Borneol

Formula: C₁₀H₁₈O
Molecular weight: 154.2493
IUPAC Standard InChI: InChI=1S/C10H18O/c1-9(2)7-4-5-10(9,3)8(11)6-7/h7-8,11H,4-6H2,1-3H3/t7?,8-,10?/m1/s1
IUPAC Standard InChIKey: DTGKSKDOIYIVQL-CCNFQMFXSA-N
CAS Registry Number: 507-70-0
Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript.
Species with the same structure:
- Isoborneol
- Bicyclo[2.2.1]heptan-2-ol, 1,7,7-trimethyl-, (1S-endo)-
Stereoisomers:
Other names: Bicyclo[2.2.1]heptan-2-ol, 1,7,7-trimethyl-; endo-Borneol; endo-2-Hydroxy-1,7,7-trimethylnorbornane; Camphol; Bicyclo[2.2.1]heptan-2-ol, 1,7,7-trimethyl-, endo-; 2-Bornanol, endo-; Baros camphor; Bhimsaim camphor; Borneo camphor; trans-Borneol; Bornyl alcohol; Camphane, 2-hydroxy-; 2-Camphanol; Dryobalanops camphor; 2-Hydroxycamphane; Malayan camphor; Sumatra camphor; 1,7,7-Trimethyl-bicyclo(2.2.1)heptan-2-ol, endo-; UN 1312; Bhimsiam camphor; dl-Borneol; Endo-1,7,7-trimethylbicyclo[2.2.1]heptan-2-ol; Endo-2-bornanol; Endo-2-camphanol; Endo-2-hydroxycamphane; Malay camphor; 1,7,7-Trimethylbicyclo[2.2.1]heptan-2-ol; 2-endo-Bornyl alcohol; Camphor
Information on this page:
Other data available:
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Van Den Dool and Kratz RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	BP-1	BP-1	DB-5	HP-5
Column length (m)	60.	50.	50.	30.	30.
Carrier gas	He	He	He	He	N2
Substrate
Column diameter (mm)	0.22	0.22	0.22	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	230.	220.	220.	240.	220.
Heat rate (K/min)	2.	2.	2.	3.	5.
Initial hold (min)					10.
Final hold (min)	30.	20.	20.
I	1148.	1148.	1149.	1167.	1167.
Reference	Bendahou, Muselli, et al., 2008	Castilho, Liu, et al., 2007	Duquesnoy, Castola, et al., 2007	Flamini, Cioni, et al., 2007	Flamini, Tebano, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5MS	BP-1	DB-5	RTX-1
Column length (m)	30.	30.	50.	30.	60.
Carrier gas	He	He	He		He
Substrate
Column diameter (mm)	0.25	0.25	0.22	0.22	0.22
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	246.	280.	220.	240.	230.
Heat rate (K/min)	3.	3.	2.	3.	2.
Initial hold (min)				2.
Final hold (min)			20.		30.
I	1164.	1167.	1148.	1166.	1148.
Reference	Hongratanaworakit and Buchbauer, 2007	Kundakovic, Fokialakis, et al., 2007	Lesueur, de Rocca Serra, et al., 2007	Martins, Santos, et al., 2007	Muselli, Rossi, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Equity-5	DB-5	ZB-5	HP-5MS	DB-5
Column length (m)	60.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	1.	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	50.	60.	50.
T_end (C)	260.	260.	250.	280.	250.
Heat rate (K/min)	5.	5.	3.	3.	3.
Initial hold (min)	1.
Final hold (min)	15.				10.
I	1213.	1172.	1164.	1166.	1172.
Reference	Rocha, Coelho, et al., 2007	Sabulal, Dan, et al., 2007	Simoniatto, Bonani, et al., 2007	Vagionas, Ngassapa, et al., 2007	Yu, Liao, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	CP Sil 5 CB	DB-5	BP-1	BP-1
Column length (m)	30.	30.	30.	50.	50.
Carrier gas	He	N2	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.22	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	80.	50.	60.	60.	60.
T_end (C)	300.	200.	240.	220.	220.
Heat rate (K/min)	4.	5.	3.	2.	2.
Initial hold (min)
Final hold (min)				20.	20.
I	1171.	1165.	1165.	1150.	1148.
Reference	Zeng, Zhao, et al., 2007	Andrianoelisoa H.S., Menut C., et al., 2006	Block, Flamini, et al., 2006	Boti, Bighelli, et al., 2006	Bousmaha, Boti, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	HP-5MS	DB-5	DB-5	BP-1
Column length (m)	60.	30.	30.	30.	50.
Carrier gas	He	He	N2	N2	He
Substrate
Column diameter (mm)	0.22	0.25	0.32	0.25	0.22
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	230.	280.	240.	240.	220.
Heat rate (K/min)	2.	3.	3.	3.	2.
Initial hold (min)			3.	3.
Final hold (min)	45.		5.	3.	20.
I	1150.	1166.	1164.	1165.	1150.
Reference	Cavalli, Tomi, et al., 2006	Chorianopoulos N., Evergets E., et al., 2006	Dob, Dahmane, et al., 2006	Dob, Dahmane, et al., 2006, 2	Duquesnoy, Dinh, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	BP-1	HP-5	DB-1	HP-5
Column length (m)	50.	50.	30.	30.	30.
Carrier gas	N2	He	He	N2	He
Substrate
Column diameter (mm)	0.2	0.22	0.25	0.25	0.25
Phase thickness (μm)	0.32	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	50.	60.
T_end (C)	220.	220.	250.	220.	250.
Heat rate (K/min)	5.	2.	3.	4.	10.
Initial hold (min)	3.				2.
Final hold (min)	5.	20.			10.
I	1165.	1151.	1169.	1154.	1175.
Reference	Esmaeili, Nematollahi, et al., 2006	Gonny, Cavaleiro, et al., 2006	Javidnia, Miri, et al., 2006	Kuiate, Bessière, et al., 2006	Liu J.M., Nan P., et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-1	RTX-1	HP-5MS	SPB-1	SPB-1
Column length (m)	25.	60.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.2	0.22	0.25	0.2	0.25
Phase thickness (μm)	0.33	0.25	0.25	0.2	0.25
T_start (C)	60.	60.	60.	70.	50.
T_end (C)	300.	230.	280.	220.	250.
Heat rate (K/min)	5.	2.	3.	3.	5.
Initial hold (min)	3.				3.
Final hold (min)	30.	35.		15.	15.
I	1144.	1150.	1146.	1144.	1162.
Reference	Nath, Baruah, et al., 2006	Paolini J., Desjobert J.M., et al., 2006	Pavlovic, Kovacevic, et al., 2006	Pinto, Pina-Vaz, et al., 2006	Radulovic, Mananjarasoa, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	SPB-1	DB-5	HP-5MS	CP Sil 5 CB
Column length (m)	30.	30.	30.	30.	25.
Carrier gas	He	He	He	H2	H2
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.2	0.25	0.25
T_start (C)	50.	70.	50.	50.	80.
T_end (C)	265.	220.	250.	285.	270.
Heat rate (K/min)	2.5	3.	5.	4.3	10.
Initial hold (min)			2.
Final hold (min)		15.
I	1165.	1146.	1169.	1168.	1150.
Reference	Ramezani, Behravan, et al., 2006	Salgueiro L.R., Pinto E., et al., 2006	Su, Ho, et al., 2006	Vujisic L., Vuckovic I., et al., 2006	Ziegenbein, Hanssen, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-1	DB-5	SE-54	HP-5	RTX-1
Column length (m)	30.	30.	50.	30.	60.
Carrier gas	He	He	H2	N2
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.22
Phase thickness (μm)	0.25	0.25	0.27	0.25	0.25
T_start (C)	50.	50.	50.	60.	60.
T_end (C)	250.	250.	300.	220.	220.
Heat rate (K/min)	5.	5.	5.	5.	2.
Initial hold (min)	3.	3.		10.
Final hold (min)	15.	15.			20.
I	1162.	1155.	1165.	1169.	1151.
Reference	Boskovic, Radulovic, et al., 2005	Boskovic, Radulovic, et al., 2005	Brantner, Pfeifhofer, et al., 2005	Cioni, Flamini, et al., 2005	Cozzani, Muselli, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	5 % Phenyl methyl siloxane	CP Sil 5 CB	DB-5
Column length (m)	30.	30.	30.	50.	25.
Carrier gas	N2		He	H2	N2
Substrate
Column diameter (mm)	0.32	0.32	0.25	0.22	0.25
Phase thickness (μm)	0.25	0.25	1.	0.13	0.25
T_start (C)	50.	50.	40.	40.	75.
T_end (C)	260.	250.	250.	300.	210.
Heat rate (K/min)	2.	2.	7.	4.	3.
Initial hold (min)	3.	8.	10.		10.
Final hold (min)	5.		5.	10.	1.
I	1165.	1149.	1210.	1145.	1167.
Reference	Dob, Berramdane, et al., 2005	Dob, Dahmane, et al., 2005	Estevez, Ventanas, et al., 2005	Idzojtic, Kajba, et al., 2005	bin Jantan, Yalvema, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	HP-5MS	DB-5	DB-5	DB-5MS
Column length (m)	60.	30.	30.	30.	60.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.22	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.26	0.25	0.25
T_start (C)	60.	60.	60.	40.	40.
T_end (C)	230.	250.	210.	260.	200.
Heat rate (K/min)	2.	4.	3.	2.	2.
Initial hold (min)		2.		5.
Final hold (min)	35.	20.		20.	20.
I	1149.	1164.	1179.	1164.	1160.
Reference	Paolini, Costa, et al., 2005	Pino, Mesa, et al., 2005	Sati and Mathela, 2005	Senatore, Napolitano, et al., 2005	Seo and Baek, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Mega 5MS	HP-5MS	HP-5MS	HP-5MS	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	80.	80.	80.	45.
T_end (C)	240.	290.	290.	290.	180.
Heat rate (K/min)	3.	2.	4.	6.	2.5
Initial hold (min)	2.				10.
Final hold (min)					20.
I	1152.	1166.	1170.8	1171.8	1165.
Reference	Verzera, Trozzi, et al., 2005	Zhao, Liang, et al., 2005	Zhao, Liang, et al., 2005	Zhao, Liang, et al., 2005	Zhang, Xu, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-54	SPB-1	HP-5	HP-5MS	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He		He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	70.	60.	60.	60.
T_end (C)	260.	220.	220.	280.	240.
Heat rate (K/min)	2.	3.	5.	3.	3.
Initial hold (min)	5.		10.
Final hold (min)		15.
I	1162.	1144.	1169.	1166.	1175.
Reference	Alma, Nitz, et al., 2004	Antunes, Sevinate-Pinto, et al., 2004	Ceccarini, Macchia, et al., 2004	Chorianopoulos, Kalpoutzakis, et al., 2004	Flamini, Bader, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	BP-1	HP-5	DB-5	HP-5MS
Column length (m)	30.	50.	30.	30.	30.
Carrier gas	N2		He	He	He
Substrate
Column diameter (mm)	0.25	0.22	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	240.	220.	260.	260.	280.
Heat rate (K/min)	3.	2.	3.	3.	4.
Initial hold (min)					5.
Final hold (min)		20.
I	1168.	1149.	1166.	1165.	1166.
Reference	Flamini, Cioni, et al., 2004	Gonny, Bradesi, et al., 2004	Javidnia, Miri, et al., 2004	Javidnia, Miri, et al., 2004, 2	Karioti, Hadjipavlou-Litina, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5MS	SPB-1	SPB-1	HP-5MS	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.2	0.2	0.25	0.25
Phase thickness (μm)	0.25	0.2	0.2	0.25	0.25
T_start (C)	40.	70.	70.	50.	50.
T_end (C)	280.	220.	220.	300.	250.
Heat rate (K/min)	4.	3.	3.	5.	3.
Initial hold (min)	2.			5.
Final hold (min)		15.	15.
I	1173.	1149.	1149.	1167.	1167.
Reference	Mardarowicz, Wianowska, et al., 2004	Moldão-Martins, Beirão-da-Costa, et al., 2004	Moldão-Martins, Beirão-da-Costa, et al., 2004	Mumm, Tiemann, et al., 2004	Salido, Valenzuela, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	BP-1	HP-5MS	DB-5MS	DB-5MS
Column length (m)	25.	50.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.2	0.22	0.25	0.25	0.25
Phase thickness (μm)	0.33	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	40.	40.
T_end (C)	240.	220.	200.	200.	200.
Heat rate (K/min)	3.	2.	6.	4.	4.
Initial hold (min)			1.5	5.	5.
Final hold (min)	7.	20.	5.	20.	20.
I	1169.	1148.	1174.	1171.	1171.
Reference	Sartoratto, Machado, et al., 2004	Tam, Thuam, et al., 2004	Weissbecker, Holighaus, et al., 2004	Yu, Kim, et al., 2004	Yu, Kim, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5MS	DB-5	BPX-5	HP-5	HP-5
Column length (m)	30.	25.	30.	30.	30.
Carrier gas	He	N2	N2	N2	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	75.	75.	60.	60.
T_end (C)	200.	210.	210.	220.	220.
Heat rate (K/min)	4.	3.	3.	5.	5.
Initial hold (min)	5.	10.	10.	10.	10.
Final hold (min)	20.	1.	1.
I	1171.	1166.	1166.	1167.	1167.
Reference	Yu, Kim, et al., 2004, 2	bin Ahmad and bin Jantan, 2003	bin Ahmad and bin Jantan, 2003, 2	Angelini, Carpanese, et al., 2003	Angelini, Carpanese, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	SPB-1	RTX-1	SPB-1
Column length (m)	30.	30.	30.	60.	25.
Carrier gas	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.22	0.25
Phase thickness (μm)	0.25	0.25	0.2	0.25	0.25
T_start (C)	60.	60.	70.	60.	35.
T_end (C)	240.	240.	220.	230.	225.
Heat rate (K/min)	3.	3.	3.	2.	4.
Initial hold (min)					10.
Final hold (min)	30.		15.	45.
I	1167.	1168.	1149.	1150.	1147.
Reference	Bader, Caponi, et al., 2003	Bader, Flamini, et al., 2003	Cavaleiro, Salgueiro, et al., 2003	Cavalli, Tomi, et al., 2003	Chisholm, Wilson, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-1	DB-1	HP-5	HP-5	HP-5
Column length (m)	25.	30.	30.	30.	30.
Carrier gas		He	N2	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25
T_start (C)	35.	40.	60.	60.	25.
T_end (C)	225.	250.	220.	220.	150.
Heat rate (K/min)	4.	2.	5.	5.	3.
Initial hold (min)	10.	5.	10.	10.	5.
Final hold (min)		20.
I	1147.	1137.	1175.	1167.	1165.
Reference	Chisholm, Wilson, et al., 2003	de Feo, Bruno, et al., 2003	Flamini, Luigi Cioni, et al., 2003	Flamini, Luigi Cioni, et al., 2003, 2	Isidorov, Vinogorova, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	HP-5	HP-5
Column length (m)	30.	30.	25.	30.	30.
Carrier gas	He	N2	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	75.	75.	60.	60.	60.
T_end (C)	230.	230.	260.	240.	280.
Heat rate (K/min)	3.	3.	4.	3.	3.
Initial hold (min)	10.	10.
Final hold (min)	20.
I	1166.	1166.	1168.	1168.	1165.
Reference	Jantan, Ling, et al., 2003	bin Jantan, Yassin, et al., 2003	Javidnia, Miri, et al., 2003	Macchioni, Cioni, et al., 2003	Ngassapa, Runyoro, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	MS5	HP-5	HP-5	HP-5
Column length (m)	30.	25.	30.	30.	30.
Carrier gas	He		He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	40.	60.	60.	60.
T_end (C)	250.	180.	280.	280.	280.
Heat rate (K/min)	3.	3.	3.	3.	3.
Initial hold (min)
Final hold (min)
I	1165.	1165.	1169.	1169.	1168.
Reference	Salido, Altarejos, et al., 2003	Shao, Marriott, et al., 2003	Tsiri, Kretsi, et al., 2003	Tsiri, Kretsi, et al., 2003	Tzakou, Couladis, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	DB-5	DB-5	HP-5	RTX-5 MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas			He	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	50.	60.	60.	45.
T_end (C)	280.	280.	240.	220.	180.
Heat rate (K/min)	3.	3.	3.	5.	2.5
Initial hold (min)	5.	5.		10.	10.
Final hold (min)
I	1165.	1165.	1168.	1175.	1165.
Reference	Demetzos, Angelopoulou, et al., 2002	Economakis, Skaltsa, et al., 2002	Flamini, Cioni, et al., 2002	Flamini, Cioni, et al., 2002, 2	Hudaib, Speroni, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5	DB-5	RTX-5	HP-1
Column length (m)	25.	30.	25.	30.	24.
Carrier gas	N2	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)		0.25		0.25	0.17
T_start (C)	60.	60.	70.	45.	60.
T_end (C)	180.	280.	260.	300.	250.
Heat rate (K/min)	3.	3.	4.	3.	4.
Initial hold (min)	10.	5.		6.	2.
Final hold (min)	10.			10.	20.
I	1154.	1165.	1165.	1167.	1144.
Reference	bin Jantan and bin Ahmad, 2002	Magiatis, Skaltsounis, et al., 2002	Miri, Ramezani, et al., 2002	Mondello, Zappia, et al., 2002	Nath, Sarma, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	CP Sil 5 CB	CP Sil 5 CB	DB-1	RTX-5
Column length (m)	25.	30.	50.	50.	30.
Carrier gas	N2	H2	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.22	0.25
Phase thickness (μm)	0.25	0.25	0.4	0.25	0.25
T_start (C)	60.	60.	60.	60.	45.
T_end (C)	280.	280.	280.	220.	250.
Heat rate (K/min)	4.	2.	3.	2.	3.
Initial hold (min)	6.	10.	10.		6.
Final hold (min)		40.	60.	20.
I	1147.	1151.	1151.	1150.	1165.
Reference	Pino, Marbot, et al., 2002	Pino, Marbot, et al., 2002, 2	Pino, Marbot, et al., 2002, 3	Pintore, Usai, et al., 2002	Shellie, Mondello, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-5	HP-5	HP-5	BP-1	SPB-1
Column length (m)	30.	30.	30.	50.	15.
Carrier gas	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.22	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	45.	60.	60.	60.	35.
T_end (C)	250.	280.	280.	230.	225.
Heat rate (K/min)	3.	3.	3.	2.	6.
Initial hold (min)	6.	5.	5.		3.
Final hold (min)				35.	10.
I	1172.	1166.	1164.	1151.	1147.
Reference	Shellie, Mondello, et al., 2002	Aligiannis, Kalpoutzakis, et al., 2001	Aligiannis, Kalpoutzakis, et al., 2001, 2	Bianchini, Tomi, et al., 2001	Chisholm, Wilson, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-1	HP-5	HP-5	HP-5	HP-5MS
Column length (m)	15.	30.	30.	30.	30.
Carrier gas		He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.50	0.25
T_start (C)	35.	60.	60.	60.	60.
T_end (C)	225.	260.	380.	280.	280.
Heat rate (K/min)	6.	3.	3.	3.	3.
Initial hold (min)	3.				5.
Final hold (min)	10.	10.
I	1147.	1163.	1164.	1168.	1165.
Reference	Chisholm, Wilson, et al., 2001	Couladis, Baziou, et al., 2001	Couladis, Tsortanidou, et al., 2001	Couladis, Tzakou, et al., 2001	Giamakis, Kretsi, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-1	HP-5	RTX-5 MS	SE-30	CP Sil 5 CB
Column length (m)	60.	50.	30.	25.	50.
Carrier gas	He	He	He	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.20	0.32
Phase thickness (μm)	0.25	0.25	0.25		0.4
T_start (C)	50.	50.	70.	60.	60.
T_end (C)	250.	250.	210.	180.	280.
Heat rate (K/min)	2.5	2.5	4.	3.	3.
Initial hold (min)	5.	5.	10.	10.	10.
Final hold (min)			10.	1.	60.
I	1160.	1165.	1170.	1166.	1151.
Reference	Guilliard, Delgado, et al., 2001	Guilliard, Delgado, et al., 2001	Hudaib, Grazia Bellardi, et al., 2001	bin Jantan, Basni, et al., 2001	Pino, Marbot, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	HP-5MS	HP-5MS	SE-54	DB-5
Column length (m)	50.	30.	30.	25.	60.
Carrier gas		He	He		He
Substrate
Column diameter (mm)	0.22	0.25	0.25	0.31	0.25
Phase thickness (μm)	0.25	0.25	0.25		0.25
T_start (C)	60.	50.	60.	35.	40.
T_end (C)	220.	250.	280.	230.	290.
Heat rate (K/min)	2.	3.	4.	4.	4.
Initial hold (min)			5.	3.	2.
Final hold (min)	20.			10.	5.
I	1148.	1167.	1165.	1175.90	1160.
Reference	Rezzi, Cavaleiro, et al., 2001	Salido, Altarejos, et al., 2001	Skaltsa, Mavrommati, et al., 2001	Yin, Xiu, et al., 2001	Bartley and Jacobs, 2000
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	CP Sil 5 CB	DB-1	DB-1	DB-1
Column length (m)	30.	50.	60.	60.	60.
Carrier gas	He	H2		He	He
Substrate
Column diameter (mm)	0.25	0.22	0.32	0.32	0.25
Phase thickness (μm)	0.25	0.13	1.		0.25
T_start (C)	40.	40.	-50.	60.	50.
T_end (C)	200.	300.	175.	230.	220.
Heat rate (K/min)	2.	4.	6.	3.	4.
Initial hold (min)	5.		2.
Final hold (min)	20.	10.		5.
I	1160.	1155.	1162.9	1155.	1155.
Reference	Kim, Thuy, et al., 2000	Pfeifhofer, 2000	Helmig, Klinger, et al., 1999	Javidnia and Shafiee, 1999	Mirza and Sefidkon, 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-1	Methyl Silicone	CP Sil 5 CB	OV-1	DB-5
Column length (m)	60.	50.	25.	25.	30.
Carrier gas	He	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.17		0.3	0.25
T_start (C)	50.	80.	60.	50.	50.
T_end (C)	250.	200.	260.	200.	250.
Heat rate (K/min)	2.5	2.	5.	3.	3.
Initial hold (min)	5.			1.
Final hold (min)				20.
I	1169.	1164.	1155.	1143.	1166.
Reference	Stashenko, Cervantes, et al., 1999	Sumathykutty, Rao, et al., 1999	Weyerstahl, Marschall, et al., 1999	Bicchi, Rubiolo, et al., 1998	Isidorov, Zenkevich, et al., 1998
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	Methyl Silicone	BP-1	DB-5	Methyl Silicone
Column length (m)	50.		50.	30.	25.
Carrier gas	He		He	He	He
Substrate
Column diameter (mm)	0.22		0.22	0.26	0.2
Phase thickness (μm)	0.25		0.25	0.25	0.3
T_start (C)	60.	50.	60.	50.	40.
T_end (C)	220.	250.	230.	225.	200.
Heat rate (K/min)	2.	4.	2.	2.	2.
Initial hold (min)
Final hold (min)	20.		35.	20.
I	1154.	1149.	1148.	1174.	1164.
Reference	Tam, An, et al., 1998	Analytical Methods Committee, 1997	Mariotti, Tomi, et al., 1997	Sagrero-Nieves, Bartley, et al., 1997	Píry, Príbela, et al., 1995
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	CP Sil 5 CB	HP-101	OV-101	OV-101
Column length (m)	60.	25.	50.	50.	50.
Carrier gas		He	N2	N2	N2
Substrate
Column diameter (mm)	0.32	0.22	0.25	0.25	0.25
Phase thickness (μm)	0.5	0.11
T_start (C)	40.	80.	70.	80.	80.
T_end (C)	290.	230.	200.	200.	200.
Heat rate (K/min)	4.	1.	3.	2.	2.
Initial hold (min)	2.	8.
Final hold (min)	5.	16.
I	1154.	1147.	1180.	1153.	1155.
Reference	Bartley and Foley, 1994	Chanegriha and Baaliouamer, 1993	Chung, Eiserich, et al., 1993	Yang, Sugisawa, et al., 1992	Yang, Sugisawa, et al., 1992
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Packed	Capillary
Active phase	OV-101	OV-1	OV-1	OV-101	OV-101
Column length (m)	50.	30.	30.	2.
Carrier gas	H2	He	He	Ar
Substrate				W-AW-DMCS
Column diameter (mm)	0.32	0.5	0.5
Phase thickness (μm)		0.8	0.8
T_start (C)	50.	40.	40.	100.	100.
T_end (C)	200.	220.	220.
Heat rate (K/min)	2.	2.	2.	2.	2.
Initial hold (min)
Final hold (min)
I	1146.	1144.	1149.	1153.	1153.
Reference	Pieribattesti, Smadja, et al., 1988	De Pooter, Omar, et al., 1985	De Pooter, Omar, et al., 1985	Szabolcs, Benecke, et al., 1985	Benecke, Thieme, et al., 1982
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

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Chisholm, Wilson, et al., 2001
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bin Jantan, Basni, et al., 2001
bin Jantan, I.; Basni, I.; Ahmad, A.S.; Ali, N.A.M.; Ahmad, A.R.; Ibrahim, H., Constituents of the rhizome oils of Boesenbergia pandurata (Roxb.) Schlecht from Malaysia, Indonesia and Thailand, Flavour Fragr. J., 2001, 16, 2, 110-112, https://doi.org/10.1002/ffj.956 . [all data]

Pino, Marbot, et al., 2001
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Rezzi, Cavaleiro, et al., 2001
Rezzi, S.; Cavaleiro, C.; Bighelli, A.; Salgueiro, L.; da Cunha, A.P.; Casanova, J., Intraspecific chemical variability of the leaf essential oil of Juniperus phoenicea subsp. turbinata from Corsica, Biochem. Syst. Ecol., 2001, 29, 2, 179-188, https://doi.org/10.1016/S0305-1978(00)00044-2 . [all data]

Salido, Altarejos, et al., 2001
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Skaltsa, Mavrommati, et al., 2001
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Yin, Xiu, et al., 2001
Yin, W.; Xiu, Z.; Aijin, H., Analysis of the volatile components in trogopterorum feces by capillary gas chromatography and gas chromatography/mass spectrometry, Fenxi Huaxue, 2001, 29, 2, 195-198. [all data]

Bartley and Jacobs, 2000
Bartley, J.P.; Jacobs, A.L., Effects of drying on flavour compounds in Australian-grown ginger (Zingiber officinale), J. Sci. Food Agric., 2000, 80, 2, 209-215, https://doi.org/10.1002/(SICI)1097-0010(20000115)80:2<209::AID-JSFA516>3.0.CO;2-8 . [all data]

Kim, Thuy, et al., 2000
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Pfeifhofer, 2000
Pfeifhofer, H.W., Composition of the essential oil of Pinus canariensis Sweet ex Sprengel, Flavour Fragr. J., 2000, 15, 4, 266-270, https://doi.org/10.1002/1099-1026(200007/08)15:4<266::AID-FFJ908>3.0.CO;2-E . [all data]

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Javidnia and Shafiee, 1999
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Mirza and Sefidkon, 1999
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Stashenko, Cervantes, et al., 1999
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Sumathykutty, Rao, et al., 1999
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Weyerstahl, Marschall, et al., 1999
Weyerstahl, P.; Marschall, H.; Wahlburg, H.-C.; Christiansen, C.; Rustaiyan, A.; Mirdjalili, F., Constituents of the essential oil of Pulicaria gnaphalodes (Vent.) Boiss. from Iran, Flavour Fragr. J., 1999, 14, 2, 121-130, https://doi.org/10.1002/(SICI)1099-1026(199903/04)14:2<121::AID-FFJ790>3.0.CO;2-K . [all data]

Bicchi, Rubiolo, et al., 1998
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Isidorov, Zenkevich, et al., 1998
Isidorov, V.A.; Zenkevich, I.G.; Dubis, E.N.; Slowikowski, A.; Wojciuk, E., Group identification of essential oils components using partition coefficients in a hexane-acetonitrile system, J. Chromatogr. A, 1998, 814, 1-2, 253-260, https://doi.org/10.1016/S0021-9673(98)00398-7 . [all data]

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Bartley and Foley, 1994
Bartley, J.P.; Foley, P., Supercritical fluid extraction of Australian-grown ginger (Zingiber officinale), J. Sci. Food Agric., 1994, 66, 3, 365-371, https://doi.org/10.1002/jsfa.2740660314 . [all data]

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Chung, Eiserich, et al., 1993
Chung, T.Y.; Eiserich, J.P.; Shibamoto, T., Volatile compounds isolated from edible Korean chamchwi (Aster scaber Thunb), J. Agric. Food Chem., 1993, 41, 10, 1693-1697, https://doi.org/10.1021/jf00034a033 . [all data]

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De Pooter, H.L.; Omar, M.N.; Coolsaet, B.A.; Schamp, N.M., The Essential Oil of Greater Galanga (Alpinia Galanga) from Malaysia, Phytochemistry, 1985, 24, 1, 93-96, https://doi.org/10.1016/S0031-9422(00)80814-6 . [all data]

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Benecke, R.; Thieme, H.; Nyiredy, Sz., Retentionsverhalten der Hauptkomponenten der Lavendel und Lavandinöle an Verschiedenen stationären Phasen in Abhängigkeit von der Säulentemperatur, J. Chromatogr., 1982, 238, 1, 75-87, https://doi.org/10.1016/S0021-9673(00)82713-2 . [all data]

Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References

Symbols used in this document:

T_end Final temperature

T_start Initial temperature
Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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