1,3-Cyclohexadiene, 5-(1,5-dimethyl-4-hexenyl)-2-methyl-, [S-(R*,S*)]-
- Formula: C15H24
- Molecular weight: 204.3511
- IUPAC Standard InChI: InChI=1S/C15H24/c1-12(2)6-5-7-14(4)15-10-8-13(3)9-11-15/h6,8-10,14-15H,5,7,11H2,1-4H3
- IUPAC Standard InChIKey: KKOXKGNSUHTUBV-UHFFFAOYSA-N
- CAS Registry Number: 495-60-3
- Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript. - Stereoisomers:
- Other names: (-)-Zingiberene; l-Zingiberene; Zingiberene; α-Zingiberene; 5-(1,5-Dimethyl-4-hexenyl)-2-methyl-1,3-cyclohexadiene; α-zingibirene; [S-(R*,S*)]-5-(1,5-dimethylhexen-4-yl)-2-methyl-1,3-cyclohexa-1,3-diene
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Kovats' RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-1 | 1493. | Allegrone, Belliardo, et al., 2006 | 30. m/0.25 mm/0.25 μm, He, 50. C @ 3. min, 5. K/min; Tend: 280. C |
| Capillary | BP-1 | 1491. | Raina, Verma, et al., 2006 | 25. m/0.32 mm/0.25 μm, N2, 5. K/min, 220. C @ 13. min; Tstart: 60. C |
| Capillary | BP-1 | 1484. | Srivastava, Srivastava, et al., 2006 | 30. m/0.32 mm/0.25 μm, N2, 5. K/min, 220. C @ 3. min; Tstart: 60. C |
| Capillary | CP Sil 5 CB | 1486. | Ogunwande, Olawore, et al., 2003 | 25. m/0.25 mm/0.15 μm, H2, 3. K/min; Tstart: 50. C; Tend: 230. C |
| Capillary | SPB-1 | 1463. | Jayaprakasha, Jena, et al., 2002 | 30. m/0.32 mm/0.25 μm, He, 60. C @ 3. min, 2. K/min, 225. C @ 5. min |
| Capillary | BP-1 | 1487. | Raina, Srivastava, et al., 2002 | 25. m/0.55 mm/0.25 μm, N2, 5. K/min, 220. C @ 15. min; Tstart: 60. C |
| Capillary | DB-1 | 1473. | Palá-Paúl, Velasco-Negueruela, et al., 2001 | 50. m/0.25 mm/0.25 μm, N2, 4. K/min; Tstart: 80. C; Tend: 225. C |
| Capillary | BP-5 | 1496. | Weissbecker B., Van Loon J.J.A., et al., 2000 | 25. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 200. C |
| Capillary | HP-5MS | 1487. | Siani, Ramos, et al., 1999 | 30. m/0.32 mm/0.25 μm, He, 70. C @ 5. min, 3. K/min; Tend: 250. C |
| Capillary | DB-5 | 1500. | da Silva, Andrade, et al., 1999 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C |
| Packed | OV-1 | 1454. | Carter, Gianfagna, et al., 1989 | 15. K/min; Column length: 1.83 m; Tstart: 90. C; Tend: 200. C |
| Capillary | Methyl Silicone | 1471.8 | Rao, Rajanikanth, et al., 1989 | 4. K/min, 250. C @ 15. min; Column length: 12. m; Column diameter: 0.5 mm; Tstart: 70. C |
Kovats' RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | BP-1 | 1490. | Khan, Srivastava, et al., 2003 | 25. m/0.25 mm/0.25 μm, N2; Program: 60C => 5C/min => 220C (5min) => 3C/min => 245 C (5min) |
| Capillary | BP-1 | 1490. | Khan, Srivastava, et al., 2002 | 30. m/0.32 mm/0.25 μm, N2; Program: 60 C 5 C/min -> 220 C (5 min) 3 C/min -> 245 C (5 min) |
Kovats' RI, polar column, isothermal
| Column type | Active phase | Temperature (C) | I | Reference | Comment |
|---|---|---|---|---|---|
| Packed | Carbowax 20M | 165. | 1738. | Andersen and Falcone, 1969 |
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | HP-5MS | 1493. | Benkaci-Ali, Baaliouamer, et al., 2007 | 30. m/0.25 mm/0.25 μm, He, 60. C @ 8. min, 2. K/min, 250. C @ 30. min |
| Capillary | DB-5 | 1495. | Maccioni, Baldini, et al., 2007 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C |
| Capillary | DB-5 | 1495. | Maccioni, Baldini, et al., 2007 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C |
| Capillary | DB-5 | 1495. | Rout, Rao, et al., 2007 | 25. m/0.25 mm/0.25 μm, He, 2. K/min, 200. C @ 60. min; Tstart: 60. C |
| Capillary | DB-5 | 1500. | Sabulal, Dan, et al., 2007 | 30. m/0.25 mm/0.25 μm, He, 5. K/min; Tstart: 60. C; Tend: 260. C |
| Capillary | DB-1 | 1492. | Sonboli, Azizian, et al., 2007 | 60. m/0.25 mm/0.25 μm, N2, 5. K/min, 250. C @ 10. min; Tstart: 60. C |
| Capillary | HP-5MS | 1495. | Pino, Mesa, et al., 2005 | 30. m/0.25 mm/0.25 μm, He, 60. C @ 2. min, 4. K/min, 250. C @ 20. min |
| Capillary | HP-5MS | 1495. | Grujic-Jovanovic, Skaltsa, et al., 2004 | 30. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 4. K/min; Tend: 280. C |
| Capillary | HP-5 | 1495. | Sartoratto, Machado, et al., 2004 | 25. m/0.2 mm/0.33 μm, He, 3. K/min, 240. C @ 7. min; Tstart: 60. C |
| Capillary | HP-5MS | 1476. | Tzakou, Vagias, et al., 2004 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C |
| Capillary | DB-5 | 1494. | bin Jantan, Yassin, et al., 2003 | 30. m/0.25 mm/0.25 μm, N2, 75. C @ 10. min, 3. K/min; Tend: 230. C |
| Capillary | MS5 | 1492. | Shao, Marriott, et al., 2003 | 25. m/0.25 mm/0.25 μm, 3. K/min; Tstart: 40. C; Tend: 180. C |
| Capillary | BPX-5 | 1499. | Shellie, Marriott, et al., 2003 | 30. m/0.25 mm/0.25 μm, He, 60. C @ 2. min, 3. K/min; Tend: 240. C |
| Capillary | HP-5 | 1495. | Skaltsa, Demetzos, et al., 2003 | 30. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 4. K/min; Tend: 280. C |
| Capillary | HP-5 | 1494. | Fokialakis, Magiatis, et al., 2002 | 30. m/0.25 mm/0.25 μm, 60. C @ 5. min, 3. K/min; Tend: 280. C |
| Capillary | HP-5 | 1493. | Aligiannis, Kalpoutzakis, et al., 2001 | 30. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 3. K/min; Tend: 280. C |
| Capillary | DB-5 | 1496. | Bortolomeazzi, Berno, et al., 2001 | 30. m/0.25 mm/0.25 μm, He, 60. C @ 3. min, 5. K/min; Tend: 300. C |
| Capillary | DB-5 | 1490. | Bartley and Jacobs, 2000 | 60. m/0.25 mm/0.25 μm, He, 40. C @ 2. min, 4. K/min, 290. C @ 5. min |
| Capillary | DB-5 | 1496. | Bortolomeazzi, Pizzale, et al., 2000 | 30. m/0.25 mm/0.25 μm, He, 60. C @ 3. min, 5. K/min; Tend: 300. C |
| Capillary | CP Sil 8 CB | 1497. | Chevance and Farmer, 1999 | 60. C @ 5. min, 4. K/min, 220. C @ 30. min; Column length: 50. m; Column diameter: 0.32 mm |
| Capillary | Ultra-1 | 1489. | Richmond and Pombo-Villar, 1998 | 25. m/0.32 mm/0.52 μm, He, 15. K/min, 320. C @ 10. min; Tstart: 35. C |
| Capillary | Ultra-1 | 1489.28 | Richmond and Pombo-Villar, 1997 | 25. m/0.32 mm/0.52 μm, 15. K/min, 320. C @ 10. min; Tstart: 35. C |
| Capillary | DB-1 | 1490. | Bartley and Foley, 1994 | 60. m/0.32 mm/0.5 μm, 40. C @ 2. min, 4. K/min, 290. C @ 5. min |
Van Den Dool and Kratz RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | BPX-5 | 1505. | Cardeal, da Silva, et al., 2006 | 30. m/0.25 mm/0.25 μm; Program: 35C(5min) => 3C/min => 210C => 40C/min => 240C (4min) |
| Capillary | 5 % Phenyl methyl siloxane | 1494. | Sacchetti, Maietti, et al., 2005 | 30. m/0.32 mm/0.15 μm, He; Program: 45C => 1C/min => 100C => 5C/min => 250C (10min) |
Van Den Dool and Kratz RI, polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | HP-Innowax | 1713. | Grujic-Jovanovic, Skaltsa, et al., 2004 | 30. m/0.25 mm/0.5 μm, He, 3. K/min; Tstart: 60. C; Tend: 260. C |
| Capillary | CP-Wax 52CB | 1745. | Kjeldsen, Christensen, et al., 2003 | 50. m/0.25 mm/0.2 μm, He, 32. C @ 1. min, 1. K/min; Tend: 220. C |
| Capillary | CP-Wax 52CB | 1745. | Kjeldsen, Christensen, et al., 2001 | 50. m/0.25 mm/0.2 μm, 32. C @ 1. min, 1. K/min; Tend: 220. C |
| Capillary | DB-Wax | 1728. | Bartley and Jacobs, 2000 | 60. m/0.5 mm/0.32 μm, He, 40. C @ 2. min, 4. K/min, 290. C @ 5. min |
| Capillary | CP-Wax 52CB | 1702. | Chevance and Farmer, 1999 | 60. C @ 5. min, 4. K/min, 220. C @ 30. min; Column length: 50. m; Column diameter: 0.32 mm |
| Capillary | CP-Wax 52CB | 1713. | Chevance and Farmer, 1999, 2 | 60. C @ 5. min, 4. K/min, 220. C @ 30. min; Column length: 50. m; Column diameter: 0.32 mm |
| Capillary | CP-Wax 52CB | 1710. | Chevance and Farmer, 1999, 2 | 40. C @ 5. min, 4. K/min, 220. C @ 30. min; Column length: 50. m; Column diameter: 0.32 mm |
| Capillary | DB-Wax | 1722. | Cha, Kim, et al., 1998 | 60. m/0.25 mm/0.25 μm, 40. C @ 5. min, 3. K/min, 200. C @ 60. min |
| Capillary | DB-Wax | 1715. | Möllenbeck, König, et al., 1997 | 25. m/0.25 mm/0.25 μm, He, 50. C @ 3. min, 4. K/min; Tend: 240. C |
| Capillary | CP-Wax 52CB | 1743. | Chyau, Mau, et al., 1996 | 50. m/0.23 mm/0.12 μm, H2, 50. C @ 10. min, 1.5 K/min, 200. C @ 10. min |
| Capillary | CP-Wax 52CB | 1683. | Wu and Yang, 1994 | H2, 50. C @ 10. min, 1.5 K/min, 200. C @ 40. min; Column length: 50. m; Column diameter: 0.32 mm |
| Capillary | Carbowax 20M | 1701. | Chen and Ho, 1988 | He, 1.5 K/min, 225. C @ 80. min; Column length: 60. m; Column diameter: 0.32 mm; Tstart: 50. C |
| Capillary | Carbowax 20M | 1696. | Chen and Ho, 1988 | He, 1.5 K/min, 225. C @ 80. min; Column length: 60. m; Column diameter: 0.32 mm; Tstart: 50. C |
| Capillary | Carbowax 20M | 1696. | Chen and Ho, 1988 | He, 1.5 K/min, 225. C @ 80. min; Column length: 60. m; Column diameter: 0.32 mm; Tstart: 50. C |
Van Den Dool and Kratz RI, polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | Carbowax 20M | 1721. | Bortolomeazzi, Berno, et al., 2001 | 30. m/0.25 mm/0.25 μm, He; Program: 60C(3min) => 4C/min => 160C => 10C/min => 280C |
| Capillary | Carbowax 20M | 1721. | Bortolomeazzi, Pizzale, et al., 2000 | 30. m/0.25 mm/0.25 μm, He; Program: 60C(3min) => 4C/min => 160C => 10C/min => 280C |
Normal alkane RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | Polydimethyl siloxane with 5 % Ph | 1490. | Priya, Prathapan, et al., 2012 | Helium, 5. K/min, 200. C @ 25. min; Column length: 30. m; Tstart: 80. C |
| Capillary | HP-5 | 1495. | Kahriman, Tosun, et al., 2011 | 30. m/0.32 mm/0.25 μm, Helium, 60. C @ 2. min, 3. K/min; Tend: 240. C |
| Capillary | HP-5 MS | 1497. | Miyazawa, Marumoto, et al., 2011 | 30. m/0.25 mm/0.25 μm, Helium, 4. K/min, 260. C @ 5. min; Tstart: 40. C |
| Capillary | HP-5 | 1503. | Cavar, Maksimovic, et al., 2010 | 30. m/0.252 mm/0.25 μm, Helium, 3. K/min; Tstart: 60. C; Tend: 240. C |
| Capillary | RTX-1 | 1489. | Dib, Djabou, et al., 2010 | 60. m/0.22 mm/0.25 μm, Helium, 2. K/min, 230. C @ 30. min; Tstart: 60. C |
| Capillary | HP-5 MS | 1500. | Lazarevic, Radulovic, et al., 2010 | 30. m/0.25 mm/0.25 μm, Helium, 5. K/min; Tstart: 70. C; Tend: 290. C |
| Capillary | DB-1 | 1489. | Mirjalili, Salehi, et al., 2010 | 25. m/0.25 mm/0.25 μm, Nitrogen, 60. C @ 1. min, 4. K/min, 250. C @ 10. min |
| Capillary | HP-5 | 1499. | Miyazawa, Kawauchi, et al., 2010 | 30. m/0.25 mm/0.25 μm, Helium, 4. K/min, 260. C @ 5. min; Tstart: 40. C |
| Capillary | HP-5 MS | 1497. | Radulovic, Blagojevic, et al., 2010 | 30. m/0.25 mm/0.25 μm, Helium, 5. K/min, 290. C @ 10. min; Tstart: 70. C |
| Capillary | HP-5 | 1502. | Radulovic, Dordevic, et al., 2010 | 30. m/0.25 mm/0.25 μm, Hydrogen, 5. K/min; Tstart: 70. C; Tend: 290. C |
| Capillary | OV-101 | 1494. | Benites, Moiteiro, et al., 2009 | 50. m/0.25 mm/0.25 μm, Helium, 2. K/min; Tstart: 70. C; Tend: 220. C |
| Capillary | OV-101 | 1500. | Benites, Moiteiro, et al., 2009 | 50. m/0.25 mm/0.25 μm, Helium, 2. K/min; Tstart: 70. C; Tend: 220. C |
| Capillary | ZB-5 | 1447. | Gardini, Beletti, et al., 2009 | 30. m/0.25 mm/0.25 μm, Helium, 3. K/min, 240. C @ 1. min; Tstart: 50. C |
| Capillary | HP-5 | 1506. | Maridass, 2009 | 25. m/0.20 mm/0.33 μm, Helium, 3. K/min, 240. C @ 7. min; Tstart: 60. C |
| Capillary | RTX-1 | 1489. | Museli, Pau, et al., 2009 | 60. m/0.22 mm/0.25 μm, Helium, 2. K/min, 230. C @ 30. min; Tstart: 60. C |
| Capillary | RTX-1 | 1489. | Museli, Pau, et al., 2009 | 60. m/0.22 mm/0.25 μm, Helium, 2. K/min, 230. C @ 30. min; Tstart: 60. C |
| Capillary | RTX-1 | 1488. | Paolini, Tomi, et al., 2008 | 60. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C |
| Capillary | HP-5 | 1495. | Yassa and Akhani, 2008 | 30. m/0.25 mm/0.32 μm, Helium, 60. C @ 30. min, 5. K/min; Tend: 250. C |
| Capillary | HP-5MS | 1508. | Argyropoulou, Daferera, et al., 2007 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C |
| Capillary | Col-Elite 5MS | 1504. | Gudaityte and Venskutonis R.P., 2007 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 30. C; Tend: 246. C |
| Capillary | AT-5 | 1500. | Meccia, Rojas, et al., 2007 | 60. m/0.25 mm/0.25 μm, Helium, 4. K/min; Tstart: 60. C; Tend: 260. C |
| Capillary | DB-5 | 1489. | Miyazawa and Tamura, 2007 | 30. m/0.25 mm/0.25 μm, He, 2. K/min; Tstart: 60. C; Tend: 240. C |
| Capillary | DB-5 | 1490. | Pontes, de Olivera, et al., 2007 | 30. m/0.25 mm/0.25 μm, Hydrogen, 4. K/min; Tstart: 50. C; Tend: 250. C |
| Capillary | SPB-5 | 1490. | Raal, Orav, et al., 2007 | 30. m/0.25 mm/0.25 μm, He, 2. K/min; Tstart: 50. C; Tend: 250. C |
| Capillary | HP-5 | 1495. | Yassa and Akhani, 2007 | 30. m/0.25 mm/0.32 μm, He, 60. C @ 30. min, 5. K/min; Tend: 250. C |
| Capillary | DB-5 | 1497. | Bazargani, Almasirad, et al., 2006 | 30. m/0.25 mm/0.25 μm, He, 50. C @ 1. min, 2.5 K/min, 265. C @ 20. min |
| Capillary | DB-5 | 1500. | Garneau F.X., Collin G., et al., 2006 | 30. m/0.25 mm/0.25 μm, 40. C @ 2. min, 2. K/min, 210. C @ 33. min |
| Capillary | HP-5 | 1494. | Ibañez and Usubillaga, 2006 | 30. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 60. C; Tend: 240. C |
| Capillary | HP-5MS | 1492. | Ibanez and Usubillaga, 2006 | 30. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 60. C; Tend: 260. C |
| Capillary | RTX-1 | 1488. | Kula, Izydorczyk, et al., 2006 | 30. m/0.32 mm/0.25 μm, He, 4. K/min; Tstart: 60. C; Tend: 300. C |
| Capillary | DB-5MS | 1484. | Maronigiu, Piras, et al., 2006 | 30. m/0.25 mm/0.25 μm, He, 3. K/min, 280. C @ 30. min; Tstart: 60. C |
| Capillary | DB-1 | 1501. | Pala-Paul J., Perez-Alonso M.J., et al., 2006 | 50. m/0.25 mm/0.25 μm, N2, 4. K/min; Tstart: 95. C; Tend: 240. C |
| Capillary | DB-5 | 1497. | Rout, Naik, et al., 2006 | 30. m/0.25 mm/0.25 μm, He, 2. K/min, 200. C @ 60. min; Tstart: 60. C |
| Capillary | DB-5 | 1513. | Shen X., Gao Y., et al., 2006 | 30. m/0.25 mm/0.25 μm, He, 40. C @ 2. min, 4. K/min, 250. C @ 10. min |
| Capillary | DB-1 | 1469. | Velasco-Negueruela, Pérez-Alonso, et al., 2006 | 50. m/0.25 mm/0.25 μm, N2, 4. K/min; Tstart: 90. C; Tend: 240. C |
| Capillary | BPX-5 | 1521. | Wohlmuth, Smith, et al., 2006 | 50. m/0.22 mm/1. μm, 4. K/min, 280. C @ 4. min; Tstart: 70. C |
| Capillary | CP Sil 5 CB | 1486. | Olawore, Ogunwande, et al., 2005 | 25. m/0.25 mm/0.15 μm, 3. K/min; Tstart: 50. C; Tend: 230. C |
| Capillary | HP-5MS | 1492. | Sajjadi, 2005 | 30. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 60. C; Tend: 280. C |
| Capillary | HP-5 | 1485. | Utsunomia, Kawata, et al., 2005 | 30. m/0.32 mm/0.25 μm, Helium, 4. K/min, 300. C @ 5. min; Tstart: 40. C |
| Capillary | DB-1 | 1469. | Velasco-Negueruela, Pérez-Alonso, et al., 2005 | 50. m/0.25 mm/0.25 μm, N2, 4. K/min; Tstart: 90. C; Tend: 240. C |
| Capillary | SPB-1 | 1494. | Wong, Lee, et al., 2005 | 50. m/0.2 mm/0.33 μm, He, 50. C @ 3. min, 4. K/min, 220. C @ 30. min |
| Capillary | DB-5 | 1489. | Limberger, Sobral, et al., 2004 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 300. C |
| Capillary | NB-30 | 1488. | Orav, Stulova, et al., 2004 | 50. m/0.2 mm/0.25 μm, He, 2. K/min; Tstart: 50. C; Tend: 250. C |
| Capillary | NB-30 | 1488. | Orav, Stulova, et al., 2004 | 50. m/0.2 mm/0.25 μm, He, 2. K/min; Tstart: 50. C; Tend: 250. C |
| Capillary | DB-5 | 1496. | Senatore, Rigano, et al., 2004 | 30. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 2. K/min, 250. C @ 20. min |
| Capillary | HP-5MS | 1493. | Afsharypuor and Jahromy, 2003 | 30. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 60. C; Tend: 275. C |
| Capillary | DB-1 | 1483. | Dabiri and Sefidkon, 2003 | He, 4. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tstart: 50. C; Tend: 250. C |
| Capillary | DB-5MS | 1496. | Maia, Taveira, et al., 2003 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C |
| Capillary | HP-5 | 1494. | Stashenko, Jaramillo, et al., 2003 | 60. m/0.25 mm/0.25 μm, 40. C @ 15. min, 5. K/min; Tend: 250. C |
| Capillary | Cross-Linked Methylsilicone | 1469. | Velasco-Negueruela, Pérez-Alonso, et al., 2003 | 25. m/0.2 mm/0.33 μm, He, 4. K/min; Tstart: 70. C; Tend: 250. C |
| Capillary | RSL-200 | 1494. | Jirovetz, Buchbauer, et al., 2002 | 30. m/0.32 mm/0.25 μm, H2, 40. C @ 5. min, 6. K/min, 280. C @ 5. min |
| Capillary | DB-5MS | 1497. | Maia, Zoghbi, et al., 2002 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C |
| Capillary | CP Sil 5 CB | 1477. | Mojab, Rustaiyan, et al., 2002 | 25. m/0.25 mm/0.39 μm, He, 5. K/min; Tstart: 60. C; Tend: 220. C |
| Capillary | DB-1 | 1473. | Palá-Paúl, Pérez-Alonso, et al., 2002 | 50. m/0.25 mm/0.25 μm, N2, 4. K/min; Tstart: 80. C; Tend: 225. C |
| Capillary | DB-1 | 1469. | Velasco-Negueruela, Pérez-Alonso, et al., 2002 | 50. m/0.25 mm/0.25 μm, N2, 4. K/min; Tstart: 95. C; Tend: 240. C |
| Capillary | SPB-5 | 1495. | Cornu, Carnat, et al., 2001 | He, 40. C @ 5. min, 3. K/min, 220. C @ 15. min; Column length: 60. m; Column diameter: 0.32 mm |
| Capillary | CBP-1 | 1489. | Ly, Yamauchi, et al., 2001 | 25. m/0.25 mm/0.25 μm, Nitrogen, 50. C @ 2. min, 3. K/min; Tend: 210. C |
| Capillary | SPB-5 | 1499. | Doneanu and Anitescu, 1998 | 50. m/0.32 mm/0.25 μm, He, 3. K/min, 240. C @ 20. min; Tstart: 60. C |
| Capillary | OV-101 | 1494. | Zollo, Biyiti, et al., 1998 | 5. K/min; Column length: 25. m; Column diameter: 0.32 mm; Tstart: 50. C; Tend: 200. C |
| Capillary | CP Sil 8 CB | 1493. | Jantan and Goh, 1990 | 60. C @ 10. min, 3. K/min; Column length: 25. m; Column diameter: 0.20 mm; Tend: 230. C |
| Capillary | SE-30 | 1486. | Ramaswami, Briscese, et al., 1988 | 50. C @ 2. min, 4. K/min, 240. C @ 10. min; Column length: 30. m |
| Capillary | SE-30 | 1486. | Ramaswami, Briscese, et al., 1986 | 50. C @ 2. min, 4. K/min, 240. C @ 10. min; Column length: 30. m |
Normal alkane RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | VF-5 | 1515. | Shivashankar, Roy, et al., 2012 | 30. m/0.25 mm/0.25 μm, Helium; Program: 50 0C (2 min) 3 0C/min -> 200 0C (3 min) 10 0C/min -> 220 0C (8 min) |
| Capillary | VF-5 | 1500. | Shivashankar, Roy, et al., 2012 | 30. m/0.25 mm/0.25 μm, Helium; Program: not specified |
| Capillary | HP-5 | 1489. | Citron, Riclea, et al., 2011 | Program: not specified |
| Capillary | HP-5 | 1496. | Citron, Riclea, et al., 2011 | Program: not specified |
| Capillary | HP-5 | 1494. | Kahriman, Tosun, et al., 2011 | 30. m/0.32 mm/0.25 μm, Helium; Program: not specified |
| Capillary | HP-5 MS | 1495. | Payo, Colo, et al., 2011 | Program: not specified |
| Capillary | HP-5 MS | 1496. | Payo, Colo, et al., 2011 | Program: not specified |
| Capillary | RTX-1 | 1483. | Dib, Djabou, et al., 2010 | 60. m/0.22 mm/0.25 μm, Helium; Program: not specified |
| Capillary | HP-5 MS | 1492. | Liu, Chu, et al., 2010 | 30. m/0.25 mm/0.25 μm, Helium; Program: 60 0C (1 min) 10 0C/min -> 180 0C (1 min) 20 0C/min -> 280 0C (15 min) |
| Capillary | HP-5 | 1492. | Custer, 2009 | 25. m/0.32 mm/0.17 μm, Helium; Program: 60 0C (5 min) 4 0C/min -> 220 0C 11 0C/min -> 280 0C (15 min) |
| Capillary | HP-5 | 1494. | Custer, 2009 | 25. m/0.32 mm/0.17 μm, Helium; Program: 60 0C (5 min) 4 0C/min -> 220 0C 11 0C/min -> 280 0C (15 min) |
| Capillary | HP-5 | 1493. | Custer, 2009 | 25. m/0.32 mm/0.17 μm, Helium; Program: not specified |
| Capillary | HP-5 | 1493. | Custer, 2009 | 25. m/0.32 mm/0.17 μm, Helium; Program: not specified |
| Capillary | DB-1 | 1492. | Mendes, Trindade, et al., 2009 | 30. m/0.25 mm/0.25 μm, Hydrogen; Program: 45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min) |
| Capillary | DB-1 | 1492. | Mendes, Trindade, et al., 2009, 2 | 30. m/0.25 mm/0.25 μm, Hydrogen; Program: 45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min) |
| Capillary | DB-5 | 1507. | Yang, Yang, et al., 2009 | 30. m/0.25 mm/0.25 μm, Helium; Program: 50 0C 95 min) 3 0C/min -> 100 0C 4 0C/min -> 160 0C 5 0C/min -> 220 0C (15 min) |
| Capillary | DB-1 | 1494. | Albuquerque, Vasconcelos Silva, et al., 2007 | 30. m/0.25 mm/0.1 μm, He; Program: 35C => 4C/min => 180C => 10C/min => 250C |
| Capillary | HP-5MS | 1486. | Chokeprasert P., Charles A.L., et al., 2007 | 30. m/0.25 mm/0.25 μm, He; Program: 40C => 3C/min => 100C => 5C/min => 230C(2min) |
| Capillary | HP-5MS | 1509. | Cole, Haber, et al., 2007 | 30. m/0.25 mm/0.25 μm, He; Program: 40C(10min) => 3C/min => 200C => 2C/min => 220C |
| Capillary | HP-5MS | 1494. | Liu, Song, et al., 2007 | 30. m/0.25 mm/0.25 μm, He; Program: 40C(3min) => 8C/min => 160C => 15C/min => 300C (10min) |
| Capillary | CP Sil 8 CB | 1494. | Mockute, Bernotiene, et al., 2007 | 50. m/0.32 mm/0.25 μm, He; Program: 60 0C (2 min) 5 0C/min -> 160 0C 5 0C/min -> 250 0C (10 min) |
| Capillary | DB-5 | 1495. | Pontes, de Olivera, et al., 2007 | 30. m/0.25 mm/0.25 μm, Hydrogen; Program: not specified |
| Capillary | HP-5 MS | 1498. | Stokes, Cole, et al., 2007 | Program: not specified |
| Capillary | HP-5MS | 1498. | Yu, Huang, et al., 2007 | 30. m/0.25 mm/0.25 μm, He; Program: 40C(3min) => 6C/min => 160C => 10C/min => 300C (10min) |
| Capillary | HP-5MS | 1488. | Li, Deng, et al., 2006 | 30. m/0.25 mm/0.25 μm, He; Program: 40C(1min) => 8C/min => 160C => 12C/min => 300C(5min) |
| Capillary | HP-5 MS | 1498. | Schmidt, Noletto, et al., 2006 | 30. m/0.25 mm/0.25 μm, Helium; Program: 40 0C (10 min) 3 0C/min -> 200 0C 2 0C/min -> 220 0C |
| Capillary | HP-5MS | 1495. | Singh G., Maurya S., et al., 2006 | 30. m/0.32 mm/0.25 μm, He; Program: 60C(1min) => 1.5C => 185C => 9C/min => 275C (2min) |
| Capillary | SE-52 | 1494. | Tognolini, Barocelli, et al., 2006 | 30. m/0.32 mm/0.15 μm, He; Program: 45C => 1C/min => 100C => 5C/min => 250C (10min) |
| Capillary | DB-1 | 1473. | Al-Burtamani, Fatope, et al., 2005 | 30. m/0.25 mm/0.25 μm, He; Program: 35C => 2C/min => 200C => 5C/min => 240C |
| Capillary | DB-1 | 1492. | Belhattab, Larous, et al., 2005 | 30. m/0.25 mm/0.25 μm, He; Program: 45C => 3C/min => 175C => 15C/min => 300C(10min) |
| Capillary | CP Sil 8 CB | 1495. | Nivinskienë, Butkienë, et al., 2005 | 50. m/0.32 mm/0.25 μm, He; Program: 60C(1min) => 5C/min => 160C => 5C/min => 250C(3min) |
| Capillary | HP-5 | 1495. | Singh, Maurya, et al., 2005 | Column length: 30. m; Column diameter: 0.32 mm; Program: 65C(1min) => 1C/min => 75C (2min) => 0.5C/min => 81C(2min) => 3C/min => 180C(7min) |
| Capillary | SE-30 | 1487. | Vinogradov, 2004 | Program: not specified |
| Capillary | SE-30 | 1520. | Vinogradov, 2004 | Program: not specified |
| Capillary | SE-30 | 1501. | Li, Wu, et al., 2002 | He; Column length: 60. m; Column diameter: 0.25 mm; Program: 50 0C (5 min) 5 0C/min -> 165 0C 4 0C/min -> 230 0C |
| Capillary | SE-30 | 1502. | Li, Wu, et al., 2002 | He; Column length: 60. m; Column diameter: 0.25 mm; Program: not specified |
| Capillary | HP-5 | 1494. | Aparicio, Romero, et al., 2001 | 30. m/0.25 mm/0.25 μm; Program: not specified |
| Capillary | DB-1 | 1492. | Pedro, da Silva, et al., 1999 | 30. m/0.25 mm/0.25 μm, He; Program: 45C => 3C/min => 170C => 15C/min => 300C(10min) |
| Capillary | CP Sil 5 CB | 1487. | Weyerstahl, Marschall, et al., 1999 | 25. m/0.25 mm/0.39 μm, N2; Program: not specified |
| Capillary | DB-1 | 1492. | Figueiredo, Barroso, et al., 1997 | 30. m/0.25 mm/0.25 μm, H2; Program: 45C => 3C/min => 175C => 15C/min => 240C(10min) |
| Capillary | CP Sil 5 CB | 1488. | Weyerstahl, Marschall, et al., 1997 | He; Column length: 25. m; Program: not specified |
| Capillary | DB-1 | 1492. | Barroso, Figueiredo, et al., 1996 | 30. m/0.25 mm/0.25 μm, H2; Program: 45 0C 3 0C/min -> 175 0C 15 0C/min -> 240 0C (10 min) |
| Capillary | Methyl Silicone | 1487. | Zenkevich, 1996 | Program: not specified |
| Capillary | DB-5 | 1490. | Storer, Elmore, et al., 1993 | 30. m/0.32 mm/1. μm; Program: 0C(5min) => 60C/min => 60C (5min) => 4C/min => 250C (5min) |
Normal alkane RI, polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | RTX-Wax | 1717. | Dib, Djabou, et al., 2010 | 60. m/0.22 mm/0.25 μm, Helium, 2. K/min, 230. C @ 30. min; Tstart: 60. C |
| Capillary | DB-Wax | 1736. | Miyazawa, Kawauchi, et al., 2010 | 15. m/0.25 mm/0.25 μm, Helium, 4. K/min, 260. C @ 5. min; Tstart: 40. C |
| Capillary | Supelcowax-10 | 1724. | Benites, Moiteiro, et al., 2009 | 30. m/0.25 mm/0.25 μm, Helium, 2. K/min; Tstart: 70. C; Tend: 220. C |
| Capillary | Supelcowax-10 | 1726. | Benites, Moiteiro, et al., 2009 | 30. m/0.25 mm/0.25 μm, Helium, 2. K/min; Tstart: 70. C; Tend: 220. C |
| Capillary | DB-Wax | 1715. | Karlsson, Birgersson, et al., 2009 | 30. m/0.25 mm/0.25 μm, Hydrogen, 30. C @ 5. min, 8. K/min, 230. C @ 10. min |
| Capillary | RTX-Wax | 1698. | Museli, Pau, et al., 2009 | 60. m/0.22 mm/0.25 μm, Helium, 2. K/min, 230. C @ 30. min; Tstart: 60. C |
| Capillary | RTX-Wax | 1714. | Paolini, Tomi, et al., 2008 | 60. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C |
| Capillary | TC-Wax | 1718. | Miyazawa and Tamura, 2007 | 60. m/0.25 mm/0.25 μm, He, 2. K/min; Tstart: 60. C; Tend: 240. C |
| Capillary | Supelcowax-10 | 1726. | Raal, Orav, et al., 2007 | 30. m/0.25 mm/0.25 μm, He, 2. K/min; Tstart: 50. C; Tend: 250. C |
| Capillary | Supelcowax-10 | 1728. | Garneau F.X., Collin G., et al., 2006 | 30. m/0.25 mm/0.25 μm, 40. C @ 2. min, 2. K/min, 210. C @ 33. min |
| Capillary | CP-Wax | 1708. | Ka, Choi, et al., 2005 | 30. m/0.32 mm/0.25 μm, He, 40. C @ 2. min, 5. K/min; Tend: 180. C |
| Capillary | Supelcowax-10 | 1706. | Wong, Lee, et al., 2005 | 30. m/0.25 mm/0.25 μm, He, 50. C @ 3. min, 4. K/min, 220. C @ 30. min |
| Capillary | HP-20M | 1687. | Mastelic and Jerkovic, 2003 | 50. m/0.2 mm/0.2 μm, He, 70. C @ 4. min, 4. K/min, 180. C @ 10. min |
| Capillary | CP-Wax 52CB | 1715. | Mau, Lai, et al., 2003 | 60. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 40. C; Tend: 220. C |
| Capillary | HP-Innowax | 1726. | Stashenko, Jaramillo, et al., 2003 | 50. m/0.2 mm/0.2 μm, 50. C @ 5. min, 4. K/min; Tend: 220. C |
| Capillary | DB-Wax | 1718. | Umano, Hagi, et al., 2000 | 60. m/0.25 mm/0.25 μm, He, 40. C @ 2. min, 2. K/min; Tend: 200. C |
| Capillary | DB-Wax | 1724. | Ngassoum, Yonkeu, et al., 1999 | 60. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 60. C; Tend: 240. C |
| Capillary | DB-Wax | 1728. | van Beek, Kleis, et al., 1989 | 60. m/0.25 mm/0.25 μm, H2, 4. K/min, 238. C @ 13. min; Tstart: 50. C |
| Capillary | Supelcowax-10 | 1728. | Ramaswami, Briscese, et al., 1988 | 50. C @ 2. min, 4. K/min, 240. C @ 10. min; Column length: 30. m |
| Capillary | Supelcowax-10 | 1728. | Ramaswami, Briscese, et al., 1986 | He, 50. C @ 2. min, 4. K/min, 240. C @ 10. min; Column length: 30. m |
Normal alkane RI, polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | HP-Innowax | 1681. | Sun, Hua, et al., 2010 | 30. m/0.32 mm/0.50 μm, Helium; Program: 50 0C (5 min) 3 0C/min -> 210 0C (10 min) 3 0C/min -> 230 0C |
| Capillary | Supelcowax-10 | 1735. | Vichi, Guadayol, et al., 2007 | 30. m/0.25 mm/0.25 μm, He; Program: 40C(3min) => 4C/min => 75C => 8C/min => 250C(5min) |
| Capillary | HP-Innowax FSC | 1726. | Kürkçüoglu, Hüsnü Can Baser, et al., 2006 | 60. m/0.25 mm/0.25 μm, He; Program: 60C(10min) => 4C/min => 220C (10min) => 1C/min => 240C |
| Capillary | HP-Innowax FSC | 1726. | Suleimenov Y.M., Atazhanova G.A., et al., 2006 | 60. m/0.25 mm/0.25 μm, He; Program: 60(10min) => 4C/min => 220C(10min) => 1C/min => 240C |
| Capillary | HP-Innowax FSC | 1725. | Tabanca, Demirci, et al., 2006 | 60. m/0.25 mm/0.25 μm; Program: 60C(10min) => 4C/min => 220C (10min) => 1C/min => 240C |
| Capillary | Supelcowax-10 | 1732. | Vichi, Guadayol, et al., 2006 | 30. m/0.25 mm/0.25 μm, He; Program: 40C(3min) => 4C/min => 75C => 8C/min => 260C(5min) |
| Capillary | HP-Innowax | 1726. | Duman, Kartal, et al., 2005 | 60. m/0.25 mm/0.25 μm, N2; Program: 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C |
| Capillary | HP-Innowax FSC | 1725. | Tabanca, Demirci, et al., 2005 | 60. m/0.25 mm/0.25 μm, He; Program: 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C |
| Capillary | Carbowax 20M | 1733. | Vinogradov, 2004 | Program: not specified |
| Capillary | Carbowax 20M | 1738. | Vinogradov, 2004 | Program: not specified |
| Capillary | Innowax FSC | 1726. | Baser, Demirei, et al., 2002 | 60. m/0.25 mm/0.25 μm, He; Program: 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C |
| Capillary | Innowax FSC | 1726. | Kirimer, Tabanca, et al., 2000 | 60. m/0.25 mm/0.25 μm, He; Program: 60C(10 min) => 4C/min => 220C(10min) => 1C/min => 240C |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
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Notes
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