initial hold (min)		5.			2.
Final hold (min)
I	1583.	1582.	1583.	1577.	1579.
Reference	Farah, Fechtal, et al., 2002	Farah, Fechtal. M., et al., 2002	Gudzic, Djokovic, et al., 2002	Iñigo, Palá-Paúl, et al., 2002	Juteau, Masotti, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	HP-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas		He	He		He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	35.	100.	60.
T_end (C)	210.	240.	280.	240.	250.
Heat rate (K/min)	2.	3.	4.	5.	3.
Initial hold (min)	2.		2.	2.
Final hold (min)	33.		15.	5.
I	1581.	1582.	1596.	1585.	1572.
Reference	Kabouss, Charrouf, et al., 2002	Kobaisy, Tellez, et al., 2002	Krauze-Baranowska, Mardarowicz, et al., 2002	Lago, Reis, et al., 2002	Limberger, Simões-Pires, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5MS	DB-5	DB-1	DB-1
Column length (m)	30.	30.	30.	50.	60.
Carrier gas	He	He	He	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	80.	40.
T_end (C)	240.	240.	220.	225.	250.
Heat rate (K/min)	3.	3.	4.	4.	4.
Initial hold (min)			5.
Final hold (min)
I	1585.	1588.	1585.	1567.	1587.
Reference	Maia, da Silva, et al., 2002	Maia, Zoghbi, et al., 2002	Morteza-Semnani, Saeedi, et al., 2002	Palá-Paúl, Pérez-Alonso, et al., 2002	Sefidkon, Dabiri, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	DB-5MS	DB-1	DB-1
Column length (m)	60.	60.	30.	60.	60.
Carrier gas	He	He	He	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.248	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	40.	60.	60.	40.
T_end (C)	280.	280.	270.	220.	280.
Heat rate (K/min)	4.	4.	3.	3.	4.
Initial hold (min)	5.	5.		5.	5.
Final hold (min)				22.
I	1572.	1572.	1585.	1589.	1593.
Reference	Sefidkon, Jalili, et al., 2002	Sefidkon, 2002	Zoghbi, Andrade, et al., 2002	Bailac, Dellacasa, et al., 2001	Dabiri and Sefidkon, 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5	Optima-5	RSL-200	RTX-1
Column length (m)	60.	30.	30.	30.	30.
Carrier gas	He	N2	He	H2	N2
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.32	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	40.	60.	50.	40.	60.
T_end (C)	280.	220.	250.	280.	300.
Heat rate (K/min)	4.	5.	3.	6.	4.
Initial hold (min)	5.	10.	3.	5.
Final hold (min)				5.
I	1595.	1584.	1593.	1571.	1582.
Reference	Dabiri and Sefidkon, 2001	Gallori, Flamini, et al., 2001	Jacquemond-Collet, Bessière, et al., 2001	Jirovetz L., Buchbauer G., et al., 2001	Kalemba, Marschall, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5MS	DB-5	DB-1	SPB-1	DB-1
Column length (m)	30.	60.	30.	30.	25.
Carrier gas	He	He	He	He	Nitrogen
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.32	0.50
Phase thickness (μm)	0.25			0.25	0.25
T_start (C)	60.	50.	60.	50.	60.
T_end (C)	240.	250.	240.	250.	220.
Heat rate (K/min)	3.	3.	3.	2.	5.
Initial hold (min)		5.
Final hold (min)	30.
I	1568.	1583.	1588.5	1561.	1584.
Reference	Marongiu, Porcedda, et al., 2001	Rousis, Papadogianni, et al., 2001	Santos, Moreira, et al., 2001	Vijayanand, Rao, et al., 2001	Mallavarapu, Rao, et al., 2000
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-1	OV-101	CP Sil 5 CB	DB-5
Column length (m)	30.	60.	50.	25.	30.
Carrier gas	He	N2	N2	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.25	0.25
Phase thickness (μm)	0.25	0.25			0.25
T_start (C)	40.	75.	80.	50.	40.
T_end (C)	240.	220.	200.	230.	250.
Heat rate (K/min)	3.	4.	1.	3.	2.
Initial hold (min)	5.	1.			5.
Final hold (min)		8.	20.		60.
I	1587.	1594.	1583.	1566.	1556.
Reference	Novak, Novak, et al., 2000	Bailac, Dellacasa, et al., 1999	Menon, Chacko, et al., 1999	Oyedeji, Olawore, et al., 1999	Porta, Porcedda, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	OV-1	CBP-1	DB-5	DB-5
Column length (m)	30.	50.	30.	30.	30.
Carrier gas	He	He	He	He	Helium
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	60.	50.	60.	60.	60.
T_end (C)	240.	250.	240.	240.	240.
Heat rate (K/min)	3.	10.	4.	3.	3.
Initial hold (min)		5.
Final hold (min)		20.
I	1583.	1584.	1559.	1595.	1586.
Reference	Zoghbi, Andrade, et al., 1999	Kökdil, Kurucu, et al., 1998	Lamarque, Maestri, et al., 1998	Maia, Zohhbi, et al., 1998	Santos, Andrade, et al., 1998
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-1	CBP-1	OV-1	DB-1	BP-1
Column length (m)	60.	25.	50.	60.	50.
Carrier gas	He	He	N2		H2
Substrate
Column diameter (mm)	0.25	0.22	0.27	0.32	0.30
Phase thickness (μm)	0.25		0.2
T_start (C)	50.	60.	80.	50.	40.
T_end (C)	280.	240.	240.	250.	250.
Heat rate (K/min)	4.	5.	3.	4.	10.
Initial hold (min)	5.			0.1	1.
Final hold (min)				5.
I	1595.	1585.	1569.	1570.	1585.
Reference	Stashenko, Cervantes, et al., 1998	Zygadlo, Ariza-Espinar, et al., 1997	Ramanoelina, Viano, et al., 1994	Binder and Flath, 1989	Brophy, Davies, et al., 1989
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

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Bertoli, Lepnardi, et al., 2011
Bertoli, A.; Lepnardi, M.; Krzyzanowska, J.; Oleszek, W.; Pistelli, L., Mentha longifolia in vitro cultures as safe source of flavouring ingradients, Acta Biochem. Polonica, 2011, 58, 4, 581-587. [all data]

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Lawal and Oyedelji, 2009
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Retta, Gattuso, et al., 2009
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Xu, Han, et al., 2009
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Aicha, Ines, et al., 2008
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Khokra, Prakash, et al., 2008
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Apel, Sobral, et al., 2006, 2
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Borges, Rojas, et al., 2006
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Elfami, Komar, et al., 2006
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Lis and Milczarek, 2006
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Maronigiu, Piras, et al., 2006
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Marongiu, Piras, et al., 2006
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Morteza-Semnani, Akbarzadeh, et al., 2006
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Morteza-Semnani K., Akbarzadeh M., et al., 2006
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Najafpour Navaei, Mirza, et al., 2006
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Pintore G., Chessa M., et al., 2006
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Pino, Marbot, et al., 2006
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Robinson, 2006
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Rout, Naik, et al., 2006
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Sabulal, Dan, et al., 2006
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Trilles, Bombarda, et al., 2006
Trilles, B.L.; Bombarda, I.; Bouraïma-Madjebi, S.; Raharivelomanana, P.; Bianchini, J.-P.; Gaydou, E.M., Occurrence of various chemotypes in niaouli [Melaleuca quinquenervia (Cav.) S. T. Blake] essential oil from New Caledonia, Flavour Fragr. J., 2006, 21, 4, 677-682, https://doi.org/10.1002/ffj.1649 . [all data]

Wang, Kong, et al., 2006
Wang, P.; Kong, C.H.; Zhang, C.X., Chemical Composition and Antimicrobial Activity of the Essential Oil from Ambrosia trifida L., Molecules, 2006, 11, 7, 549-555, https://doi.org/10.3390/11070549 . [all data]

Wong, Lim, et al., 2006
Wong, K.C.; Lim, T.B.; Ali, D.M.H., Essential oil of Homalomena sagittifolia Jungh., Flavour Fragr. J., 2006, 21, 5, 786-788, https://doi.org/10.1002/ffj.1714 . [all data]

Ahuja, Bakshi, et al., 2005
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Chaverri and Cicció, 2005
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Porta, Porcedda, et al., 1999
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Maia, Zohhbi, et al., 1998
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Stashenko, Cervantes, et al., 1998
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Binder and Flath, 1989
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Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References

Symbols used in this document:

T_end Final temperature

T_start Initial temperature
Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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