α-Farnesene

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Normal alkane RI, non-polar column, custom temperature program

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Polydimethyl siloxane with 5 % Ph groupsPolydimethyl siloxane with 5 % Ph groupsOV-1HP-5 MS 
Column length (m)   30.30. 
Carrier gas   HeliumHelium 
Substrate      
Column diameter (mm)   0.250.25 
Phase thickness (μm)    0.25 
Program not specifiednot specified40 0C 2 0C/min -> 120 0C 10 0C/min -> 230 0C (15 min)60 0C (1 min) 10 0C -> 180 0C (1 min) 20 0C/min -> 280 0C (15 min)not specified
I 1508.1511.1491.1511.1511.
ReferenceRobinson, Adams, et al., 2012Robinson, Adams, et al., 2012Chen and Li, 2011Chu, Liu, et al., 2011Karimi, Farmany, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5CP-Sil 8 CBHP-5 MSOptima-5MS
Column length (m) 30.60.30.30.30.
Carrier gas NitrogenHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.251.000.250.250.25
Program 35 0C (10 min) 3 0C/min -> 205 0C 10 0C/min -> 225 0C40 0C 4 0C/min -> 230 0C 100 0C/min -> 260 0C (11.7 min)Multi-rise program60 0C (1 min) 10 0C/min -> 180 0C (1 min) 20 0C/min -> 280 0C (15 min)40 0C (5 min) 5 0C/min -> 230 0C 30 0C/min -> 280 0C (5 min)
I 1508.1518.1505.1512.1506.
ReferenceLaribi, Kouki, et al., 2011Miyazaki, Plotto, et al., 2011Di Giusto, Bessiere, et al., 2010Liu, Chu, et al., 2010HEuskin, Godin, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-1HP-5DB-5DB-5
Column length (m) 25.30.30.30.25.
Carrier gas HeliumHydrogen HeliumNitrogen
Substrate      
Column diameter (mm) 0.320.250.320.250.22
Phase thickness (μm) 0.170.25 0.250.25
Program 60 0C (5 min) 4 0C/min -> 220 0C 11 0C/min -> 280 0C45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min)not specified50 0C 95 min) 3 0C/min -> 100 0C 4 0C/min -> 160 0C 5 0C/min -> 220 0C (15 min)not specified
I 1509.1500.1508.1514.1500.
ReferenceMaggi, Bilek, et al., 2009Mendes, Trindade, et al., 2009Riahi, Pourbasheer, et al., 2009Yang, Yang, et al., 2009Chieng, Assim, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Sil 5 CbCB-1CB-1HP-5MSDB-1
Column length (m) 50.30.30.30.30.
Carrier gas NitrogenHeliumHeliumHeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 1.200.250.250.250.25
Program 40 0C 20 0C/min -> 85 0C 1 0C/min -> 145 0C 3 0C/min -> 250 0C (30 min)40 0C (2 min) 4 0C/min -> 180 0C 20 0C/min -> 220 0C (1 min)not specified40 0C (2 min) 3 0C/min -> 180 0C (2 min) 15 0C -> 280 0C45C => 3C/min => 175C => 15C/min => 300C (10min)
I 1489.1516.1498.1524.1500.
ReferenceCollin, Nizet, et al., 2008Kannaste, Vongvanich, et al., 2008Kannaste, Vongvanich, et al., 2008Ning, Zheng, et al., 2008Nogueira, Marcelo-Curto, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Sil 8CB-MSDB-1HP-1CBP-5HP-5MS
Column length (m) 30.30.50.30.30.
Carrier gas HeliumHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (μm) 0.250.10.330.250.25
Program 50 0C(3 min) 3 0C/min -> 100 0C 2.7 0C/min -> 140 0C 2.4 0C/min -> 180 0C 6 0C/min -> 260 0C35C => 4C/min => 180C => 10C/min => 250C40C(2min) => 2C/min => 200C => 15C/min => 250C (30min)60C(2min) => 3C/min => 240C => 10C/min => 300C40C => 3C/min => 100C => 5C/min => 230C(2min)
I 1506.1505.1493.1491.1494.
ReferenceProfitt, Schatz, et al., 2008Albuquerque, Vasconcelos Silva, et al., 2007Barra, Baldovini, et al., 2007Cheriti, Saad, et al., 2007Chokeprasert P., Charles A.L., et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-1LM-5LM-5LM-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.25   
Program 40C(10min) => 3C/min => 200C => 2C/min => 220C45C => 3C/min => 175C => 15C/min => 300C (10min)50 0C (10 min) 2 oC/min -> 75 0C 3 0C/min -> 150 0C 5 0C/min -> 200 0Cnot specifiednot specified
I 1513.1500.1514.1508.1522.
ReferenceCole, Haber, et al., 2007Ferreira, Meireles de Sousa, et al., 2007Janzanntti, Franco, et al., 2007Janzanntti, Franco, et al., 2007Janzanntti, Franco, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSCP Sil 8 CBCP Sil 8 CBHP-5 MSZB-5
Column length (m) 30.30.50.30.30.
Carrier gas HeHeHeHelium 
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 40C(3min) => 8C/min => 160C => 15C/min => 300C (10min)50C(3min) => 3C/min => 100C => 2.7C/min => 140C => 2.4C/min => 180C => 6C/min => 250C60 0C (2 min) 5 0C/min -> 160 0C 5 0C/min -> 250 0C (10 min)40 0C (10 min) 3 0C/min -> 200 0C 2 0C/min -> 220 0C60C => 3C/min => 240C 20C/min => 320C
I 1503.1503.1506.1510.1502.
ReferenceLiu, Song, et al., 2007Meekijjaroenroj, Bessière, et al., 2007Mockute, Bernotiene, et al., 2007Moriarity, Bansal, et al., 2007Piskorski R., Hanus R., et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-SilCP-SilCP-SilCP-SilHP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 50 0C (3 min) 3 0C/min -> 100 0C 2.7 0C/min -> 140 0C 2.4 0C/min -> 180 0C 6 0C/min -> 250 0C50 0C (3 min) 3 0C/min -> 100 0C 2.7 0C/min -> 140 0C 2.4 0C/min -> 180 0C 6 0C/min -> 250 0C50 0C (3 min) 3 0C/min -> 100 0C 2.7 0C/min -> 140 0C 2.4 0C/min -> 180 0C 6 0C/min -> 250 0C50 0C (3 min) 3 0C/min -> 100 0C 2.7 0C/min -> 140 0C 2.4 0C/min -> 180 0C 6 0C/min -> 250 0Cnot specified
I 1480.1499.1506.1506.1506.
ReferenceProffit, 2007Proffit, 2007Proffit, 2007Proffit, 2007Ristic, Krivokuca-Dokic, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5 MSHP-5 MSHP-5MSHP-5MS
Column length (m) 30.30. 30.30.
Carrier gas HeliumHelium HeHe
Substrate      
Column diameter (mm) 0.250.25 0.250.25
Phase thickness (μm)     0.25
Program 40 0C (10 min) 3 oC/min -> 200 0C 2 0C/min -> 220 0C40 0C (10 min) 3 oC/min -> 200 0C 2 0C/min -> 220 0Cnot specified40C(10min) => 3C/min => 200C => 2C/min => 220C40C(3min) => 6C/min => 160C => 10C/min => 300C (10min)
I 1511.1463.1511.1510.1510.
ReferenceSetzer, Stokes, et al., 2007Setzer, Stokes, et al., 2007Stokes, Cole, et al., 2007Takaku, Haber, et al., 2007Yu, Huang, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5 MSHP-5MSDB-5
Column length (m) 26.30.30.30.30.
Carrier gas HeHeliumHeliumHeHe
Substrate      
Column diameter (mm) 0.20.320.250.250.32
Phase thickness (μm) 0.250.250.250.250.25
Program 60C(5min) => 6C/min => 200C => 15C/min => 250C(5min)not specified40 0C (10 min) 3 0C/min -> 200 0C 2 0C/min -> 220 0C40C(5min) => 2C/min => 250C (15min) => 10C/min => 270C60C => 2C/min => 100C => 3C/min => 160C => 5C/min => 280C
I 1485.1508.1512.1505.1504.
ReferenceBaroni, Nores, et al., 2006Kucuk, Gulec, et al., 2006Schmidt, Noletto, et al., 2006Senatore, Apostolides Arnold, et al., 2006Srivastava, Mallavarapu, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-1HP-5CP-Sil5 CB MSCP Sil 8 CB
Column length (m) 30.30.50.50.50.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.250.250.20.320.32
Phase thickness (μm) 0.250.250.51.20.25
Program 50C => 8C/min => 200C => 10C/min => 270C (5min)45C => 3C/min => 175C => 15C/min => 300C (10min)40C(1min) => 5C/min => 210C => 20C/min => 250C(8min)36C(2min) => 20C/min => 85C => 1C/min => 145C => 3C/min => 250C(30min)60C(2min) => 5C/min => 160C(1min) => 10C/min => 250C (3min)
I 1456.1500.1485.1489.1508.
ReferenceDeng, Yao, et al., 2005Figueiredo, Sim-Sim, et al., 2005Himanen, Vuorinen, et al., 2005Iraqi, Vermeulen, et al., 2005Radudienë, Judpintienë, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-1DB-5CP Sil 8 CBCP Sil 8 CB
Column length (m) 30.30.30.50.50.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.320.250.250.320.32
Phase thickness (μm)  0.250.25 0.25
Program 65C(1min) => 1C/min => 75C (2min) => 0.5C/min => 81C(2min) => 3C/min => 180C(7min)45C => 3C/min => 175C => 15C/min => 300C (15min)60C(4min) => 6C/min => 240 => 10C/min => 280C50 0C (2 min) 3 0C/min -> 180 0C (1 min) 20 0C/min -> 250 0C (2 min)50C(2min) => 3C/min => 180C(1min) => 20C/min => 250C (2min)
I 1510.1508.1506.1508.1508.
ReferenceSingh, Maurya, et al., 2005Touafek, Nacer, et al., 2005Letchamo, Ward, et al., 2004Mockutë, Bernotienë, et al., 2004Mockutë, Judbentienë, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30CP-Sil 8CB-MSSE-54CP Sil 8 CBDB-5
Column length (m)  50.  30.
Carrier gas  He  He
Substrate      
Column diameter (mm)  0.32  0.25
Phase thickness (μm)     0.1
Program not specified50C(2min) => 3C/min => 180C(1min) => 20C/min => 250C(2min)not specifiednot specified35C => 4C/min => 180C => 20C/min => 280C
I 1492.1509.1472.1508.1508.
ReferenceVinogradov, 2004Mockute, Bernotiene, et al., 2003Kilic, 2002Schwob, Bessière, et al., 2002Viana, Andrade-Neto, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CBP-1DB-5CP Sil 5 CBDB-1OV-1
Column length (m) 25. 25.30.50.
Carrier gas Nitrogen HeHeHe
Substrate      
Column diameter (mm) 0.25 0.390.250.32
Phase thickness (μm) 0.25  0.250.25
Program not specifiednot specifiednot specified45C => 3C/min => 175C => 15C/min => 240C (10min)1)50C(1min) => 4C/min => 180C => 2C/min => 250C(10min) 2)50C(1min) => 6C/min => 200C => 12C/min => 250C(5min)
I 1501.1514.1494.1500.1495.
ReferenceLy, Yamauchi, et al., 2001Dittmann and Nitz, 2000Weyerstahl, Marschall, et al., 1999Baratta, Dorman, et al., 1998Kökdil, 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5Methyl SiliconeDB-5DB-1DB-1
Column length (m) 30. 30.60.60.
Carrier gas He  He 
Substrate      
Column diameter (mm) 0.25 0.250.320.32
Phase thickness (μm) 0.25 0.250.25 
Program 60C => 3C/min => 240C => 30C/min => 300Cnot specified35C(1min) => 5C/min => 230C => 20C/min => 280Cnot specifiednot specified
I 1503.1492.1538.1487.1495.
ReferenceYusuf, Begum, et al., 1998Zenkevich, 1996Jelen H.H., Mirocha C.J., et al., 1995Nishimura, 1995Binder and Flath, 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase DB-1DB-1DB-1
Column length (m) 60.60.60.
Carrier gas HeHeHe
Substrate    
Column diameter (mm) 0.320.320.32
Phase thickness (μm) 0.250.250.25
Program -80 C (20 min; during thermal desorption) 50-200 C at 4 C/min 200-320 C at 10 C/min-80 C (20 min; during thermal desorption) 50-200 C at 4 C/min 200-320 C at 10 C/min-80 C (20 min; during thermal desorption) 50-200 C at 4 C/min 200-320 C at 10 C/min
I 1495.1498.1490.
ReferenceMiller, Bills, et al., 1989Miller, Bills, et al., 1989Miller, Bills, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Robinson, Adams, et al., 2012
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Chen and Li, 2011
Chen, S.; Li, X., Analysis of common volatile constituents between herbal pair Ephedra Sinica Stapf-Zingiber offoconale Rosc. and its single herb by GC-MS combined with AMWFA method, 2011, retrieved from http://www.webmedcentral.com. [all data]

Chu, Liu, et al., 2011
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Karimi, Farmany, et al., 2011
Karimi, H.; Farmany, A.; Noorizadeh, H., Prediction of linear retention index of Teucrium chamaedrys volatiles in GCxGC-TOF/MS by linear model, World Appl. Sci. J., 2011, 15, 8, 1086-1088. [all data]

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Liu, Chu, et al., 2010
Liu, Z.L.; Chu, S.S.; Liu, Q.R., Chemical composition and insecticidial activity against Sitophilus zeamais of the essential oils of Artemisia capillaris and Artemisia mongolica, Molecules, 2010, 15, 4, 2600-2608, https://doi.org/10.3390/molecules15042600 . [all data]

HEuskin, Godin, et al., 2009
HEuskin, S.; Godin, B.; Leroy, P.; Quentin C.; Wathelet, J.-P.; Verheggen, F.; Haubruge, E.; Lognay, G., Fast gas chromatography characterization of purified semiochemicals from essential oils of Matricaria chamomilla L. (Asteraceae) and Nepeta cataria L. (Lamiaceae), J. Chromatorg. A., 2009, 1216, 14, 2768-2775, https://doi.org/10.1016/j.chroma.2008.09.109 . [all data]

Maggi, Bilek, et al., 2009
Maggi, F.; Bilek, T.; Lucarini, D.; Papa, F.; Sagratini, G.; Vittori, S., Melittis melissophyllum L. subsp. melissophylum (Lamiaceae) from central Italy: A new source of a mushrrom-like flavour, Food Chem., 2009, 113, 1, 216-221, https://doi.org/10.1016/j.foodchem.2008.07.066 . [all data]

Mendes, Trindade, et al., 2009
Mendes, M.D.; Trindade, H.; Figueiredo, A.C.; Pedro, L.G.; Barroso, J.G., Chaerophyllum azoricun Trel. grown in the Azores archipelago, Portugal: evaluation of the genetic diversity using molecular markers and comparison with volatile oils profiles, Flavour Fragr. J., 2009, 24, 5, 259-265, https://doi.org/10.1002/ffj.1939 . [all data]

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Profitt, Schatz, et al., 2008
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Cole, Haber, et al., 2007
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Ferreira, Meireles de Sousa, et al., 2007
Ferreira, N.J.; Meireles de Sousa, I.G.; Luís, T.C.; Currais, A.J.M.; Figueiredo, C.; Cost, M.M.; Lima, A.S.B.; Santos, P.A.G.; Barroso, J.G.; Pedro, L.G.; Scheffer, J.J.C., Pittosporum undulatum Vent. grown in Portugal: secretory structures, seasonal variation and enantiomeric composition of its essential oil, Flavour Fragr. J., 2007, 22, 1, 1-9, https://doi.org/10.1002/ffj.1748 . [all data]

Janzanntti, Franco, et al., 2007
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Notes

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