1,3-Cyclohexadiene, 5-(1,5-dimethyl-4-hexenyl)-2-methyl-, [S-(R*,S*)]-

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Kovats' RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1BP-1BP-1CP Sil 5 CBSPB-1
Column length (m) 30.25.30.25.30.
Carrier gas HeN2N2H2He
Substrate      
Column diameter (mm) 0.250.320.320.250.32
Phase thickness (μm) 0.250.250.250.150.25
Tstart (C) 50.60.60.50.60.
Tend (C) 280.220.220.230.225.
Heat rate (K/min) 5.5.5.3.2.
Initial hold (min) 3.   3.
Final hold (min)  13.3. 5.
I 1493.1491.1484.1486.1463.
ReferenceAllegrone, Belliardo, et al., 2006Raina, Verma, et al., 2006Srivastava, Srivastava, et al., 2006Ogunwande, Olawore, et al., 2003Jayaprakasha, Jena, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1DB-1BP-5HP-5MSDB-5
Column length (m) 25.50.25.30.30.
Carrier gas N2N2HeHeHe
Substrate      
Column diameter (mm) 0.550.250.250.320.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.80.60.70.60.
Tend (C) 220.225.200.250.240.
Heat rate (K/min) 5.4.3.3.3.
Initial hold (min)    5. 
Final hold (min) 15.    
I 1487.1473.1496.1487.1500.
ReferenceRaina, Srivastava, et al., 2002Palá-Paúl, Velasco-Negueruela, et al., 2001Weissbecker B., Van Loon J.J.A., et al., 2000Siani, Ramos, et al., 1999da Silva, Andrade, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedCapillary
Active phase OV-1Methyl Silicone
Column length (m) 1.8312.
Carrier gas   
Substrate   
Column diameter (mm)  0.5
Phase thickness (μm)   
Tstart (C) 90.70.
Tend (C) 200.250.
Heat rate (K/min) 15.4.
Initial hold (min)   
Final hold (min)  15.
I 1454.1471.8
ReferenceCarter, Gianfagna, et al., 1989Rao, Rajanikanth, et al., 1989
Comment MSDC-RI MSDC-RI

References

Go To: Top, Kovats' RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Allegrone, Belliardo, et al., 2006
Allegrone, G.; Belliardo, F.; Cabella, P., Comparison of volatile concentrations in hand-squeezed juices of four different lemon varieties, J. Agric. Food Chem., 2006, 54, 5, 1844-1848, https://doi.org/10.1021/jf051206s . [all data]

Raina, Verma, et al., 2006
Raina, V.K.; Verma, S.C.; Dhawan, S.; Khan, M.; Ramesh, S.; Singh, S.C.; Yadav, A.; Srivastava, S.K., Essential oil composition of Murraya exotica from the plains of northern India, Flavour Fragr. J., 2006, 21, 1, 140-142, https://doi.org/10.1002/ffj.1547 . [all data]

Srivastava, Srivastava, et al., 2006
Srivastava, A.K.; Srivastava, S.K.; Syamsundar, K.V., Volatile composition of Curcuma angustifolia Roxb. rhizome from central and southern India, Flavour Fragr. J., 2006, 21, 3, 423-426, https://doi.org/10.1002/ffj.1680 . [all data]

Ogunwande, Olawore, et al., 2003
Ogunwande, I.A.; Olawore, N.O.; Kasali, A.A.; König, W.A., Chemical composition of the leaf volatile oils of Callitris intratropica R.T. Baker H.G. Smith from Nigeria, Flavour Fragr. J., 2003, 18, 5, 387-389, https://doi.org/10.1002/ffj.1214 . [all data]

Jayaprakasha, Jena, et al., 2002
Jayaprakasha, G.K.; Jena, B.S.; Negi, P.S.; Sakariah, K.K., Evaluation of antioxidant activities and antimutagenicity of turmeric oil: a byproduct from curcumin production, Z. Naturforsch. C:, 2002, 57c, 828-835, retrieved from http://www.znaturforsch.com/57c/s57c0828.pdf. [all data]

Raina, Srivastava, et al., 2002
Raina, V.K.; Srivastava, S.K.; Jain, N.; Ahmad, A.; Syamasundar, K.V.; Aggarwal, K.K., Essential oil composition of Curcuma longa L. cv. Roma from the plains of northern India, Flavour Fragr. J., 2002, 17, 2, 99-102, https://doi.org/10.1002/ffj.1053 . [all data]

Palá-Paúl, Velasco-Negueruela, et al., 2001
Palá-Paúl, J.; Velasco-Negueruela, A.; Pérez-Alonso, M.J.; Sanz, J., Analysis of the volatile components of Argyranthemum adauctum (Link.) Humphries by gas chromatography-mass spectrometry, J. Chromatogr. A, 2001, 923, 1-2, 295-298, https://doi.org/10.1016/S0021-9673(01)01003-2 . [all data]

Weissbecker B., Van Loon J.J.A., et al., 2000
Weissbecker B.; Van Loon J.J.A.; Posthumus M.A.; Bouwmeester H.J.; Dicke M., Identification of volatile potato sesquiterpenoids and their olfactory detection by the two-spotted stinkbug Perillus bioculatus, J. Chem. Ecol., 2000, 26, 6, 1433-1445, https://doi.org/10.1023/A:1005535708866 . [all data]

Siani, Ramos, et al., 1999
Siani, A.C.; Ramos, M.F.S.; Menezes-de-Lima, O., Jr.; Ribeiro-dos-Santos, R.; Fernadez-Ferreira, E.; Soares, R.O.A.; Rosas, E.C.; Susunaga, G.S.; Guimarães, A.C.; Zoghbi, M.G.B.; Henriques, M.G.M.O., Evaluation of anti-inflammatory-related activity of essential oils from the leaves and resin of species of Protium, J. Ethnopharmacol., 1999, 66, 1, 57-69, https://doi.org/10.1016/S0378-8741(98)00148-2 . [all data]

da Silva, Andrade, et al., 1999
da Silva, M.H.L.; Andrade, E.H.A.; Zoghbi, M.G.B.; Luz, A.I.R.; da Silva, J.D.; Maia, J.G.S., The essential oils of Lantana camara L. occurring in North Brazil, Flavour Fragr. J., 1999, 14, 4, 208-210, https://doi.org/10.1002/(SICI)1099-1026(199907/08)14:4<208::AID-FFJ811>3.0.CO;2-F . [all data]

Carter, Gianfagna, et al., 1989
Carter, C.D.; Gianfagna, T.J.; Sacalis, J.N., Sesquiterpenes in glandular trichomes of a wild tomato species and toxicity to the Colorado potato beetle, J. Agric. Food Chem., 1989, 37, 5, 1425-1428, https://doi.org/10.1021/jf00089a048 . [all data]

Rao, Rajanikanth, et al., 1989
Rao, A.S.; Rajanikanth, B.; Seshadri, R., Volatile aroma components of Curcuma amada Roxb., J. Agric. Food Chem., 1989, 37, 3, 740-743, https://doi.org/10.1021/jf00087a036 . [all data]


Notes

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