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Bicyclo[3.1.0]hexan-2-one, 5-(1-methylethyl)-


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5 MSDB-5DB-5HP-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.260.260.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 70.70.60.60.60.
Tend (C) 290.290.240.290.280.
Heat rate (K/min) 5.5.3.3.3.
Initial hold (min)      
Final hold (min)  10.   
I 1154.1160.1156.1156.1159.
ReferenceLazarevic, Radulovic, et al., 2010Radulovic, Dordevic, et al., 2010Bos, Woerdenbag, et al., 2007Elfami, Bos, et al., 2007Vagionas, Graikou, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-5HP-5DB-5
Column length (m) 30.30.30.25.30.
Carrier gas HeliumHeHeHeHe
Substrate      
Column diameter (mm) 0.260.250.2490.20.32
Phase thickness (mum) 0.250.250.250.330.25
Tstart (C) 60.50.60.60.40.
Tend (C) 290.300.290.240.250.
Heat rate (K/min) 3.5.3.3.5.
Initial hold (min)  5.  0.5
Final hold (min)  5. 7.2.
I 1156.1159.1156.1153.1156.
ReferenceElfami, Komar, et al., 2006Figuérédo, Cabassu, et al., 2006Bos, Stojanova, et al., 2005Duarte, Figueira, et al., 2005Özel, Gögüs, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1SE-54DB-1HP-5DB-5
Column length (m) 60.30.60.30.50.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.50.60.50.
Tend (C) 250.260.250.275.220.
Heat rate (K/min) 4.2.4.4.3.
Initial hold (min)  5.  2.
Final hold (min)      
I 1147.1153.1147.1154.1153.
ReferenceRasooli and Owlia, 2005Kilic, Hafizoglu, et al., 2004Rasooli and Razzaghi Abyaneh, 2004Ghannadi and Zolfaghari, 2003Masotti, Juteau, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5HP-5SPB-5
Column length (m) 50.30.30.50.
Carrier gas N2H2N2He
Substrate     
Column diameter (mm) 0.250.250.250.32
Phase thickness (mum) 0.250.250.250.25
Tstart (C) 95.60.60.60.
Tend (C) 240.280.220.240.
Heat rate (K/min) 4.4.5.3.
Initial hold (min)  10.10. 
Final hold (min)  40. 20.
I 1143.1158.1158.1187.
ReferencePerez-Alonso, Velasco-Negueruela, et al., 2003Pino, Marbot, et al., 2003Gallori, Flamini, et al., 2001Doneanu and Anitescu, 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Lazarevic, Radulovic, et al., 2010
Lazarevic, J.; Radulovic, N.; Palic, R.; Zlatkovic, B., Chemical Analusis of volatile constituents of Berula erecta (Hudson) Coville subsp. erecta (Apiaceae) from Serbia, J. Essential Oil. Res., 2010, 22, 3, 153-156, https://doi.org/10.1080/10412905.2010.9700290 . [all data]

Radulovic, Dordevic, et al., 2010
Radulovic, N.; Dordevic, N.; Markovic, M.; Palic, R., Volatile constituents of Glechoma Hirsuta Waldst. Kit. and G. Hederacea L. (Lamiaceae), Bull. Chem. Soc. Ethiop., 2010, 24, 1, 67-76, https://doi.org/10.4314/bcse.v24i1.52962 . [all data]

Bos, Woerdenbag, et al., 2007
Bos, R.; Woerdenbag, H.J.; Kayser, O.; Quax, W.J.; Ruslan, K.; Elfami, Essential oil constituents of Piper cubeba L. fils. from Indonesia, J. Essent. Oil Res., 2007, 19, 1, 14-17, https://doi.org/10.1080/10412905.2007.9699217 . [all data]

Elfami, Bos, et al., 2007
Elfami; Bos, R.; Ruslan, K.; Woerdenbag, H.J.; Kayser, P.; Quax, W.J., Essential Oil Constituents of Piper cubeba from Indonesia, 2007, 53-60. [all data]

Vagionas, Graikou, et al., 2007
Vagionas, K.; Graikou, K.; Ngassapa, O.; Runyoro, D.; Chinou, I., Composition and antimicrobial activity of the essential oils of three Satureja species growing in Tansania, Food Chem., 2007, 103, 2, 319-324, https://doi.org/10.1016/j.foodchem.2006.07.051 . [all data]

Elfami, Komar, et al., 2006
Elfami, R.B.; Komar, R.; Woerdenbag, H.J.; Kayser, P.; Quax, W.J., Essential oil constituents of Piper cubeba from Indonesia, 2006, retrieved from http://dissertations.ub.rug.nl/FILES/facultiew/science/2006/elfahmi/05c5.pdf. [all data]

Figuérédo, Cabassu, et al., 2006
Figuérédo, G.; Cabassu, P.; Chalchat, J.-C.; Pasquier, B., Studies of Mediterranean oregano populations. VIII. Chemical composition of essential oils of oreganos of various origins, Flavour Fragr. J., 2006, 21, 1, 134-139, https://doi.org/10.1002/ffj.1543 . [all data]

Bos, Stojanova, et al., 2005
Bos, R.; Stojanova, A.; Woerdenbag, H.J.; Koulman, A.; Quax, W.J., Volatile components of the aerial parts of Artemisia pontica L. grown in Bulgaria, Flavour Fragr. J., 2005, 20, 2, 145-148, https://doi.org/10.1002/ffj.1399 . [all data]

Duarte, Figueira, et al., 2005
Duarte, M.C.T.; Figueira, G.M.; Sartoratto, A.; Rehder, V.L.G.; Delarmelina, C., Anti-Candida activity of Brazilian medicinal plants, J. Ethnopharmacol., 2005, 97, 2, 305-311, https://doi.org/10.1016/j.jep.2004.11.016 . [all data]

Özel, Gögüs, et al., 2005
Özel, M.Z.; Gögüs, F.; Hamilton, J.F.; Lewis, A.C., Analysis of volatile components from Ziziphora taurica subsp. taurica by steam distillation, superheated-water extraction, and direct thermal desorption with GC×GC-TOFMS, Anal. Bioanal. Chem., 2005, 382, 1, 115-119, https://doi.org/10.1007/s00216-005-3156-x . [all data]

Rasooli and Owlia, 2005
Rasooli, I.; Owlia, P., Chemoprevention by thyme oils of Aspergillus parasiticus growth and aflatoxin production, Phytochemistry, 2005, 66, 24, 2851-2856, https://doi.org/10.1016/j.phytochem.2005.09.029 . [all data]

Kilic, Hafizoglu, et al., 2004
Kilic, A.; Hafizoglu, H.; Kollmannsberger, H.; Nitz, S., Volatile constituents and key odorants in leaves, buds, flowers, and fruits of Laurus nobilis L., J. Agric. Food Chem., 2004, 52, 6, 1601-1606, https://doi.org/10.1021/jf0306237 . [all data]

Rasooli and Razzaghi Abyaneh, 2004
Rasooli, I.; Razzaghi Abyaneh, M., Inhibitory effects of Thyme oils on growth and aflatoxin production by Aspergillus parasiticus, Food Control, 2004, 15, 6, 479-483, https://doi.org/10.1016/j.foodcont.2003.07.002 . [all data]

Ghannadi and Zolfaghari, 2003
Ghannadi, A.; Zolfaghari, B., Compositional analysis of the essential oil of Lallemantia royleana (Benth. in Wall.) Benth. from Iran, Flavour Fragr. J., 2003, 18, 3, 237-239, https://doi.org/10.1002/ffj.1215 . [all data]

Masotti, Juteau, et al., 2003
Masotti, V.; Juteau, F.; Bessière, J.M.; Viano, J., Seasonal and phenological variations of the essential oil from the narrow endemic species Artemisia molinieri and its biological activities, J. Agric. Food Chem., 2003, 51, 24, 7115-7121, https://doi.org/10.1021/jf034621y . [all data]

Perez-Alonso, Velasco-Negueruela, et al., 2003
Perez-Alonso, M.J.; Velasco-Negueruela, A.; Palá-Paúl, J.; Sanz, J., Variations in the essential oil composition of Artemisia pedemontana gathered in Spain: chemotype camphor-1,8-cineole and chemotype davanone, Biochem. Syst. Ecol., 2003, 31, 1, 77-84, https://doi.org/10.1016/S0305-1978(02)00082-0 . [all data]

Pino, Marbot, et al., 2003
Pino, J.A.; Marbot, R.; Fuentes, V., Characterization of volatiles in Bullock's heart (Annona reticulata L.) fruit cultivars from Cuba, J. Agric. Food Chem., 2003, 51, 13, 3836-3839, https://doi.org/10.1021/jf020733y . [all data]

Gallori, Flamini, et al., 2001
Gallori, S.; Flamini, G.; Bilia, A.R.; Morelli, I.; Landini, A.; Vincieri, F.F., Chemical composition of some traditional herbal drug preparations: essential oil and aromatic water of costmary (Balsamita suaveolens Pers.), J. Agric. Food Chem., 2001, 49, 12, 5907-5910, https://doi.org/10.1021/jf0107656 . [all data]

Doneanu and Anitescu, 1998
Doneanu, C.; Anitescu, G., Supercritical carbon dioxide extraction of Angelica archangelica L. root oil, J. Supercrit. Fluids, 1998, 12, 1, 59-67, https://doi.org/10.1016/S0896-8446(97)00040-5 . [all data]


Notes

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