Guaiol

Mass spectrum (electron ionization)

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Spectrum

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Additional Data

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Owner NIST Mass Spectrometry Data Center
Collection (C) 2014 copyright by the U.S. Secretary of Commerce
on behalf of the United States of America. All rights reserved.
Origin Chemical Concepts
NIST MS number 185098

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Gas Chromatography

Go To: Top, Mass spectrum (electron ionization), References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-51597.Lucero, Fredrickson, et al., 200630. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C
CapillaryDB-51595.Shatar S., 20053. K/min; Tstart: 60. C; Tend: 240. C
CapillaryHP-5MS1602.Siani, Garrido, et al., 200430. m/0.32 mm/0.25 μm, He, 70. C @ 5. min, 3. K/min; Tend: 250. C
CapillaryDB-51588.El-Massry, El-Ghorab, et al., 200230. m/0.25 mm/0.5 μm, 50. C @ 3. min, 7. K/min, 250. C @ 10. min
CapillaryBP-11605.Raina, Srivastava, et al., 200225. m/0.32 mm/0.25 μm, N2, 5. K/min, 220. C @ 15. min; Tstart: 60. C
CapillaryDB-51600.Moreira, Sousa, et al., 2001H2, 3. K/min; Column length: 30. m; Column diameter: 0.20 mm; Tstart: 60. C; Tend: 240. C
CapillaryDB-11589.Palá-Paúl, Velasco-Negueruela, et al., 200150. m/0.25 mm/0.25 μm, N2, 4. K/min; Tstart: 80. C; Tend: 225. C
CapillaryDB-11576.Senatore and Rigano, 200130. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 2. K/min, 260. C @ 20. min
CapillaryDB-51602.da Silva, Andrade, et al., 199930. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-51591.de Feo, Porta, et al., 199830. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 2. K/min, 250. C @ 20. min
CapillaryDB-51591.Senatore, Urrunaga Soria, et al., 199830. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 2. K/min, 250. C @ 20. min
CapillarySE-301588.Jantan, Ali, et al., 1995N2, 60. C @ 10. min, 3. K/min, 180. C @ 1. min; Column length: 25. m; Column diameter: 0.2 mm
CapillaryHP-11578.Raharivelomanana, Cambon, et al., 19936. K/min, 240. C @ 10. min; Column length: 15. m; Column diameter: 0.32 mm; Tstart: 40. C
CapillaryBP-11600.Ekundayo, Laakso, et al., 1988H2, 65. C @ 2. min, 5. K/min; Column length: 50. m; Column diameter: 0.33 mm; Tend: 220. C

Kovats' RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-5MS1614.Tuberoso, Kowalczyk, et al., 200530. m/0.25 mm/0.25 μm, He; Program: 60C(5min) => 2C/min => 140C= 5C/min => 250C(5min)
CapillaryHP-51600.Frizzo, Serafini, et al., 200130. m/0.32 mm/0.25 μm, H2; Program: 60 0C (8 min) 3 K/min -> 180 0C 20 K/min (20 min)
CapillaryDB-51595.Moreira, Sousa, et al., 2001H2; Column length: 30. m; Column diameter: 0.20 mm; Program: not specified

Kovats' RI, polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-Innowax2105.Frizzo, Serafini, et al., 200130. m/0.32 mm/0.50 μm, H2; Program: 60 0C (8 min) 3 K/min -> 180 0C 20 K/min -> 230 0C (20 min)

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-51596.Flamini, Cioni, et al., 200730. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-51597.Maccioni, Baldini, et al., 200730. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryMethyl Silicone1588.Melo, Corrêa, et al., 200730. m/0.25 mm/0.25 μm, He, 2. K/min, 220. C @ 15. min; Tstart: 80. C
CapillaryZB-51603.Simoniatto, Bonani, et al., 200730. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 250. C
CapillaryDB-51595.Telascrea, de Araujo, et al., 200730. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-51595.Block, Flamini, et al., 200630. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryHP-51598.Flamini, Tebano, et al., 200630. m/0.25 mm/0.25 μm, N2, 60. C @ 10. min, 5. K/min; Tend: 220. C
CapillaryHP-51601.Javidnia K., Miri R., et al., 200630. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 260. C
CapillaryRTX-11582.Paolini J., Desjobert J.M., et al., 200660. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C
CapillaryBP-11584.Boti J.B., Koukoua G., et al., 200550. m/0.22 mm/0.25 μm, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryRTX-11585.Cozzani, Muselli, et al., 200560. m/0.22 mm/0.25 μm, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryHP-5MS1595.Pino, Mesa, et al., 200530. m/0.25 mm/0.25 μm, He, 60. C @ 2. min, 4. K/min, 250. C @ 20. min
CapillarySE-541595.Simionatto, Porto, et al., 200525. m/0.25 mm/0.2 μm, H2, 4. K/min; Tstart: 50. C; Tend: 250. C
CapillaryHP-5MS1599.Karioti, Hadjipavlou-Litina, et al., 200430. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 4. K/min; Tend: 280. C
CapillaryHP-51586.Stashenko, Jaramillo, et al., 200450. m/0.2 mm/0.2 μm, He, 40. C @ 15. min, 3. K/min, 250. C @ 40. min
CapillaryDB-51598.bin Ahmad and bin Jantan, 200325. m/0.25 mm/0.25 μm, N2, 75. C @ 10. min, 3. K/min, 210. C @ 1. min
CapillaryBP-11589.Bianchini, Tomi, et al., 200350. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C
CapillaryBP-11589.Bianchini, Tomi, et al., 200350. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C
CapillaryRTX-11584.Cavalli, Tomi, et al., 200360. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 45. min; Tstart: 60. C
CapillaryHP-51597.Dural, Bagci, et al., 200330. m/0.25 mm/0.25 μm, N2, 60. C @ 10. min, 5. K/min; Tend: 220. C
CapillaryDB-11602.de Feo, Bruno, et al., 200330. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 2. K/min, 250. C @ 20. min
CapillaryPE-51596.Isidorov and Vinogorova, 2003He, 3. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tstart: 40. C; Tend: 280. C
CapillaryDB-51598.Jantan, Ling, et al., 200330. m/0.25 mm/0.25 μm, He, 75. C @ 10. min, 3. K/min, 230. C @ 20. min
CapillaryHP-51597.Macchioni, Cioni, et al., 200330. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-11588.bin Jantan and bin Ahmad, 2002N2, 60. C @ 10. min, 3. K/min, 180. C @ 10. min; Column length: 25. m; Column diameter: 0.25 mm
CapillaryCP Sil 5 CB1584.Pino, Marbot, et al., 200225. m/0.25 mm/0.25 μm, N2, 60. C @ 6. min, 4. K/min; Tend: 280. C
CapillaryCP Sil 5 CB1585.Pino, Marbot, et al., 2002, 230. m/0.25 mm/0.25 μm, H2, 60. C @ 10. min, 2. K/min, 280. C @ 40. min
CapillaryBP-11589.Bianchini, Tomi, et al., 200150. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C
CapillaryDB-51594.Nogueira, Bittrich, et al., 200130. m/0.25 mm/0.25 μm, H2, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-51625.Bartley and Jacobs, 200060. m/0.25 mm/0.25 μm, He, 40. C @ 2. min, 4. K/min, 290. C @ 5. min
CapillaryDB-51591.Maia, de Paula, et al., 200030. m/0.25 mm/0.25 μm, He, 60. C @ 2. min, 3. K/min; Tend: 240. C
CapillaryMethyl Silicone1598.Sumathykutty, Rao, et al., 199950. m/0.25 mm/0.17 μm, N2, 2. K/min; Tstart: 80. C; Tend: 200. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-5MS1605.4Andriamaharavo, 201430. m/0.25 mm/0.25 μm, He; Program: 60C (1 min) => 5 C/min => 210C => 10 C/min => 280C (15 min)
CapillaryCBP-51604.Silva, Oliveira, et al., 200730. m/0.25 mm/0.25 μm, He; Program: 60C => 3C/min => 246C => 10C/min => 270C (5min)
CapillaryBPX-51617.Cardeal, da Silva, et al., 200630. m/0.25 mm/0.25 μm; Program: 35C(5min) => 3C/min => 210C => 40C/min => 240C (4min)

Van Den Dool and Kratz RI, polar column, temperature ramp

View large format table.

Column type Active phase I Reference Comment
CapillaryBP-202088.Boti J.B., Koukoua G., et al., 200550. m/0.22 mm/0.25 μm, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryRTX-Wax2064.Cozzani, Muselli, et al., 200560. m/0.22 mm/0.25 μm, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryPEG-20M2077.Simionatto, Porto, et al., 20054. K/min; Tstart: 50. C; Tend: 250. C
CapillaryBP-202080.Bianchini, Tomi, et al., 200350. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C
CapillaryBP-202080.Bianchini, Tomi, et al., 200350. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C
CapillaryRTX-Wax2077.Cavalli, Tomi, et al., 200360. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 45. min; Tstart: 60. C
CapillaryBP-202080.Bianchini, Tomi, et al., 200150. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C
CapillaryDB-Wax2096.Brophy, Forster, et al., 1998He, 3. K/min; Column length: 60. m; Column diameter: 0.32 mm; Tstart: 35. C; Tend: 220. C
CapillarySP-10002100.Brophy, Goldsack, et al., 1997He, 3. K/min; Column length: 85. m; Column diameter: 0.5 mm; Tstart: 65. C; Tend: 225. C

Van Den Dool and Kratz RI, polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryHP-Innowax2090.Bisio, Ciarallo, et al., 199830. m/0.25 mm/0.25 μm, He; Program: 60C(8min) => 3C/min => 180C(5min) => 40C/min => 250C

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-5 MS1600.Phungpanya, Thongpoon, et al., 201230. m/0.25 mm/0.25 μm, Helium, 2. K/min; Tstart: 50. C; Tend: 180. C
CapillaryDB-51595.Silva, Suzuki, et al., 201235. m/0.20 mm/0.10 μm, Helium, 4. K/min; Tstart: 50. C; Tend: 200. C
CapillaryDB-51617.Silva, Suzuki, et al., 201235. m/0.20 mm/0.10 μm, Helium, 4. K/min; Tstart: 50. C; Tend: 200. C
CapillaryDB-51626.Silva, Suzuki, et al., 201235. m/0.20 mm/0.10 μm, Helium, 4. K/min; Tstart: 50. C; Tend: 200. C
CapillaryDB-51595.Karimi, Farmani, et al., 201130. m/0.25 mm/0.25 μm, Helium, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryCP-Sil 5 CB1592.Mothana, Hasson, et al., 201130. m/0.25 mm/0.26 μm, Nitrogen, 3. K/min, 280. C @ 22. min; Tstart: 45. C
CapillaryZB-51595.Vazques, Aimar, et al., 201130. m/0.25 mm/0.25 μm, Nitrogen, 40. C @ 5. min, 5. K/min; Tend: 200. C
CapillaryZB-51598.Vazquez, Demmel, et al., 201130. m/0.25 mm/0.25 μm, Nitrogen, 40. C @ 5. min, 5. K/min, 200. C @ 5. min
CapillaryHP-51600.Cavar, Maksimovic, et al., 201030. m/0.252 mm/0.25 μm, Helium, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-51601.Ho, Wang, et al., 201030. m/0.25 mm/0.25 μm, Helium, 2. K/min; Tstart: 50. C; Tend: 250. C
CapillaryBP-11585.Mishra, Chaudhary, et al., 2010Nitrogen, 60. C @ 10. min, 5. K/min, 220. C @ 30. min
CapillaryHP-5 MS1595.Ogunwande, Flamini, et al., 201030. m/0.25 mm/0.25 μm, Helium, 60. C @ 10. min, 5. K/min; Tend: 220. C
CapillaryCP-Sil 5 CB1611.Hnawia, Menut, et al., 200930. m/0.25 mm/0.25 μm, Nitrogen, 5. K/min; Tstart: 50. C; Tend: 200. C
CapillaryDB-51601.Ho, Wang, et al., 200930. m/0.25 mm/0.25 μm, Helium, 50. C @ 2. min, 5. K/min; Tend: 250. C
CapillaryHP-11585.Wetwiayaklung, Thavanapong, et al., 200925. m/0.32 mm/0.17 μm, 50. C @ 5. min, 1. K/min, 260. C @ 5. min
CapillaryDB-51587.Chieng, Assim, et al., 200825. m/0.22 mm/0.25 μm, Nitrogen, 50. C @ 2. min, 6.5 K/min, 300. C @ 7. min
CapillaryVF-5MS1608.Kowalski, 200830. m/0.25 mm/0.25 μm, Helium, 240. C @ 1. min, 20. K/min; Tend: 320. C
CapillaryHP-51595.Lago, Romoff, et al., 200830. m/0.32 mm/0.25 μm, Helium, 100. C @ 2. min, 5. K/min, 240. C @ 5. min
CapillaryDB-51615.Amiri, 200750. m/0.20 mm/0.32 μm, Nitrogen, 60. C @ 3. min, 5. K/min, 220. C @ 5. min
CapillaryDB-51596.Bos, Woerdenbag, et al., 200730. m/0.26 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-5MS1600.Da Silva J.K.R., Sousa P.J.C., et al., 200730. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-51596.Elfami, Bos, et al., 200730. m/0.26 mm/0.25 μm, Helium, 3. K/min; Tstart: 60. C; Tend: 290. C
CapillaryDB-51595.Limberger, Scopel, et al., 200730. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 300. C
CapillaryDB-51591.Pontes, de Olivera, et al., 200730. m/0.25 mm/0.25 μm, Hydrogen, 4. K/min; Tstart: 50. C; Tend: 250. C
CapillaryDB-51596.Sefidkon, Abbasi, et al., 200730. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 50. C; Tend: 240. C
CapillaryDB-51597.Apel, Sobral, et al., 200630. m/0.25 mm/0.25 μm, 3. K/min; Tstart: 60. C; Tend: 300. C
CapillaryAT-51596.Borges, Rojas, et al., 200660. m/0.25 mm/0.25 μm, He, 4. K/min, 200. C @ 20. min; Tstart: 60. C
CapillaryBP-11587.Boti, Yao, et al., 200650. m/0.22 mm/0.25 μm, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryHP-51601.Coronel, Cerda-Garcia-Rojas, et al., 200630. m/0.32 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillaryHP-5MS1597.Ebrahim Sajjadi and Mehregan, 200630. m/0.25 mm/0.25 μm, 4. K/min; Tstart: 60. C; Tend: 280. C
CapillaryDB-51596.Elfami, Komar, et al., 200630. m/0.26 mm/0.25 μm, Helium, 3. K/min; Tstart: 60. C; Tend: 290. C
CapillaryDB-51592.Garneau F.X., Collin G., et al., 200630. m/0.25 mm/0.25 μm, 40. C @ 2. min, 2. K/min, 210. C @ 33. min
CapillaryCP Sil 5 CB1625.Hymete, Rohloff, et al., 200630. m/0.25 mm/0.25 μm, 3. K/min, 220. C @ 3. min; Tstart: 40. C
CapillaryHP-51602.Pintore G., Chessa M., et al., 200630. m/0.25 mm/0.25 μm, He, 60. C @ 10. min, 5. K/min; Tend: 220. C
CapillaryDB-51595.Pino, Marbot, et al., 200630. m/0.25 mm/0.25 μm, Hydrogen, 70. C @ 4. min, 4. K/min; Tend: 280. C
CapillaryDB-51594.Rout, Naik, et al., 200630. m/0.25 mm/0.25 μm, He, 2. K/min, 200. C @ 60. min; Tstart: 60. C
CapillaryDB-11626.Sonboli, Mirjalili, et al., 200660. m/0.25 mm/0.25 μm, Helium, 5. K/min, 250. C @ 10. min; Tstart: 60. C
CapillaryMethyl Silicone1619.Tonzibo, Coffy, et al., 200625. m/0.3 mm/0.15 μm, N2, 50. C @ 5. min, 2. K/min; Tend: 210. C
CapillaryDB-51599.Trilles, Bombarda, et al., 200630. m/0.25 mm/0.25 μm, N2, 4. K/min; Tstart: 60. C; Tend: 240. C
CapillaryHP-51618.Wang, Yang, et al., 200630. m/0.25 mm/0.25 μm, He, 60. C @ 2. min, 10. K/min, 250. C @ 10. min
CapillaryDB-11600.Fakhari A.R., Sonboli A., et al., 200560. m/0.25 mm/0.25 μm, N2, 5. K/min, 250. C @ 10. min; Tstart: 60. C
CapillaryHP-5MS1599.Ghasemi Y., Faridi P., et al., 2005He, 50. C @ 3. min, 3. K/min, 250. C @ 10. min; Column length: 25. m; Column diameter: 0.25 mm
CapillaryDB-51584.Limberger, Sobral, et al., 200530. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 230. C
CapillaryHP-51626.Oyedeji, Yani, et al., 200530. m/0.25 mm/0.25 μm, He, 5. K/min; Tstart: 70. C; Tend: 240. C
CapillaryDB-11595.Pala-Paul, Perez-Alonso, et al., 200550. m/0.25 mm/0.25 μm, N2, 4. K/min; Tstart: 95. C; Tend: 240. C
CapillaryHP-5MS1601.Petrakis, Roussis, et al., 20053. K/min; Column length: 30. m; Column diameter: 0.2 mm; Tstart: 60. C; Tend: 280. C
CapillaryDB-51600.Salehi, Sefidkon, et al., 200530. m/0.25 mm/0.25 μm, He, 60. C @ 4. min, 3. K/min; Tend: 220. C
CapillaryPE-51605.Singh, Raina, et al., 200530. m/0.32 mm/0.25 μm, H2, 60. C @ 2. min, 5. K/min, 230. C @ 4. min
CapillaryRTX-11623.Sonboli A., Fakhari A.R., et al., 200560. m/0.25 mm/0.25 μm, He, 5. K/min, 250. C @ 10. min; Tstart: 60. C
CapillaryDB-5MS1596.Watanabe Y., Mihara R., et al., 200530. m/0.25 mm/0.25 μm, He, 80. C @ 2. min, 5. K/min, 250. C @ 9. min
CapillaryCP Sil 5 CB1594.Agnaniet, Menut, et al., 200430. m/0.25 mm/0.25 μm, N2, 5. K/min; Tstart: 50. C; Tend: 200. C
CapillaryDB-5MS1595.paz Lima, Silva, et al., 200430. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-51593.Lopez Arze, Collin, et al., 200430. m/0.25 mm/0.25 μm, 40. C @ 2. min, 2. K/min, 210. C @ 33. min
CapillaryDB-51592.Tellez, Khan, et al., 200430. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryHP-5MS1593.Couladis, Özcan, et al., 200330. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryRSL-2001591.Jirovetz, Buchbauer, et al., 200330. m/0.32 mm/0.25 μm, H2, 40. C @ 5. min, 6. K/min, 280. C @ 5. min
CapillaryRSL-2001605.Jirovetz, Buchbauer, et al., 2003, 230. m/0.32 mm/0.25 μm, H2, 40. C @ 5. min, 6. K/min, 280. C @ 5. min
CapillaryDB-51590.Limberger, Simões-Pires, et al., 200330. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 250. C
CapillaryHP-51574.Pitarokili, Tzakou, et al., 200330. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryHP-5MS1599.Sadraei, Ghannadi, et al., 200330. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 60. C; Tend: 275. C
CapillaryOV-1011592.Boyom, Keumedjio, et al., 20025. K/min; Column length: 25. m; Column diameter: 0.32 mm; Tstart: 50. C; Tend: 200. C
CapillaryDB-51595.Farah, Fechtal, et al., 200230. m/0.25 mm/0.25 μm, N2, 4. K/min; Tstart: 50. C; Tend: 250. C
CapillaryHP-51595.Farah, Fechtal. M., et al., 200230. m/0.25 mm/0.25 μm, N2, 50. C @ 5. min, 4. K/min; Tend: 250. C
CapillaryRSL-2001589.Jirovetz, Buchbauer, et al., 200230. m/0.32 mm/0.25 μm, H2, 40. C @ 5. min, 6. K/min, 280. C @ 5. min
CapillaryRSL-2001598.Jirovetz, Ngassoum, et al., 200230. m/0.32 mm/0.25 μm, H2, 50. C @ 5. min, 6. K/min, 280. C @ 5. min
CapillaryDB-51584.Limberger, Simões-Pires, et al., 200230. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 250. C
CapillaryDB-51601.Morteza-Semnani, Saeedi, et al., 200230. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 4. K/min; Tend: 220. C
CapillaryDB-51593.Ruberto, Biondi, et al., 200230. m/0.25 mm/0.25 μm, He, 2. K/min; Tstart: 60. C; Tend: 300. C
CapillaryDB-11580.Sefidkon, Jalili, et al., 200260. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 4. K/min; Tend: 280. C
CapillaryHP-51596.Flamini, Cioni, et al., 200130. m/0.25 mm/0.25 μm, N2, 60. C @ 10. min, 5. K/min; Tend: 220. C
CapillaryDB-51595.Rousis, Papadogianni, et al., 2001He, 50. C @ 5. min, 3. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tend: 250. C
CapillaryDB-11603.0Santos, Moreira, et al., 2001He, 3. K/min; Column length: 30. m; Column diameter: 0.2 mm; Tstart: 60. C; Tend: 240. C
CapillarySE-301584.Jassbi, Ahmad, et al., 199930. m/0.25 mm/0.25 μm, N2, 60. C @ 10. min, 4. K/min; Tend: 220. C
CapillaryDB-51571.Porta, Porcedda, et al., 199930. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 2. K/min, 250. C @ 60. min
CapillaryDB-51599.Santos, Andrade, et al., 199830. m/0.25 mm/0.25 μm, Helium, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryOV-1011592.Zollo, Biyiti, et al., 19985. K/min; Column length: 25. m; Column diameter: 0.32 mm; Tstart: 50. C; Tend: 200. C
CapillaryHP-11580.Ayedoun, Adeoti, et al., 199623. m/0.32 mm/0.17 μm, He, 60. C @ 3. min, 5. K/min, 250. C @ 30. min
CapillaryOV-1011604.Chacko, Jayalekshmy, et al., 199650. m/0.25 mm/0.17 μm, N2, 5. K/min; Tstart: 50. C; Tend: 220. C

Normal alkane RI, non-polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryTR-5 MS1616.Kurashov, Mitrukova, et al., 201415. m/0.25 mm/0.25 μm, Helium; Program: 35 0C (3 min) 2 0C/min -> 60 0C (3 min) 2 0C/min -> 80 0C (3 min) 4 0C/min -> 120 0C (3 min) 5 0C/min -> 150 0C (3 min) 15 0C/min -> 240 0C (10 min)
CapillaryPolydimethyl siloxane with 5 % Ph groups1595.da Silva, de Souza, et al., 201230. m/0.25 mm/0.25 μm, Helium; Program: 50 0C 4 0C/min -> 200 0C (5 min) 20 0C/min -> 280 0C
Capillary5 % Phenyl polydimethyl siloxane1598.Chaverri, Diaz, et al., 2011Program: not specified
CapillaryZB-51593.Vazques, Aimar, et al., 201130. m/0.25 mm/0.25 μm, Nitrogen; Program: not specified
CapillaryZB-51598.Vazquez, Demmel, et al., 201130. m/0.25 mm/0.25 μm, Nitrogen; Program: not specified
CapillaryHP-51602.Custer, 200925. m/0.32 mm/0.17 μm, Helium; Program: 60 0C (5 min) 4 0C/min -> 220 0C 11 0C/min -> 280 0C (15 min)
CapillaryHP-51600.Custer, 200925. m/0.32 mm/0.17 μm, Helium; Program: not specified
CapillaryHP-11584.Wetwiayaklung, Thavanapong, et al., 200925. m/0.32 mm/0.17 μm; Program: not specified
CapillaryDB-51589.Chieng, Assim, et al., 200825. m/0.22 mm/0.25 μm, Nitrogen; Program: not specified
CapillaryRTX-51603.Zachariah, Leela, et al., 200830. m/0.25 mm/0.25 μm, Helium; Program: 60 0C (5 min) 5 0C/min -> 110 0C 3 0C/min -> 220 0C (5 min)
CapillaryRTX-51595.Zachariah, Leela, et al., 200830. m/0.25 mm/0.25 μm, Helium; Program: not specified
CapillaryHP-5MS1602.Cole, Haber, et al., 200730. m/0.25 mm/0.25 μm, He; Program: 40C(10min) => 3C/min => 200C => 2C/min => 220C
CapillaryDB-11575.Ferreira, Meireles de Sousa, et al., 200730. m/0.25 mm/0.25 μm, He; Program: 45C => 3C/min => 175C => 15C/min => 300C (10min)
CapillaryHP-11593.Merle, Verdeguer, et al., 200730. m/0.2 mm/0.33 μm, He; Program: 60C(5min) => 3C/min => 180C => 20C/min => 280C(10min)
CapillaryHP-5 MS1593.Moriarity, Bansal, et al., 200730. m/0.25 mm/0.25 μm, Helium; Program: 40 0C (10 min) 3 0C/min -> 200 0C 2 0C/min -> 220 0C
CapillaryDB-51595.Pontes, de Olivera, et al., 200730. m/0.25 mm/0.25 μm, Hydrogen; Program: not specified
CapillaryHP-5 MS1596.Setzer, Stokes, et al., 2007Helium; Column length: 30. m; Column diameter: 0.25 mm; Program: 40 0C (10 min) 3 oC/min -> 200 0C 2 0C/min -> 220 0C
CapillaryHP-5 MS1595.Sharififar, Mozaffarian, et al., 200730. m/0.25 mm/0.25 μm, Helium; Program: not specified
CapillaryHP-5 MS1602.Stokes, Cole, et al., 2007Program: not specified
CapillaryHP-5MS1603.Takaku, Haber, et al., 2007He; Column length: 30. m; Column diameter: 0.25 mm; Program: 40C(10min) => 3C/min => 200C => 2C/min => 220C
CapillaryDB-51598.Cysne, Canuto, et al., 200530. m/0.25 mm/0.25 μm, He; Program: 35C => 4C/min => 180C => 10C/min => 250C
CapillaryMethyl Silicone1593.Couladis, Özcan, et al., 2004Program: not specified
CapillaryDB-51589.Hamm, Bleton, et al., 200430. m/0.25 mm/0.25 μm, He; Program: 40C(1min) => 9C/min => 130C => 2C/min => 230C
CapillarySE-301590.Vinogradov, 2004Program: not specified
CapillarySE-301595.Vinogradov, 2004Program: not specified
CapillarySE-541595.Lima, Veiga, et al., 200325. m/0.25 mm/0.25 μm, H2; Program: 110C(2min) => 3C/min => 130C => 8.5C => 290C
CapillaryDB-51601.Morteza-Semnani and Vahedi, 2002Program: not specified
CapillaryDB-51593.Petrakis, Tsitsimpikou, et al., 2001Program: not specified
CapillaryDB-51596.Andrade, Maia, et al., 200030. m/0.25 mm/0.25 μm, He; Program: 40C => 2C/min => 60C => 4C/min => 260C
CapillaryDB-11575.da Silva, Figueiredo, et al., 199830. m/0.25 mm/0.25 μm, H2; Program: 45C => 3C/min => 175C => 15C => 240C(10min)
CapillaryPolydimethyl siloxanes1585.Zenkevich, 1997Program: not specified

Normal alkane RI, polar column, temperature ramp

View large format table.

Column type Active phase I Reference Comment
CapillarySupelcowax-102089.Hnawia, Menut, et al., 200930. m/0.25 mm/0.25 μm, Nitrogen, 5. K/min; Tstart: 50. C; Tend: 200. C
CapillaryCP-Wax 52CB2103.Hymete, Rohloff, et al., 200730. m/0.32 mm/0.25 μm, He, 40. C @ 1. min, 3. K/min, 220. C @ 2. min
CapillaryCarbowax 20M2065.Limberger, Scopel, et al., 200730. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 230. C
CapillaryBP-202090.Boti, Yao, et al., 200650. m/0.22 mm/0.25 μm, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillarySupelcowax-102093.Garneau F.X., Collin G., et al., 200630. m/0.25 mm/0.25 μm, 40. C @ 2. min, 2. K/min, 210. C @ 33. min
CapillaryInnowax2094.Joichi, Yomogida, et al., 200560. m/0.25 mm/0.25 μm, He, 5. K/min, 240. C @ 30. min; Tstart: 60. C
CapillarySupelcowax-102092.Lopez Arze, Collin, et al., 200430. m/0.25 mm/0.25 μm, 40. C @ 2. min, 2. K/min, 210. C @ 33. min
CapillaryBP-202104.Dunlop, Bignell, et al., 199925. m/0.33 mm/0.5 μm, 5. K/min; Tstart: 80. C; Tend: 220. C
CapillaryBP-202104.Bignell, Dunlop, et al., 199825. m/0.33 mm/0.5 μm, H2, 5. K/min; Tstart: 80. C; Tend: 220. C
CapillaryBP-202104.Bignell, Dunlop, et al., 199725. m/0.33 mm/0.5 μm, H2, 5. K/min; Tstart: 80. C; Tend: 220. C
CapillaryBP-202104.Bignell, Dunlop, et al., 1997, 225. m/0.33 mm/0.5 μm, H2, 5. K/min; Tstart: 80. C; Tend: 220. C
CapillaryBP-202104.Bignell, Dunlop, et al., 1997, 325. m/0.33 mm/0.5 μm, H2, 5. K/min; Tstart: 80. C; Tend: 220. C
CapillaryBP-202104.Bignell, Dunlop, et al., 1997, 425. m/0.33 mm/0.5 μm, H2, 5. K/min; Tstart: 80. C; Tend: 220. C
CapillaryBP-202104.Bignell, Dunlop, et al., 1997, 525. m/0.33 mm/0.5 μm, 5. K/min; Tstart: 80. C; Tend: 220. C
CapillaryBP-202104.Bignell, Dunlop, et al., 1997, 625. m/0.33 mm/0.5 μm, H2, 5. K/min; Tstart: 80. C; Tend: 220. C

Normal alkane RI, polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryInnowax2108.Noorizadeh, Farmany, et al., 201160. m/0.25 mm/0.33 μm; Program: not specified
CapillaryHP Innowax2108.Noorizadeh and Farmany, 201060. m/0.25 mm/0.33 μm; Program: not specified
CapillaryCarbowax 20M2081.Merle, Verdeguer, et al., 2007He; Column length: 30. m; Program: 60C(5min) => 3C/min => 180C => 20C/min => 280C(10min)
CapillaryHP-Innowax FSC2103.Tabanca, Demirci, et al., 200660. m/0.25 mm/0.25 μm, N2; Program: 60C(10min) => 4C/min => 220C => (10min) => 1C/min => 240C
CapillaryHP-Innowax FSC2103.Demirci, Baser, et al., 200360. m/0.25 mm/0.25 μm, He; Program: 60C (10min) => 4C/min => 220C (10min) => 1C/min => 240C
CapillaryInnowax FSC2103.Baser, Demirei, et al., 200260. m/0.25 mm/0.25 μm, He; Program: 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
CapillaryHP-Innowax2104.Demirci, Baser, et al., 200260. m/0.25 mm/0.25 μm, He; Program: 60 0C (10 min) 4 K/min -> 220 0C (10 min) 1 K/min -> 240 0C
CapillaryFFAP2084.Reddy, Angers, et al., 199825. m/0.2 mm/0.33 μm, H2; Program: 40C(5min) => 4C/min => 170C => 8C/min => 240C (12min)

References

Go To: Top, Mass spectrum (electron ionization), Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Lucero, Fredrickson, et al., 2006
Lucero, M.E.; Fredrickson, E.L.; Estell, R.E.; Morrison, A.A.; Richman, D.B., Volatile Composition of Gutierrezia sarothrae (Broom Snakeweed) as Determined by Steam Distillation and Solid Phase Microextraction, J. Essent. Oil Res., 2006, 18, 2, 121-125, https://doi.org/10.1080/10412905.2006.9699039 . [all data]

Shatar S., 2005
Shatar S., Essential oil of Ferula ferulaoides from Western Mongolia, Chem. Nat. Compd. (Engl. Transl.), 2005, 41, 5, 607-608, https://doi.org/10.1007/s10600-005-0222-8 . [all data]

Siani, Garrido, et al., 2004
Siani, A.C.; Garrido, I.S.; Monteiro, S.S.; Carvalho, E.S.; Ramos, M.F.S., Protium icicariba as a source of volatile essences, Biochem. Syst. Ecol., 2004, 32, 5, 477-489, https://doi.org/10.1016/j.bse.2003.11.003 . [all data]

El-Massry, El-Ghorab, et al., 2002
El-Massry, K.F.; El-Ghorab, A.H.; Farouk, A., Antioxidant activity and volatile components of Egyptian Artemisia judaica L., Food Chem., 2002, 79, 3, 331-336, https://doi.org/10.1016/S0308-8146(02)00164-4 . [all data]

Raina, Srivastava, et al., 2002
Raina, V.K.; Srivastava, S.K.; Syamasunder, K.V., The essential oil of 'greater galangal' [Alpinia galanga (L.) Willd.] from the lower Himalayan region of India, Flavour Fragr. J., 2002, 17, 5, 358-360, https://doi.org/10.1002/ffj.1105 . [all data]

Moreira, Sousa, et al., 2001
Moreira, D.L.; Sousa, P.O.; Pereira, N.A.; Cardoso, G.L., Effect of leaf essential oil from Piper solmsianum C.DC. in mice behaviour, An. Acad. Bras. Cienc., 2001, 73, 1, 1-7, https://doi.org/10.1590/S0001-37652001000100004 . [all data]

Palá-Paúl, Velasco-Negueruela, et al., 2001
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Senatore and Rigano, 2001
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Raharivelomanana, Cambon, et al., 1993
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Ekundayo, Laakso, et al., 1988
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Tuberoso, Kowalczyk, et al., 2005
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Frizzo, Serafini, et al., 2001
Frizzo, C.D.; Serafini, L.A.; Dellacassa, E.; Lorenzo, D.; Moyna, P., Essential oil of Baccharis uncinella DC. from Southern Brazil, Flavour Fragr. J., 2001, 16, 4, 286-288, https://doi.org/10.1002/ffj.998 . [all data]

Flamini, Cioni, et al., 2007
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Maccioni, Baldini, et al., 2007
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Melo, Corrêa, et al., 2007
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Telascrea, de Araujo, et al., 2007
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Block, Flamini, et al., 2006
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Flamini, Tebano, et al., 2006
Flamini, G.; Tebano, M.; Cioni, P.L.; Bagci, Y.; Dural, H.; Ertugrul, K.; Uysal, T.; Savran, A., A multivariate statistical approach to Centaurea classification using essential oil composition data of some species from Turkey, Pl. Syst. Evol., 2006, 261, 1-4, 217-228, https://doi.org/10.1007/s00606-006-0448-3 . [all data]

Javidnia K., Miri R., et al., 2006
Javidnia K.; Miri R.; Javidnia A., Constituents of the essential oil of Scabiosa flavida from Iran, Chem. Nat. Compd. (Engl. Transl.), 2006, 42, 5, 529-530, https://doi.org/10.1007/s10600-006-0206-3 . [all data]

Paolini J., Desjobert J.M., et al., 2006
Paolini J.; Desjobert J.M.; Costa J.; Bernardini A.F.; Castellini C.B.; Cioni P.L.; Flamini G.; Morelli I., Composition of essential oils of Helichrysum italicum (Roth) G. Don fil subsp. italicum from Tuscan archipelago islands, Flavour Fragr. J., 2006, 21, 5, 805-808, https://doi.org/10.1002/ffj.1726 . [all data]

Boti J.B., Koukoua G., et al., 2005
Boti J.B.; Koukoua G.; N'Guessan T.Y.; Muselli A.; Bernardini A.F.; Casanova J., Composition of the leaf, stem bark and root bark oils of Isolona cooperi investigated by GC (retention index), GC-MS and C-13-NMR spectroscopy, Phytochem. Anal., 2005, 16, 5, 357-363, https://doi.org/10.1002/pca.857 . [all data]

Cozzani, Muselli, et al., 2005
Cozzani, S.; Muselli, A.; Desjobert, J.-M.; Bernardini, A.-F.; Tomi, F.; Casanova, J., Chemical composition of essential oil of Teucrium polium subsp. capitatum (L.) from Corsica, Flavour Fragr. J., 2005, 20, 4, 436-441, https://doi.org/10.1002/ffj.1463 . [all data]

Pino, Mesa, et al., 2005
Pino, J.A.; Mesa, J.; Muñoz, Y.; Martí, M.P.; Marbot, R., Volatile components from mango (Mangifera indica L.) cultivars, J. Agric. Food Chem., 2005, 53, 6, 2213-2223, https://doi.org/10.1021/jf0402633 . [all data]

Simionatto, Porto, et al., 2005
Simionatto, E.; Porto, C.; da Silva, U.F.; Squizani, A.; Dalcol, I.I.; Morel, A.F., Composition and antimicrobial activity of the essential oil from Aloysia sellowii, J. Braz. Chem. Soc., 2005, 16, 6B, 1458-1462, https://doi.org/10.1590/S0103-50532005000800028 . [all data]

Karioti, Hadjipavlou-Litina, et al., 2004
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Stashenko, Jaramillo, et al., 2004
Stashenko, E.E.; Jaramillo, B.E.; Martínez, J.R., Analysis of volatile secondary metabolites from Colombian Xylopia aromatica (Lamarck) by different extraction and headspace methods and gas chromatography, J. Chromatogr. A, 2004, 1025, 1, 105-113, https://doi.org/10.1016/j.chroma.2003.10.059 . [all data]

bin Ahmad and bin Jantan, 2003
bin Ahmad, F.; bin Jantan, I., Chemical constituents of the essential oils of Goniothalamus uvariodes King, Flavour Fragr. J., 2003, 18, 2, 128-130, https://doi.org/10.1002/ffj.1142 . [all data]

Bianchini, Tomi, et al., 2003
Bianchini, A.; Tomi, P.; Bernardini, A.F.; Morelli, I.; Flamini, G.; Cioni, P.L.; Usai, M.; Marchetti, M., A comparative study of volatile constituents of two Helichrysum italicum (Roth) Guss. Don Fil subspecies growing in Corsica (France), Tuscany and Sardinia (Italy), Flavour Fragr. J., 2003, 18, 6, 487-491, https://doi.org/10.1002/ffj.1231 . [all data]

Cavalli, Tomi, et al., 2003
Cavalli, J.-F.; Tomi, F.; Bernardini, A.-F.; Casanova, J., Composition and chemical variability of the bark oil of Cedrelopsis grevei H. Baillon from Madagascar, Flavour Fragr. J., 2003, 18, 6, 532-538, https://doi.org/10.1002/ffj.1263 . [all data]

Dural, Bagci, et al., 2003
Dural, H.; Bagci, Y.; Ertugrul, K.; Demirelma, H.; Flamini, G.; Cioni, P.L.; Morelli, I., Essential oil composition of two endemic Centaurea species from Turkey, Centaurea mucronifera and Centaurea chrysantha, collected in the same habitat, Biochem. Syst. Ecol., 2003, 31, 12, 1417-1425, https://doi.org/10.1016/S0305-1978(03)00128-5 . [all data]

de Feo, Bruno, et al., 2003
de Feo, V.; Bruno, M.; Tahiri, B.; Napolitano, F.; Senatore, F., Chemical composition and antibacterial activity of essential oils from Thymus spinulosus Ten. (Lamiaceae), J. Agric. Food Chem., 2003, 51, 13, 3849-3853, https://doi.org/10.1021/jf021232f . [all data]

Isidorov and Vinogorova, 2003
Isidorov, V.A.; Vinogorova, V.T., GC-MS analysis of compounds extracted from buds of Populus balsamifera and Populus nigra, Z. Naturforsch. C:, 2003, 58, 355-360. [all data]

Jantan, Ling, et al., 2003
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Notes

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