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1,3,7-Octatriene, 3,7-dimethyl-


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBSPB-5HP-5MSBP-1DB-5
Column length (m) 25.60.30.25.30.
Carrier gas  NitrogenHeHeHe
Substrate      
Column diameter (mm) 0.250.350.250.30.32
Phase thickness (mum) 0.150.250.25 0.25
Tstart (C) 50.60.50.70.60.
Tend (C) 230.230.280.220.280.
Heat rate (K/min) 3.4.5.4.5.
Initial hold (min)   4.2.0.5
Final hold (min)  40.10.10.2.
I 1040.1047.1018.1032.1052.
ReferenceUsman, Zubair, et al., 2010Gauvin-Bialecki and Marodon, 2009Kim, El-Aty, et al., 2006Moody, Gundidza, et al., 2006Ozel, Gogus, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5MSOV-101OV-101HP-5
Column length (m) 30.30.50.50.30.
Carrier gas  HeN2N2He
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (mum)  0.25   
Tstart (C) 60.60.80.80.80.
Tend (C) 280.280.200.200.200.
Heat rate (K/min) 3.3.2.2.9.
Initial hold (min)      
Final hold (min)     10.
I 1046.1046.1039.1039.1043.
ReferencePetrakis, Roussis, et al., 2005Congiu, Falconieri, et al., 2002Yang, 2001Yang, 2001, 2Lis-Balchin and Roth, 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1Methyl SiliconeDB-5SPB-5OV-101
Column length (m) 60.60.30.60.50.
Carrier gas He H2HeN2
Substrate      
Column diameter (mm) 0.250.250.320.320.25
Phase thickness (mum) 0.250.25 1. 
Tstart (C) 60.40.32.40.80.
Tend (C) 200.220.260.200.200.
Heat rate (K/min) 4.5.7.3.2.
Initial hold (min) 5.10.5.5. 
Final hold (min) 25. 5.2. 
I 1039.1039.501051.1050.1038.
ReferenceMeccia, Rojas, et al., 2000Baraldi, Rapparini, et al., 1999Sun and Petracek, 1999Viallon C., Verdier-Metz I., et al., 1999Yang and Sugisawa, 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101OV-101SE-30SE-30+Igepal
Column length (m) 50.50.50. 100.
Carrier gas N2N2N2Helium 
Substrate      
Column diameter (mm) 0.250.250.25 0.25
Phase thickness (mum)      
Tstart (C) 80.80.80.70.70.
Tend (C) 200.200.200.170.170.
Heat rate (K/min) 2.2.2.2.1.
Initial hold (min)      
Final hold (min)      
I 1040.1038.1040.1040.1051.
ReferenceYang and Sugisawa, 1990Sugisawa, Yang, et al., 1989Sugisawa, Yang, et al., 1989Alves and Jennings, 1979Shibamoto and Jennings, 1977
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase SE-30+Igepal
Column length (m) 100.
Carrier gas  
Substrate  
Column diameter (mm) 0.25
Phase thickness (mum)  
Tstart (C) 70.
Tend (C) 170.
Heat rate (K/min) 1.
Initial hold (min)  
Final hold (min)  
I 1055.
ReferenceShibamoto and Jennings, 1977
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Usman, Zubair, et al., 2010
Usman, L.A.; Zubair, M.F.; Adabayo, S.A.; Oladosu, I.A.; Muhammad, N.O.; Akolade, J.O., Chemical composition of leaf and fruit essential oils of Hoslundia opposita Vahl grown in Nigeria, Americal-Eurasian J. Agric. Environ. Sci., 2010, 8, 1, 40-43. [all data]

Gauvin-Bialecki and Marodon, 2009
Gauvin-Bialecki, A.; Marodon, C., Essential oil of Ayapana triplinervis from Reunion island: a good natural source of thymohydroquinone dimethyl ether, Biochem. Systematics Ecol., 2009, 36, 11, 853-858, https://doi.org/10.1016/j.bse.2008.09.006 . [all data]

Kim, El-Aty, et al., 2006
Kim, M.R.; El-Aty, A.M.A.; Choi, J.-H.; Lee, K.B.; Shim, J.H., Identification of volatile components in Angelica species using supercritical-CO2 fluid extraction and solid phase microextraction coupled to gas chromatography-mass spectrometry, Biomedical Chromatography, 2006, 20, 11, 1267-1273, https://doi.org/10.1002/bmc.696 . [all data]

Moody, Gundidza, et al., 2006
Moody, J.O.; Gundidza, M.; Wyllie, G., Essential oil composition of Leucas milanjiana Guerke, Flavour Fragr. J., 2006, 21, 6, 872-874, https://doi.org/10.1002/ffj.1669 . [all data]

Ozel, Gogus, et al., 2006
Ozel, M.Z.; Gogus, F.; Lewis, A.C., Comparison of direct thermal desorption with water distillation and superheated water extraction for the analysis of volatile components of Rosa damascena Mill. using GCxGC-TOF/MS, Anal. Chim. Acta., 2006, 566, 2, 172-177, https://doi.org/10.1016/j.aca.2006.03.014 . [all data]

Petrakis, Roussis, et al., 2005
Petrakis, P.V.; Roussis, V.; Papadimitriou, D.; Vagias, C.; Tsitsimpikou, C., The effect of terpenoid extracts from 15 pine species on the feeding behavioural sequence of the late instars of the pine processionary caterpillar Thaumetopoea pityocampa, Behav. Processes, 2005, 69, 3, 303-322, https://doi.org/10.1016/j.beproc.2004.12.008 . [all data]

Congiu, Falconieri, et al., 2002
Congiu, R.; Falconieri, D.; Marongiu, B.; Piras, A.; Porcedda, S., Extraction and isolation of Pistacia lentiscus L. essential oil by supercritical CO2, Flavour Fragr. J., 2002, 17, 4, 239-244, https://doi.org/10.1002/ffj.1095 . [all data]

Yang, 2001
Yang, R., Analysis of the volatile components in peel oil of Yuzu by gas chromatography/mass spectrometry, Chin. J. Anal. Chem., 2001, 29, 3, 313-316. [all data]

Yang, 2001, 2
Yang, R., Volatile compounds in peel oil of Citrus sudachi, Food Sci. (Beijing), 2001, 22, 3, 71-73. [all data]

Lis-Balchin and Roth, 2000
Lis-Balchin, M.; Roth, G., Composition of the essential oils of Pelargonium odoratissimum, P. exstipulatum, and P. x fragrans (Geraniaceae) and their bioactivity, Flavour Fragr. J., 2000, 15, 6, 391-394, https://doi.org/10.1002/1099-1026(200011/12)15:6<391::AID-FFJ929>3.0.CO;2-W . [all data]

Meccia, Rojas, et al., 2000
Meccia, G.; Rojas, L.B.; Rosquete, C.; Feliciano, A.S., Essential oil of Croton ovalifolius Vahl from Venezuela, Flavour Fragr. J., 2000, 15, 3, 144-146, https://doi.org/10.1002/1099-1026(200005/06)15:3<144::AID-FFJ882>3.0.CO;2-C . [all data]

Baraldi, Rapparini, et al., 1999
Baraldi, R.; Rapparini, F.; Rossi, F.; Latella, A.; Ciccioli, P., Volatile organic compound emissions from flowers of the most occurring and economically important species of fruit trees, Phys. Chem. Earth, 1999, 24, 6, 729-732, https://doi.org/10.1016/S1464-1909(99)00073-8 . [all data]

Sun and Petracek, 1999
Sun, D.; Petracek, P.D., Grapefruit gland oil composition is affected by wax application, storage temperature, and storage time, J. Agric. Food Chem., 1999, 47, 5, 2067-2069, https://doi.org/10.1021/jf981064k . [all data]

Viallon C., Verdier-Metz I., et al., 1999
Viallon C.; Verdier-Metz I.; Denoyer C.; Pradel P.; Coulon J.B.; Berdague J.L., Desorbed terpenes and sesquiterpenes from forages and cheeses, J. Dairy Res., 1999, 66, 2, 319-326, https://doi.org/10.1017/S0022029999003520 . [all data]

Yang and Sugisawa, 1990
Yang, R.; Sugisawa, H., Citrus Suachi Hort. ex Shirai. Volatile components in Sudachi (Citrus Sudachi Hort. ex Shirai) juice, Nippon Shokuhin Kogyo Gakkaishi, 1990, 37, 12, 946-952, https://doi.org/10.3136/nskkk1962.37.12_946 . [all data]

Sugisawa, Yang, et al., 1989
Sugisawa, H.; Yang, R.H.; Kawabata, C.; Tamura, H., Volatile constituents in the peel oil of sudachi (Citrus sudachi), Agric. Biol. Chem., 1989, 53, 6, 1721-1723, https://doi.org/10.1271/bbb1961.53.1721 . [all data]

Alves and Jennings, 1979
Alves, S.; Jennings, W.G., Volatile composition of certain Amazonian fruits, Food Chem., 1979, 4, 2, 149-159, https://doi.org/10.1016/0308-8146(79)90039-6 . [all data]

Shibamoto and Jennings, 1977
Shibamoto, T.; Jennings, W.G., The volatile composition of the leaf oil of California Juniper (J. californica Carr.) in Proceedings of VII International Congress of Essential Oils, October 7-11, 1977, Kyoto, Japan, 1977, 413-418. [all data]


Notes

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