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2-Cyclohexen-1-one, 4-(1-methylethyl)-

Normal alkane RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1RTX-15 % Phenyl polydimethyl siloxaneOV-1HP-5 MS
Column length (m) 60.60. 30.30.
Carrier gas HeliumHelium HeliumHelium
Column diameter (mm) 0.220.22 0.250.25
Phase thickness (mum) 0.250.25  0.25
Program not specifiednot specifiednot specified40 0C 2 0C/min -> 120 0C 10 0C/min -> 230 0C (15 min)60 0C (1 min) 10 0C -> 180 0C (1 min) 20 0C/min -> 280 0C (15 min)
I 1159.1159.1187.1146.1186.
ReferenceBendiabdellah, El Amine Dib, et al., 2012Bendiabdellah, El Amine Dib, et al., 2012Chaverri, Diaz, et al., 2011Chen and Li, 2011Chu, Liu, et al., 2011
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1DB-1Elite-5 MSHP-5MSHP-5MS
Column length (m)
Carrier gas HeliumHeliumHeliumHeHe
Column diameter (mm)
Phase thickness (mum) 
Program not specified50 0C (5 min) 3 0C/min -> 120 0C 5 0C/min -> 250 0C (3 min) 15 0C/min -> 300 0C (20 min)60 0C (1 min) 1.5 0C/min -> 185 0C (1 min) 9 0C/min -> 275 0C (2 min)40 0C (2 min) 3 0C/min -> 180 0C (2 min) 15 0C -> 280 0C40C(10min) => 3C/min => 200C => 2C/min => 220C
I 1158.1167.1178.1180.1189.
ReferenceDib, Djabou, et al., 2010Delort and Jaquier, 2009Kapoor, Singh, et al., 2009Ning, Zheng, et al., 2008Takaku, Haber, et al., 2007
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BPX-5HP-5SE-52CP Sil 8 CBDB-5
Column length (m)
Carrier gas He HeHeHe
Column diameter (mm)
Phase thickness (mum)
Program 50C => 3C/min => 150C(10min) => 10C/min => 250C>2.5C/min => 180C => 100C/min => 250C (7.3min)45C => 1C/min => 100C => 5C/min => 250C (10min)60C(1min) => 5C/min => 160C => 5C/min => 250C(3min)35C => 4C/min => 180C => 10C/min => 250C
I 1181.1200.1186.1186.1173.
ReferenceBaris, Güllüce, et al., 2006Goodner, Mahattanatawee, et al., 2006Tognolini, Barocelli, et al., 2006Nivinskienë, Butkienë, et al., 2005Albuquerque, Souza, et al., 2004
Column type CapillaryCapillaryCapillary
Active phase DB-1HP-5MSCP Sil 5 CB
Column length (m) 30.30.25.
Carrier gas He  
Column diameter (mm) 0.250.320.39
Phase thickness (mum) 0.250.24 
Program 45C => 3C/min => 175C => 15C/min => 300C (15min)not specifiednot specified
I 1148.1172.1159.
ReferenceTouafek, Nacer, et al., 2004Stashenko, Jaramillo, et al., 2002Weyerstahl, Marschall, et al., 1999


Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Bendiabdellah, El Amine Dib, et al., 2012
Bendiabdellah, A.; El Amine Dib, M.; Djabou, N.; Allali, H.; Tabti, B.; Costa, J.; Myseli, A., Biological activities and volatile cinstituents of Daucus muricatus L. from Algeria, Chem. Centr. J., 2012, 6, 48, 1-22. [all data]

Chaverri, Diaz, et al., 2011
Chaverri, C.; Diaz, C.; Cicco, J.F., Chemical analysis of essential oils from Ocotea gomezii W.C. Burger and Ocotea morae Gomez-Laur. (Lauraceae) collected at Reserva biologica Alberto M. Brenes in Costa Rica and their cytotoxic activity on Tumor cell lines, J. Braz. Chem. Soc., 2011, 22, 4, s1-s4, https://doi.org/10.1590/S0103-50532011000400018 . [all data]

Chen and Li, 2011
Chen, S.; Li, X., Analysis of common volatile constituents between herbal pair Ephedra Sinica Stapf-Zingiber offoconale Rosc. and its single herb by GC-MS combined with AMWFA method, 2011, retrieved from http://www.webmedcentral.com. [all data]

Chu, Liu, et al., 2011
Chu, S.S.; Liu, S.L.; Liu, Q.Z.; Liu, Z.L.; Du, S.S., Composition and toxicity of Chinese Dracocephalum moldavica (Labiatae) essential oil against two grain storage insects, J. Med. Plants Res., 2011, 5, 21, 5262-5267. [all data]

Dib, Djabou, et al., 2010
Dib, M.ElA.; Djabou, N.; Desjobert, L.-M.; Allali, H.; Tabti, B.; Muselli, A.; Costa, J., Characterization of volatile compounds of Daucus crinitus Desf. headspace solid phase microextraction as alternative technique to hydrodistillation, Chem, Centr. J., 2010, 4, 16, 1-15. [all data]

Delort and Jaquier, 2009
Delort, E.; Jaquier, A., Novel terpenyl esters from Australian finger lime (Citrus australasica) peel extract, Flav. Fragr. J., 2009, 24, 3, 123-132, https://doi.org/10.1002/ffj.1922 . [all data]

Kapoor, Singh, et al., 2009
Kapoor, I.; Singh, B.; Singh, G.; De Heluani, C.S.; De Lampasona, M.P.; Catalan, C.A.N., Chemistry and in vitro antioxidant activity of volatile oil and oleoresins of black pepper (Piper nigrum), J. Agric. Food Chem., 2009, 57, 12, 5358-5364, https://doi.org/10.1021/jf900642x . [all data]

Ning, Zheng, et al., 2008
Ning, H.; Zheng, F.; Sun, B.; Xie, J.; Liu, Y., Solvent-free microwave extraction of essential oil from Zanthoxylum bungeanum Maxim., Food Environ. Ind. (Chinese), 2008, 34, 5, 179-184. [all data]

Takaku, Haber, et al., 2007
Takaku, S.; Haber, W.A.; Setzer, W.N., Leaf essential oil composition of 10 species of Ocotea (Lauraceae) from Monteverde, Costa Rica, Biochem. Syst. Ecol., 2007, 35, 8, 525-532, https://doi.org/10.1016/j.bse.2007.02.003 . [all data]

Baris, Güllüce, et al., 2006
Baris, Ö.; Güllüce, M.; Sahin, F.; Özer, H.; Kilic, H.; Özkan, H.; Sökmen, M.; Özbek, T., Biological Activities of the Essential Oil and Methanol Extract of Achillea biebersteinii Afan. (Asteraceae), Turk. J. Biol., 2006, 30, 65-73. [all data]

Goodner, Mahattanatawee, et al., 2006
Goodner, K.L.; Mahattanatawee, K.; Plotto, A.; Sotomayor, J.A.; Jordan, M.J., Aromatic profiles of Thymus hyemalis and Spanish T. vulgaris essential oils by GC-MS/GC-O, Ind. Crops Prod., 2006, 24, 3, 264-268, https://doi.org/10.1016/j.indcrop.2006.06.006 . [all data]

Tognolini, Barocelli, et al., 2006
Tognolini, M.; Barocelli, E.; Ballabeni, V.; Bruni, R.; Bianchi, A.; Chiavarini, M.; Impicciatore, M., Comparative screening of plant essential oils: Phenylpropanoid moiety as basic core for antiplatelet activity, Life Sciences, 2006, 78, 13, 1419-1432, https://doi.org/10.1016/j.lfs.2005.07.020 . [all data]

Nivinskienë, Butkienë, et al., 2005
Nivinskienë, O.; Butkienë, R.; Mockutë, D., Chemical composition of seed (fruit) essential oils of Angelica archangelica L. growing wild in Lithuania, Chemija, 2005, 16, 3-4, 51-54. [all data]

Albuquerque, Souza, et al., 2004
Albuquerque, M.R.J.R.; Souza, E.B.; Lins, M.U.D.S.; Nogueira, N.A.P.; Lemos, T.L.G.; Silveira, E.R.; Pessoa, O.D.L., Composition and antimicrobial activity of the essential oil from aerial parts of Baccharis trinervis (Lam.) Pers., Arkivoc, 2004, 6, 6, 59-65, https://doi.org/10.3998/ark.5550190.0005.608 . [all data]

Touafek, Nacer, et al., 2004
Touafek, O.; Nacer, A.; Kabouce, A.; Kabouche, Z.; Bruneau, C., Chemical composition of the essential oil of Rosmarinus officinalis cultivated in the Algerian sahara, Chem. Nat. Compd. (Engl. Transl.), 2004, 40, 1, 28-29, https://doi.org/10.1023/B:CONC.0000025460.78222.69 . [all data]

Stashenko, Jaramillo, et al., 2002
Stashenko, E.E.; Jaramillo, B.E.; Martínez, J.R., HRGC/FID/MSD Analysis of Secondary Metabolites Isolated from Xilopia aromatica by Different Extraction Techniques in 25th International Symposium on Capillary Chromatography, 2002, 1-5. [all data]

Weyerstahl, Marschall, et al., 1999
Weyerstahl, P.; Marschall, H.; Splittgerber, U.; Son, P.T.; Giang, P.M.; Kaul, V.K., Constituents of the essential oil from the fruits of Zanthoxylum rhetsoides Drake from Vietnam and from the aerial parts of Zanthoxylum alatum Roxb. from India, Flavour Fragr. J., 1999, 14, 4, 225-229, https://doi.org/10.1002/(SICI)1099-1026(199907/08)14:4<225::AID-FFJ818>3.0.CO;2-1 . [all data]


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