Tricyclo[2.2.1.0(2,6)]heptane, 1,7,7-trimethyl-

Formula: C₁₀H₁₆
Molecular weight: 136.2340
IUPAC Standard InChI: InChI=1S/C10H16/c1-9(2)6-4-7-8(5-6)10(7,9)3/h6-8H,4-5H2,1-3H3
IUPAC Standard InChIKey: RRBYUSWBLVXTQN-UHFFFAOYSA-N
CAS Registry Number: 508-32-7
Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript.
Species with the same structure:
- 2,3,3-trimethyltricyclo[2.2.1.02,6]heptane
Other names: Tricyclene; 1,7,7-Trimethyltricyclo[2.2.1.0,2,6]heptane; Cyclene; NSC 86978; 1,7,7-Trimethyl-tricyclo[2.2.1.0*2,6*]heptane; α-Tricyclene; Tricyclo[2.2.1.02,6]heptane, 1,7,7-trimethyl-; 1,7,7-Trimethyltricyclo[2.2.1(2.6)]heptane; 1,7,7-trimethyltricyclo[2.2.1.02,6]heptane
Information on this page:
Other data available:
Data at other public NIST sites:
- Gas Phase Kinetics Database
Options:
- Switch to calorie-based units

Normal alkane RI, non-polar column, temperature ramp

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-1	HP-5 MS	CP-Sil 5 CB	RTX-5
Column length (m)	60.	30.	30.	25.	30.
Carrier gas	Helium	Helium	Helium	Hydrogen	Nitrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.15	0.25
T_start (C)	40.	60.	50.	50.	60.
T_end (C)	250.	240.	250.	230.	210.
Heat rate (K/min)	3.	3.	7.	3.	3.
Initial hold (min)	1.		1.
Final hold (min)	20.		5.
I	921.	915.	924.	934.	928.
Reference	Sardashti, Valizadeh, et al., 2013	Alizadeh and Shaabani, 2012	Zouari, Ayadi, et al., 2012	Esseien, Aboaba, et al., 2011	Prasad, Moulekhi, et al., 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	BP-1	SPB-1	HP-5 MS	DB-1-MS
Column length (m)	30.		30.	30.	60.
Carrier gas	Helium	Nitrogen	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25		0.20	0.25	0.25
Phase thickness (μm)	0.25		0.20	0.25	0.25
T_start (C)	50.	60.	70.	60.	30.
T_end (C)	250.	220.	220.	220.	200.
Heat rate (K/min)	2.	5.	3.	5.	2.
Initial hold (min)		10.		10.	4.
Final hold (min)		30.	15.		35.
I	927.	921.	921.	926.	915.
Reference	Ho, Wang, et al., 2010	Mishra, Chaudhary, et al., 2010	Neves, Rosa, et al., 2010	Ogunwande, Flamini, et al., 2010	Takeoka, Hobbs, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-54	RTX-1	RTX-1	DB-5	HP-5MS
Column length (m)	30.	60.	60.	30.	30.
Carrier gas	Helium	Helium	Helium	Nitrogen	Helium
Substrate
Column diameter (mm)	0.25	0.22	0.22	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	40.	50.
T_end (C)	260.	230.	230.	230.	240.
Heat rate (K/min)	2.	2.	2.	2.	5.
Initial hold (min)	5.
Final hold (min)	999.	30.	30.
I	924.	901.	927.	915.	924.
Reference	Dayisoylu and Alma, 2009	Museli, Pau, et al., 2009	Museli, Pau, et al., 2009	Scrivanti, Anton, et al., 2009	Wannes, Mhamdi, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5	SLB-5 MS	ZB-1	DB-5
Column length (m)	30.	30.	30.	30.	60.
Carrier gas	Helium	Helium	Helium	Nitrogen	Nitrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	50.	50.	45.	60.
T_end (C)	230.	300.	250.	230.	250.
Heat rate (K/min)	4.	3.	3.	3.	5.
Initial hold (min)	4.		2.
Final hold (min)	10.	30.	10.		10.
I	927.	923.	922.	917.	924.
Reference	Forero, Quijano, et al., 2008	Isidorov, Lech, et al., 2008	Lo Presti, Sciarrone, et al., 2008	Mierendorff, Stahl-Biskup, et al., 2008	Mosayebi, Amin, et al., 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Elite-1	HP-5	HP-5	HP-5 MS	DB-5
Column length (m)	30.	30.	30.	30.	50.
Carrier gas	Helium	Nitrogen	Helium	Helium	Nitrogen
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.20
Phase thickness (μm)	0.25	0.25	0.32	0.25	0.32
T_start (C)	60.	50.	60.	50.	60.
T_end (C)	246.	280.	250.	230.	220.
Heat rate (K/min)	3.	5.	5.	3.	5.
Initial hold (min)		1.	30.	10.	3.
Final hold (min)		1.		10.	5.
I	920.	930.	925.	926.	924.
Reference	Raj, Baby, et al., 2008	Saidana, Mahjoub, et al., 2008	Yassa and Akhani, 2008	Adams, Beauchamp, et al., 2007	Amiri, 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	HP-5MS	DB-5	HP-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	N2	He	He	N2	Helium
Substrate
Column diameter (mm)	0.32	0.25	0.26	0.25	0.26
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	50.	60.
T_end (C)	300.	280.	240.	240.	290.
Heat rate (K/min)	4.	3.	3.	5.	3.
Initial hold (min)				1.
Final hold (min)				4.
I	916.	922.	920.	926.	920.
Reference	Baran, von Reuss, et al., 2007	Basta, Pavlovic, et al., 2007	Bos, Woerdenbag, et al., 2007	Cheraif, Ben Jannet, et al., 2007	Elfami, Bos, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	Col-Elite 5MS	DBP-5	RTX-5 MS	DB-5
Column length (m)	30.	30.	25.	30.	30.
Carrier gas	He	He	Helium	He	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.22	0.25	0.25
T_start (C)	35.	30.	40.	45.	60.
T_end (C)	220.	246.	250.	210.	300.
Heat rate (K/min)	3.	3.	3.	3.	3.
Initial hold (min)			1.
Final hold (min)	40.		10.
I	931.	901.	895.	919.	905.
Reference	El-Ghorab A., El-Massry K.F., et al., 2007	Gudaityte and Venskutonis R.P., 2007	Heravi and Sereshti, 2007	Hudaib and Aburjai, 2007	Moreno, Lima, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-1	SPB-5	DB-1	DBP-5	Elite-5MS
Column length (m)	30.	30.	60.	25.	30.
Carrier gas	He	He	He	Helium	He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.2	0.25	0.25	0.22	0.5
T_start (C)	70.	50.	60.	40.	40.
T_end (C)	220.	250.	250.	250.	280.
Heat rate (K/min)	3.	2.	5.	3.	4.
Initial hold (min)				1.	5.
Final hold (min)	15.			10.	10.
I	923.	920.	927.	895.	921.
Reference	Pinto, Salgueiro, et al., 2007	Raal, Orav, et al., 2007	Salehi, Fakhari, et al., 2007	Sereshti and Samadi, 2007	Tava, Pecetti, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5MS	HP-5 MS	HP-5MS	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	He	Helium	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.32
T_start (C)	60.	60.	60.	40.	60.
T_end (C)	280.	280.	280.	250.	250.
Heat rate (K/min)	3.	3.	3.	3.	5.
Initial hold (min)				5.	30.
Final hold (min)				10.
I	925.	906.	927.	920.	925.
Reference	Tsokou, Georgopoulos, et al., 2007	Tzakou, Bazos, et al., 2007	Vagionas, Graikou, et al., 2007	Vichi, Riu-Aumatell, et al., 2007	Yassa and Akhani, 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	ZB-5	SPB-1	HP-5MS	DB-5
Column length (m)	25.	30.	30.	30.	30.
Carrier gas	He		Helium		Helium
Substrate
Column diameter (mm)		0.25	0.20	0.25	0.26
Phase thickness (μm)		0.25	0.20	0.25	0.25
T_start (C)	80.	40.	70.	60.	60.
T_end (C)	270.	300.	220.	280.	290.
Heat rate (K/min)	10.	2.	3.	4.	3.
Initial hold (min)
Final hold (min)			15.
I	927.	924.	921.	927.	920.
Reference	Ayoub, Al-Azizi, et al., 2006	Biondi, Sari, et al., 2006	Cavaleiro, Pinto, et al., 2006	Ebrahim Sajjadi and Mehregan, 2006	Elfami, Komar, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-1	DB-5	DB-5	HP-5MS
Column length (m)	30.	50.	30.	30.	30.
Carrier gas	He	He	He	Helium	He
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.33	0.25	0.25	0.25
T_start (C)	50.	60.	50.	60.	50.
T_end (C)	300.	250.	250.	260.	280.
Heat rate (K/min)	5.	2.	3.	3.	5.
Initial hold (min)	5.				4.
Final hold (min)	5.	40.	10.		10.
I	922.	921.	926.	925.	925.
Reference	Figuérédo, Cabassu, et al., 2006	Filippi, Lanfranchi, et al., 2006	Havlik, Kokoska, et al., 2006	Javidnia, Miri, et al., 2006	Kim, El-Aty, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	CP Sil 5 CB	HP-5 MS	HP-5	DB-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	N2	Nitrogen	N2	He
Substrate
Column diameter (mm)	0.32	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.52	0.25
T_start (C)	60.	50.	50.	50.	60.
T_end (C)	300.	300.	280.	280.	280.
Heat rate (K/min)	4.	4.	5.	5.	3.
Initial hold (min)
Final hold (min)			5.	5.	30.
I	916.	906.	926.	926.	915.
Reference	Kula, Izydorczyk, et al., 2006	Lis and Milczarek, 2006	Marzouk, Mansour, et al., 2006	Marzouk, Neffati, et al., 2006	Maronigiu, Piras, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	5 % Phenyl methyl siloxane	NB-30	HP-5	HP-5MS	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	He	H2	He	He
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	50.	60.	60.
T_end (C)	280.	250.	280.	280.	260.
Heat rate (K/min)	3.	2.	4.	3.	5.
Initial hold (min)			2.
Final hold (min)	30.		10.
I	905.	916.	926.	907.	923.
Reference	Marongiu, Piras, et al., 2006	Orav, Raal, et al., 2006	Pino, Sauri-Duch, et al., 2006	Pitarokili, Tzakou, et al., 2006	Sabulal, Dan, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	SPB-1	DB-5	DB-5	DB-5
Column length (m)	60.	30.	30.	30.	50.
Carrier gas	Helium	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.249	0.3
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	40.	60.	60.
T_end (C)	250.	250.	250.	290.	240.
Heat rate (K/min)	5.	4.	4.	3.	2.
Initial hold (min)		1.
Final hold (min)	10.	10.
I	924.	927.	911.	921.	918.
Reference	Sonboli, Mirjalili, et al., 2006	Wong, Sivasothy, et al., 2006	Yadegarinia, Gachkar, et al., 2006	Bos, Stojanova, et al., 2005	Chagonda and Chalchat, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-5	DB-1	HP-5	DB-1	DB-5
Column length (m)	60.	60.	30.	30.	30.
Carrier gas	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	1.	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	50.	50.	35.
T_end (C)	230.	250.	300.	265.	280.
Heat rate (K/min)	3.	5.	5.	2.5	4.
Initial hold (min)	5.		5.	1.	2.
Final hold (min)			5.	20.
I	928.	926.	922.	911.	919.
Reference	Cornu, Kondjoyan, et al., 2005	Fakhari, Salehi, et al., 2005	Figuérédo, Cabassu, et al., 2005	Khanavi, Ghasemian, et al., 2005	Kowalski and Wolski, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5MS	DB-5	CP Sil 5 CB	HP-5MS
Column length (m)	30.	30.	30.	25.	30.
Carrier gas	Helium	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.15
T_start (C)	35.	60.	60.	50.	60.
T_end (C)	280.	280.	220.	230.	280.
Heat rate (K/min)	4.	3.	4.	3.	3.
Initial hold (min)	2.	30.	5.
Final hold (min)
I	919.	906.	927.	928.	927.
Reference	Kowalski, 2005	Marongiu, Piras, et al., 2005	Morteza-Semnani, Akbarzadeh, et al., 2005	Ogunwande, Olawore, et al., 2005	Petrakis, Roussis, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5MS	HP-5MS	RTX-1	DB-5
Column length (m)	60.	30.	30.	60.	30.
Carrier gas	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	60.	60.	40.
T_end (C)	250.	240.	280.	25.	210.
Heat rate (K/min)	4.	3.	3.	5.	2.
Initial hold (min)					2.
Final hold (min)				10.	33.
I	909.	926.	922.	926.	928.
Reference	Rasooli and Owlia, 2005	da Silva, Andrade, et al., 2005	Slavkovska, Couladis, et al., 2005	Sonboli, Salehi, et al., 2005	Stevanovic, Garneau, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5MS	DB-1	DB-5	SE-54
Column length (m)	30.	30.	50.	60.	30.
Carrier gas	He	He		He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	60.	40.	60.
T_end (C)	240.	280.	240.	280.	260.
Heat rate (K/min)	3.	3.	3.	4.	2.
Initial hold (min)	3.			4.	5.
Final hold (min)
I	904.	907.	908.	922.	923.
Reference	Tepe B., Sokmen M., et al., 2005	Tzakou, Bazos, et al., 2005	Velasco-Negueruela, Pérez-Alonso, et al., 2005	Kalvandi, Sefidkon, et al., 2004	Kilic, Hafizoglu, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	DB-5MS	DB-5MS	NB-30	DB-1
Column length (m)	30.	30.	30.	50.	60.
Carrier gas	N2	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.2	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	50.	50.
T_end (C)	300.	280.	280.	250.	250.
Heat rate (K/min)	4.	3.	3.	2.	4.
Initial hold (min)
Final hold (min)		30.	30.
I	908.	902.	908.	920.	909.
Reference	Lis, Boczek, et al., 2004	Marongiu, Piras, et al., 2004	Marongiu, Porcedda, et al., 2004	Raal, Arak, et al., 2004	Rasooli and Razzaghi Abyaneh, 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5MS	HP-5MS	HP-5	RSL-200
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	H2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	35.	60.	60.	60.	40.
T_end (C)	220.	275.	280.	275.	280.
Heat rate (K/min)	2.5	4.	3.	4.	6.
Initial hold (min)					5.
Final hold (min)	6.				5.
I	927.	925.	923.	921.	929.
Reference	Rohloff, Mordal, et al., 2004	Afsharypuor and Jahromy, 2003	Couladis, Özcan, et al., 2003	Ghannadi and Zolfaghari, 2003	Jirovetz, Buchbauer, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	ZB-1	DB-1	DB-1	DB-5	HP-5
Column length (m)	30.	60.	50.	30.	30.
Carrier gas	N2	He	N2	H2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	45.	50.	95.	60.	60.
T_end (C)	230.	270.	240.	280.	280.
Heat rate (K/min)	3.	4.	4.	4.	3.
Initial hold (min)				10.
Final hold (min)				40.
I	917.	935.	934.	926.	905.
Reference	Mierendorff, Stahl-Biskup, et al., 2003	Mirza, Nik, et al., 2003	Perez-Alonso, Velasco-Negueruela, et al., 2003	Pino, Marbot, et al., 2003	Pitarokili, Tzakou, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5	HP-5	HP-5	HP-5
Column length (m)	30.	25.	25.	25.	25.
Carrier gas	He	H2	H2	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.32	0.32	0.32	0.32
Phase thickness (μm)	0.25	0.53	0.53	0.53	0.53
T_start (C)	60.	40.	40.	40.	40.
T_end (C)	275.	280.	280.	280.	280.
Heat rate (K/min)	4.	4.	4.	4.	4.
Initial hold (min)
Final hold (min)
I	925.	923.	927.	917.	927.
Reference	Sadraei, Ghannadi, et al., 2003	Velickovic, Randjelovic, et al., 2003	Velickovic, Randjelovic, et al., 2003	Velickovic, Ristic, et al., 2003	Velickovic, Ristic, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-1	DB-5MS	BP-1	HP-5
Column length (m)	30.	30.	30.	25.	30.
Carrier gas	He	He	He	N2	He
Substrate
Column diameter (mm)	0.249	0.25	0.25	0.50	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	70.	60.	60.	60.
T_end (C)	300.	220.	280.	220.	275.
Heat rate (K/min)	3.	3.	3.	5.	4.
Initial hold (min)
Final hold (min)	5.	15.		10.
I	921.	921.	938.	920.	920.
Reference	Bos, Koulman, et al., 2002	Cavaleiro, Salgueiro, et al., 2002	Congiu, Falconieri, et al., 2002	Das, Ram, et al., 2002	Ghannadi, Sajjadi, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	PTE-5	SE-30	HP-5	DB-5	DB-1
Column length (m)	60.	50.	30.	30.	30.
Carrier gas	H2	He		He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.30	0.25		0.25	0.25
T_start (C)	60.	70.	50.	35.	60.
T_end (C)	285.	240.	200.	280.	250.
Heat rate (K/min)	4.3	4.	3.	3.	4.
Initial hold (min)				2.	10.
Final hold (min)				15.
I	926.	932.	924.	920.	918.
Reference	Gudzic, Djokovic, et al., 2002	Iñigo, Palá-Paúl, et al., 2002	Isidorov and Jdanova, 2002	Krauze-Baranowska, Mardarowicz, et al., 2002	Norouzi-Arasi, Yavari, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5MS	HP-1	DB-1	DB-1	DB-1
Column length (m)	30.	50.	50.	60.	60.
Carrier gas	He	N2	N2	N2	N2
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.248	0.248
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	90.	60.	60.	60.
T_end (C)	280.	220.	240.	220.	220.
Heat rate (K/min)	4.	3.	3.	3.	3.
Initial hold (min)				5.	5.
Final hold (min)	5.			22.	22.
I	921.	917.	908.	926.	926.
Reference	Phutdhawong, Korth, et al., 2002	Priestap, van Baren, et al., 2002	Velasco-Negueruela, Pérez-Alonso, et al., 2002	Bailac, Dellacasa, et al., 2001	Bailac, Dellacasa, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5MS	SPB-5	DB-1	DB-1	DB-1
Column length (m)	30.	60.	60.	60.	60.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25		0.25	0.25	0.25
T_start (C)	60.	40.	40.	40.	50.
T_end (C)	240.	220.	280.	280.	270.
Heat rate (K/min)	3.	3.	4.	4.	4.
Initial hold (min)		5.	5.	5.
Final hold (min)		15.
I	925.	911.	918.	919.	933.
Reference	Cherchi, Deidda, et al., 2001	Cornu, Carnat, et al., 2001	Dabiri and Sefidkon, 2001	Dabiri and Sefidkon, 2001	Mirza, Ahmadi, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-1	DB-1	DB-1
Column length (m)	30.	30.	25.	30.	25.
Carrier gas	H2	He	Nitrogen	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.50	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	40.	50.
T_end (C)	285.	240.	220.	260.	290.
Heat rate (K/min)	3.	3.	5.	2.	4.
Initial hold (min)				5.
Final hold (min)				2.
I	920.	927.	921.	922.	921.
Reference	Santos-Gomes and Fernandes-Ferreira, 2001	Tellez M., Estell R., et al., 2001	Mallavarapu, Rao, et al., 2000	Senatore, Napolitano, et al., 2000	Koulman, 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	DB-5	DB-5MS	SPB-5
Column length (m)	60.	30.	30.	30.	50.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	60.	60.	60.
T_end (C)	280.	240.	240.	240.	240.
Heat rate (K/min)	4.	3.	3.	3.	3.
Initial hold (min)	5.
Final hold (min)					20.
I	940.	927.	926.	924.	925.
Reference	Sefidkon, Dabiri, et al., 1999	Tellez, Canel, et al., 1999	Zoghbi, Andrade, et al., 1999	Zoghbi, Andrade, et al., 1999, 2	Doneanu and Anitescu, 1998
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	HP-1	CP Sil 5 CB	SPB-Sulfur
Column length (m)	30.	30.	60.	25.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	4.
T_start (C)	60.	60.	50.	60.	45.
T_end (C)	240.	240.	280.	300.	240.
Heat rate (K/min)	3.	3.	4.	6.	5.
Initial hold (min)			5.		13.
Final hold (min)					5.
I	918.	927.	922.	919.	936.
Reference	El-Sakhawy, El-Tantawy, et al., 1998	Maia, Zohhbi, et al., 1998	Stashenko, Cervantes, et al., 1998	Bos, Woerdenbag, et al., 1997	Mariaca, Berger, et al., 1997
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-Sulfur	DB-1	DB-5	OV-101	OV-101
Column length (m)	30.		30.	50.	50.
Carrier gas	He		Helium	He	He
Substrate
Column diameter (mm)	0.32		0.25	0.25	0.2
Phase thickness (μm)	4.		0.25		0.5
T_start (C)	45.	80.	60.	50.	70.
T_end (C)	240.	220.	240.	250.	180.
Heat rate (K/min)	5.	6.	3.	2.	1.
Initial hold (min)	13.
Final hold (min)	5.
I	936.	921.	926.	918.	919.
Reference	Mariaca, Berger, et al., 1997	Salgueiro, Vila, et al., 1997	Tellez, Estell, et al., 1997	Orav, Kailas, et al., 1996	Orav, Kuningas, et al., 1995
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	SE-54
Column length (m)			30.
Carrier gas			Hydrogen
Substrate
Column diameter (mm)			0.25
Phase thickness (μm)			0.25
T_start (C)	40.	40.	60.
T_end (C)	210.	210.	250.
Heat rate (K/min)	2.	2.	2.
Initial hold (min)			5.
Final hold (min)			2.
I	926.	934.	920.
Reference	Collin, Deslauriers, et al., 1993	Collin, Deslauriers, et al., 1993	Kollmannsberger, Nitz, et al., 1992
Comment	MSDC-RI	MSDC-RI	MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

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Sardashti, A.R.; Valizadeh, J.; Adhami, Y., Variations in the essential oil composition of Peroskia abrotonolides of different growth stage in Baluchestan, Middle-East J. Sci. Res., 2013, 13, 6, 781-784. [all data]

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Salehi, Fakhari, et al., 2007
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Sereshti and Samadi, 2007
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Tava, Pecetti, et al., 2007
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Tsokou, Georgopoulos, et al., 2007
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Tzakou, Bazos, et al., 2007
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Vagionas, Graikou, et al., 2007
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Vichi, Riu-Aumatell, et al., 2007
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Yassa and Akhani, 2007
Yassa, N.; Akhani, H., The essential oils composition in two species of the genus Eriocycla Lindl. (Apiaceae) from Iran, 2007, retrieved from http://biology.ut.ac.ir/members/akhani/PdfReprintNumber/27.pdf. [all data]

Ayoub, Al-Azizi, et al., 2006
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Biondi, Sari, et al., 2006
Biondi, D.M.; Sari, M.i.; Ghani, Z.A.l.; Ruberto, G., Essential oil of Algerian Saccocalyx satureioides Coss. et Durieu, Flavour Fragr. J., 2006, 21, 3, 546-548, https://doi.org/10.1002/ffj.1661 . [all data]

Cavaleiro, Pinto, et al., 2006
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Ebrahim Sajjadi and Mehregan, 2006
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Koulman, 1999
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Salgueiro, Vila, et al., 1997
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Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References

Symbols used in this document:

T_end Final temperature

T_start Initial temperature
Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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