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Chlorpromazine


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type PackedPackedCapillaryCapillaryCapillary
Active phase Polydimethyl siloxaneSE-30BP-1BP-1BP-1
Column length (m) 2.2.12.12.12.
Carrier gas NitrogenNitrogenHeHeHe
Substrate  Chromosorb G AW DMCS (80-100 mesh)   
Column diameter (mm)   0.220.220.22
Phase thickness (mum)   0.250.250.25
Tstart (C) 100.100.100.120.50.
Tend (C) 300.300.295.280.300.
Heat rate (K/min)   5.8.20.
Initial hold (min)      
Final hold (min)      
I 2487.2486.2452.2474.2481.
ReferenceMHA, 9999MHA, 9999Stowell and Wilson, 1985Stowell and Wilson, 1985Stowell and Wilson, 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPackedPacked
Active phase OV-101OV-1SE-30SE-30SE-30
Column length (m) 0.62.2.2.2.
Carrier gas N2  NitrogenN2
Substrate Chromosorb G HPGas Chrom PGas Chrom PChromosorb W AW DMS (80-100 mesh)Chromosorb W AW DMS
Column diameter (mm)      
Phase thickness (mum)      
Tstart (C) 100.150.150.130.130.
Tend (C) 310.300.300.290.290.
Heat rate (K/min) 20.5.5.8.8.
Initial hold (min)    2.2.
Final hold (min) 3.  8.8.
I 2500.2480.2490.2490.2490.
ReferenceMaurer and Pfleger, 1984Marozzi, Gambaro, et al., 1982Marozzi, Gambaro, et al., 1982Peel and Perrigo, 1976Peel and Perrigo, 1975
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

MHA, 9999
MHA, Directorate of ForensicScience., Forensic Toxicology, 9999. [all data]

Stowell and Wilson, 1985
Stowell, A.; Wilson, L., Use of retention indices in drug screening by capillary gas chromatography, Rep. # CD 2362, Department of Scientific and Industrial Reseach, Chemistry Division, Lower Hutt, NZ, 1985, 32. [all data]

Maurer and Pfleger, 1984
Maurer, H.; Pfleger, K., Screening procedure for detection of phenothiazine and analogous neuroleptics and their metabolites in urine using a computerized gas chromatographic-mass spectrometric technique, J. Chromatogr., 1984, 306, 125-145, https://doi.org/10.1016/S0378-4347(00)80876-2 . [all data]

Marozzi, Gambaro, et al., 1982
Marozzi, E.; Gambaro, V.; Saligari, E.; Mariani, R.; Lodi, F., Use of the retention index in gas chromatographic studies of drugs, J. Anal. Toxicol., 1982, 6, 4, 185-192, https://doi.org/10.1093/jat/6.4.185 . [all data]

Peel and Perrigo, 1976
Peel, H.W.; Perrigo, B., A practical gas chromatographic screening procedure for toxicological analysis, Can. Soc. Forens. Sci. J., 1976, 9, 2, 69-74, https://doi.org/10.1080/00085030.1976.10757247 . [all data]

Peel and Perrigo, 1975
Peel, H.W.; Perrigo, B., A practical gas chromatographic screening procedure for toxicological analysis, Can.Soc.Forens.Sci.J., 1975, 9, 2, 69-74, https://doi.org/10.1080/00085030.1976.10757247 . [all data]


Notes

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