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1,4-Dithiane

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Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1SE-54DB-1DB-5DB-1
Column length (m) 15.25.15.15.15.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.320.530.530.32
Phase thickness (mum) 0.250.25  0.25
Tstart (C) 50.40.50.50.50.
Tend (C) 280.280.  300.
Heat rate (K/min) 10.10.10.10.10.
Initial hold (min) 2.1.2.2.2.
Final hold (min) 10.10.  5.
I 1019.1068.1028.1067.71019.
ReferenceKostiainen, 2000Kostiainen, 2000Hancock and Peters, 1991Hancock and Peters, 1991D'agostino and Provost, 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase DB-5DB-1DB-5
Column length (m) 15.15.15.
Carrier gas  HeHe
Substrate    
Column diameter (mm) 0.320.320.32
Phase thickness (mum) 0.250.250.25
Tstart (C) 50.50.50.
Tend (C) 300.300.300.
Heat rate (K/min) 10.10.10.
Initial hold (min) 2.2.2.
Final hold (min) 5.5. 
I 1060.21018.71060.2
ReferenceD'agostino and Provost, 1988D'Agostino and Provost, 1985D'Agostino and Provost, 1985
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Kostiainen, 2000
Kostiainen, O., Gas Chromatography in Screening of Chemicals Related to the Chemical Weapons Convention in Encyclopedia of Analytical Chemistry, Meyers, R.A., ed(s)., John Wiley Sons Ltd, Chichester, 2000, 963-979. [all data]

Hancock and Peters, 1991
Hancock, J.R.; Peters, G.R., Retention index monitoring of compounds of chemical defence interest using thermal desorption gas chromatography, J. Chromatogr., 1991, 538, 2, 249-257, https://doi.org/10.1016/S0021-9673(01)88845-2 . [all data]

D'agostino and Provost, 1988
D'agostino, P.A.; Provost, L.R., Gas chromatographic retention indices of sulphur vesicants and related compounds, J. Chromatogr., 1988, 436, 399-411, https://doi.org/10.1016/S0021-9673(00)94599-0 . [all data]

D'Agostino and Provost, 1985
D'Agostino, P.A.; Provost, L.R., Gas chromatographic retention indices of chemical warfare agents and simulants, J. Chromatogr., 1985, 331, 47-54, https://doi.org/10.1016/0021-9673(85)80005-4 . [all data]


Notes

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