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Hygrine


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-11060.Jenett-Siems, Weigl, et al., 2005He, 6. K/min; Column length: 30. m; Column diameter: 0.32 mm; Tstart: 70. C; Tend: 300. C

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-5MS1093.Humam, Munoz, et al., 200730. m/0.25 mm/0.25 «mu»m, 70. C @ 1. min, 5. K/min, 285. C @ 15. min

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-5MS1320.1Andriamaharavo, 201430. m/0.25 mm/0.25 «mu»m, He; Program: 60C (1 min) => 5 C/min => 210C => 10 C/min => 280C (15 min)
CapillaryHP-5MS1091.Humam, Munoz, et al., 200730. m/0.25 mm/0.25 «mu»m; Program: not specified

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-11060.Tofern, Kaloga, et al., 1999He, 6. K/min; Column length: 30. m; Column diameter: 0.32 mm; Tstart: 70. C; Tend: 300. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryOV-11060.Ei-Shazly and Wink M., 200815. m/0.317 mm/0.25 «mu»m, He; Program: 100 0C (2 min) 15 0C/min -> 250 0C 25 0C/min -> 300 0C (5 min)

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Jenett-Siems, Weigl, et al., 2005
Jenett-Siems, K.; Weigl, R.; Böhm, A.; Mann, P.; Tofern-Reblin, B.; Ott, S.C.; Ghomian, A.; Kaloga, M.; Siems, K.; Witte, L.; Hilker, M.; Müller, F.; Eich, E., Chemotaxonomy of the pantropical genus Merremia (Convolvulaceae) based on the distribution of tropane alkaloids, Phytochemistry, 2005, 66, 12, 1448-1464, https://doi.org/10.1016/j.phytochem.2005.04.027 . [all data]

Humam, Munoz, et al., 2007
Humam, M.; Munoz, O.; Christen, P.; Hostettmann, K., Tropane alkaloids of the aerial part of Schizanthus tricolor, Nat. Prod. Commun., 2007, 2, 7, 743-747. [all data]

Andriamaharavo, 2014
Andriamaharavo, N.R., Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2014. [all data]

Tofern, Kaloga, et al., 1999
Tofern, B.; Kaloga, M.; Witte, L.; Hartmann, T.; Eich, E., Occurrence of loline alkaloids in Argyreia mollis (Convolvulaceae), Phytochemistry, 1999, 51, 8, 1177-1180, https://doi.org/10.1016/S0031-9422(99)00121-1 . [all data]

Ei-Shazly and Wink M., 2008
Ei-Shazly, A.; Wink M., Tropane and pyrrolidine alkaloids from Convolvulus lanatus Vahl, Z. Naturforsch. C:, 2008, 63, 5-6, 321-325. [all data]


Notes

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