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Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5SE-52BPX-5VF-5MSDB-5
Column length (m) 
Carrier gas HeHeHeHe 
Column diameter (mm) 0.250.320.250.25 
Phase thickness (mum) 
Program 40C(2min) => 4C/min => 220C => 20C/min => 280C45C => 1C/min => 100C => 5C/min => 250C(10min)35C => 4C/min => 200C => 30C/min => 300C (3min)40C(2min) => 5C/min => 200C (2min) => 30C/min => 260Cnot specified
I 1509.1508.1509.1469.1511.
ReferenceAndrade, Sampaio, et al., 2007Bruni, Bianchi, et al., 2007Dharmawan, Kasapis, et al., 2007Carasek and Pawliszyn, 2006Özel, Gögüs, et al., 2006
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-52DB-5MSSE-52DB-5MSCP Sil 8 CB
Column length (m)
Carrier gas HeHeH2HeHe
Column diameter (mm) 0.320.250.320.250.32
Phase thickness (mum)
Program 45C => 1C/min => 100C => 5C/min => 250C(10min)40 (5min) => 4C/min => 140C => 4C/min => 200C (20min)60C(8min) => 3C/min => 180C => 20C/min => 250C(10min)40C(5min) => 4C/min => 160C => 8C/min => 240C (15min)35C(2min) => 5C/min => 170C => 20C/min => 240C (10min)
I 1506.1506.1508.1510.1508.
ReferenceBruni, Pellati, et al., 2005Zheng, Kim, et al., 2005Frizzo, Lorenzo, et al., 2004Kim, Lee, et al., 2003Fuhrmann and Grosch, 2002
Column type CapillaryCapillaryCapillary
Active phase DB-5DB-1BPX-5
Column length (m) 30.60.50.
Carrier gas HeHeHe
Column diameter (mm)
Phase thickness (mum)
Program 50C (1min) => 5C/min => 100C => 10C/min => 250C (9min)-20C (5min) => 10C/min => 100C => 4C/min => 200C => 10C/min => 280C0C (5min) => 40C/min => 40C (2min) => 10C/min => 280C
I 1496.1487.1518.
ReferenceBeaulieu and Grimm, 2001Eri, Khoo, et al., 2000Elmore, Erbahadir, et al., 1997


Go To: Top, Van Den Dool and Kratz RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Andrade, Sampaio, et al., 2007
Andrade, M.S.; Sampaio, T.S.; Nogueira, P.C.L.; Ribeiro, A.S.; Bittrich, V.; Amaral, M.C.E., Volatile compounds of the leaves, flowers and fruits of Kielmeyera rugosa Choisy (Clusiaceae), Flavour Fragr. J., 2007, 22, 1, 49-52, https://doi.org/10.1002/ffj.1751 . [all data]

Bruni, Bianchi, et al., 2007
Bruni, R.; Bianchi, A.; Bellardi, M.G., Essential oil composition of Agastache anethiodora Britton (Lamiaceae) infected by cucumber mosaic virus (CMV), Flavour Fragr. J., 2007, 22, 1, 66-70, https://doi.org/10.1002/ffj.1760 . [all data]

Dharmawan, Kasapis, et al., 2007
Dharmawan, J.; Kasapis, S.; Curran, P.; Johnson, J.R., Characterization of volatile compounds in selected citrus fruits from Asia. Part I: freshly-squeezed juice, Flavour Fragr. J., 2007, 22, 3, 228-232, https://doi.org/10.1002/ffj.1790 . [all data]

Carasek and Pawliszyn, 2006
Carasek, E.; Pawliszyn, J., Screening of Tropical Fruit Volatile Compounds Using Solid-Phase Microextraction (SPME) Fibers and Internally Cooled SPME Fiber, J. Agric. Food Chem., 2006, 54, 23, 8688-8696, https://doi.org/10.1021/jf0613942 . [all data]

Özel, Gögüs, et al., 2006
Özel, M.Z.; Gögüs, F.; Lewis, A.C., Determination of Teucrium chamaedrys volatiles by using direct thermal desorption-comprehensive two-dimensional gas chromatography-time-of-flight mass spectrometry, J. Chromatogr. A, 2006, 1114, 1, 164-169, https://doi.org/10.1016/j.chroma.2006.02.036 . [all data]

Bruni, Pellati, et al., 2005
Bruni, R.; Pellati, F.; Grazia Bellardi, M.; Benvenuti, S.; Paltrinieri, S.; Bertaccini, A.; Bianchi, A., Herbal drug quality and phytochemical composition of Hypericum perforatum L. affected by ash yellows phytoplasma infection, J. Agric. Food Chem., 2005, 53, 4, 964-968, https://doi.org/10.1021/jf0487654 . [all data]

Zheng, Kim, et al., 2005
Zheng, C.H.; Kim, K.H.; Kim, T.H.; Lee, H.J., Analysis and characterization of aroma-active compounds of Schizandra chinensis (omija) leaves, J. Sci. Food Agric., 2005, 85, 1, 161-166, https://doi.org/10.1002/jsfa.1975 . [all data]

Frizzo, Lorenzo, et al., 2004
Frizzo, C.D.; Lorenzo, D.; Dellacassa, E., Composition and seasonal variation of the essential oils from two mandarin cultivars of Southern Brazil, J. Agric. Food Chem., 2004, 52, 10, 3036-3041, https://doi.org/10.1021/jf030685x . [all data]

Kim, Lee, et al., 2003
Kim, T.H.; Lee, S.M.; Kim, Y.-S.; Kim, K.H.; Oh, S.; Lee, H.J., Aroma dilution method using GC injector split ratio for volatile compounds extracted by headspace solid phase microextraction, Food Chem., 2003, 83, 1, 151-158, https://doi.org/10.1016/S0308-8146(03)00221-8 . [all data]

Fuhrmann and Grosch, 2002
Fuhrmann, E.; Grosch, W., Character impact odorants of the apple cultivars Elstar and Cox Orange, Nahrung/Food, 2002, 46, 3, 187-193, https://doi.org/10.1002/1521-3803(20020501)46:3<187::AID-FOOD187>3.0.CO;2-5 . [all data]

Beaulieu and Grimm, 2001
Beaulieu, J.C.; Grimm, C.C., Identification of volatile compounds in cantaloupe at various developmental stages using solid phase microextraction, J. Agric. Food Chem., 2001, 49, 3, 1345-1352, https://doi.org/10.1021/jf0005768 . [all data]

Eri, Khoo, et al., 2000
Eri, S.; Khoo, B.K.; Lech, J.; Hartman, T.G., Direct thermal desorption-gas chromatography and gas chromatography-mass spectrometry profiling of hop (Humulus lupulus L.) essential oils in support of varietal characterization, J. Agric. Food Chem., 2000, 48, 4, 1140-1149, https://doi.org/10.1021/jf9911850 . [all data]

Elmore, Erbahadir, et al., 1997
Elmore, J.S.; Erbahadir, M.A.; Mottram, D.S., Comparison of dynamic headspace concentration on Tenax with solid phase microextraction for the analysis of aroma volatiles, J. Agric. Food Chem., 1997, 45, 7, 2638-2641, https://doi.org/10.1021/jf960835m . [all data]


Go To: Top, Van Den Dool and Kratz RI, non-polar column, custom temperature program, References