Globulol


Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1CP-Sil PONA GBBP-1DB-5Methyl Silicone
Column length (m) 50.100.50.30.30.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.220.250.220.220.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.140.60.60.80.
Tend (C) 220.230.220.240.220.
Heat rate (K/min) 2.5.2.3.2.
Initial hold (min)  10. 2. 
Final hold (min) 20.25.20. 15.
I 1578.1610.1582.1582.1578.
ReferenceBoti, Koukoua, et al., 2007Cunicao, Lopes, et al., 2007Lesueur, de Rocca Serra, et al., 2007Martins, Santos, et al., 2007Melo, Corrêa, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1RTX-1HP-5DB-5HP-5MS
Column length (m) 60.60.30.25.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.220.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.50.60.60.
Tend (C) 230.230.250.200.280.
Heat rate (K/min) 2.2.4.2.4.
Initial hold (min)   4. 5.
Final hold (min) 35.35.10.60. 
I 1576.1583.1586.1588.1585.
ReferencePaolini J., Costa J., et al., 2007Paolini, Muselli, et al., 2007Quijano, Salamanca, et al., 2007Rout, Rao, et al., 2007Saroglou, Marin, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSDB-5DB-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeN2N2
Substrate      
Column diameter (mm) 0.220.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 55.60.50.60.60.
Tend (C) 240.280.250.240.220.
Heat rate (K/min) 3.3.3.3.5.
Initial hold (min) 2.  3.10.
Final hold (min) 15. 10.3. 
I 1583.1582.1582.1587.1586.
ReferenceSilva, Barbosa, et al., 2007Vagionas, Ngassapa, et al., 2007Yu, Liao, et al., 2007Dob, Dahmane, et al., 2006Flamini, Tebano, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5DB-5DB-5HP-5MS
Column length (m) 30.25.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.50.50.80.
Tend (C) 260.240.250.250.300.
Heat rate (K/min) 3.4.5.5.4.
Initial hold (min)   2.2. 
Final hold (min)      
I 1585.1583.1585.1585.1587.7
ReferenceJavidnia K., Miri R., et al., 2006Rezazadeh, Hamedani, et al., 2006Su, Ho, et al., 2006Su, Ho, et al., 2006, 2Zhao C.X., Li, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-1DB-1RTX-1SE-54
Column length (m) 25.30.25.60.25.
Carrier gas HeHe HeH2
Substrate      
Column diameter (mm) 0.250.250.250.220.25
Phase thickness (μm) 0.40.250.250.250.2
Tstart (C) 80.40.60.60.50.
Tend (C) 270.260.180.230.250.
Heat rate (K/min) 10.2.3.2.4.
Initial hold (min)  5.10.  
Final hold (min)  20.10.35. 
I 1589.1569.1586.1576.1582.
ReferenceZiegenbein, Hanssen, et al., 2006de Feo, Urrunaga Soria, et al., 2005bin Jantan, Yalvema, et al., 2005Paolini, Costa, et al., 2005Simionatto, Porto, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1BP-1SPB-1DB-5SPB-1
Column length (m) 30.50.30.30.30.
Carrier gas N2HeHeN2He
Substrate      
Column diameter (mm) 0.250.220.20.250.2
Phase thickness (μm) 0.250.250.20.250.2
Tstart (C) 50.60.70.60.70.
Tend (C) 200.230.220.240.220.
Heat rate (K/min) 5.2.3.3.3.
Initial hold (min)      
Final hold (min)  35.15. 15.
I 1578.1576.1561.1584.1562.
ReferenceTchoumbougnang, Zollo, et al., 2005Vellutini, Baldovini, et al., 2005Cavaleiro, Salgueiro, et al., 2004Flamini, Cioni, et al., 2004Moldão-Martins, Beirão-da-Costa, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1DB-1DB-5MSBPX-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas N2 HeN2N2
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.40.75.60.
Tend (C) 220.265.200.210.220.
Heat rate (K/min) 5.2.54.3.5.
Initial hold (min)   5.10.10.
Final hold (min) 13. 20.1. 
I 1578.1607.1588.1582.1585.
ReferenceRaina, Kumar, et al., 2004Ramezani, Behravan, et al., 2004Yu, Kim, et al., 2004bin Ahmad and bin Jantan, 2003Dural, Bagci, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5HP-5BPX-5RTX-5
Column length (m) 30.30.30.30.30.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.75.60.60.45.
Tend (C) 220.230.280.240.250.
Heat rate (K/min) 5.3.3.3.3.
Initial hold (min) 10.10. 2.6.
Final hold (min)  20.   
I 1584.1582.1583.1591.1593.
ReferenceErtugrul, Dural, et al., 2003Jantan, Ling, et al., 2003Ngassapa, Runyoro, et al., 2003Shellie, Marriott, et al., 2003Shellie, Marriott, et al., 2003, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5SPB-1HP-5MSHP-5DB-1
Column length (m) 30.30.30.30.25.
Carrier gas HeHe  N2
Substrate      
Column diameter (mm) 0.250.200.250.250.25
Phase thickness (μm) 0.250.200.250.25 
Tstart (C) 60.70.50.60.60.
Tend (C) 280.220.280.280.180.
Heat rate (K/min) 3.3.3.3.3.
Initial hold (min)   5.5.10.
Final hold (min)  15.  10.
I 1584.1561.1583.1580.1580.
ReferenceTzakou, Couladis, et al., 2003Cavaleiro, Salgueiro, et al., 2002Demetzos, Angelopoulou, et al., 2002Fokialakis, Magiatis, et al., 2002bin Jantan and bin Ahmad, 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30DB-5BP-1RTX-5CP Sil 5 CB
Column length (m) 25.30.50.30.25.
Carrier gas N2HeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.220.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.45.60.
Tend (C) 180.260.220.300.280.
Heat rate (K/min) 3.4.2.3.4.
Initial hold (min) 10.  6.6.
Final hold (min) 10. 20.10. 
I 1580.1583.1580.1577.1570.
Referencebin Jantan, Ayop, et al., 2002Javidnia, Miri, et al., 2002Lota, de Rocca Serra, et al., 2002Mondello, Zappia, et al., 2002Pino, Marbot, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBCP Sil 5 CBRTX-5RTX-5DB-5
Column length (m) 30.50.30.30.30.
Carrier gas H2HeHeHeH2
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.40.250.250.25
Tstart (C) 60.60.45.45.60.
Tend (C) 280.280.250.250.240.
Heat rate (K/min) 2.3.3.3.3.
Initial hold (min) 10.10.6.6. 
Final hold (min) 40.60.   
I 1570.1573.1583.1589.1586.
ReferencePino, Marbot, et al., 2002, 2Pino, Marbot, et al., 2002, 3Shellie, Mondello, et al., 2002Shellie, Mondello, et al., 2002Nogueira, Bittrich, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5DB-5OV-101HP-5
Column length (m) 30.30.30.25.30.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.25 0.25
Tstart (C) 60.60.60.50.50.
Tend (C) 280.240.240.200.280.
Heat rate (K/min) 4.3.3.5.4.
Initial hold (min) 5.2.2. 5.
Final hold (min)      
I 1585.1581.1581.1583.1583.
ReferenceSkaltsa, Mavrommati, et al., 2001Maia, de Paula, et al., 2000Maia, de Paula, et al., 2000Menut, Bessiere, et al., 2000Lazari, Skaltsa, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-1HP-1OV-1BP-1
Column length (m) 25.60.60.25.50.
Carrier gas N2HeHeH2He
Substrate      
Column diameter (mm) 0.250.250.250.250.22
Phase thickness (μm)  0.250.250.30.25
Tstart (C) 50.50.50.50.60.
Tend (C) 200.220.250.200.230.
Heat rate (K/min) 5.4.2.53.2.
Initial hold (min)   5.1. 
Final hold (min)    20.35.
I 1580.1594.1595.1550.1570.
ReferenceMenut, Bessiere, et al., 1999Mirza and Sefidkon, 1999Stashenko, Cervantes, et al., 1999Bicchi, Fresia, et al., 1997Mariotti, Tomi, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Flamini, Cioni, et al., 2004
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Raina, Kumar, et al., 2004
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Ramezani, Behravan, et al., 2004
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Yu, Kim, et al., 2004
Yu, E.J.; Kim, T.H.; Kim, K.H.; Lee, H.J., Characterization of aroma-active compounds of Abies nephrolepis (Khingan fir) needles using aroma extract dilution analysis, Flavour Fragr. J., 2004, 19, 1, 74-79, https://doi.org/10.1002/ffj.1314 . [all data]

bin Ahmad and bin Jantan, 2003
bin Ahmad, F.; bin Jantan, I., The essential oils of Boesenbergia stenophylla R. M. Sm. as natural sources of methyl (E)-cinnamate, Flavour Fragr. J., 2003, 18, 6, 485-486, https://doi.org/10.1002/ffj.1227 . [all data]

Dural, Bagci, et al., 2003
Dural, H.; Bagci, Y.; Ertugrul, K.; Demirelma, H.; Flamini, G.; Cioni, P.L.; Morelli, I., Essential oil composition of two endemic Centaurea species from Turkey, Centaurea mucronifera and Centaurea chrysantha, collected in the same habitat, Biochem. Syst. Ecol., 2003, 31, 12, 1417-1425, https://doi.org/10.1016/S0305-1978(03)00128-5 . [all data]

Ertugrul, Dural, et al., 2003
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Jantan, Ling, et al., 2003
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Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References