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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSDB-5DB-5DB-5DB-5
Column length (m) 30.35.35.35.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.200.200.200.25
Phase thickness (mum) 0.250.100.100.100.25
Tstart (C) 50.50.50.50.60.
Tend (C) 180.200.200.200.240.
Heat rate (K/min) 2.4.4.4.3.
Initial hold (min)      
Final hold (min)      
I 1600.1595.1617.1626.1595.
ReferencePhungpanya, Thongpoon, et al., 2012Silva, Suzuki, et al., 2012Silva, Suzuki, et al., 2012Silva, Suzuki, et al., 2012Karimi, Farmani, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Sil 5 CBZB-5ZB-5HP-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas NitrogenNitrogenNitrogenHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.2520.25
Phase thickness (mum) 0.260.250.250.250.25
Tstart (C) 45.40.40.60.50.
Tend (C) 280.200.200.240.250.
Heat rate (K/min) 3.5.5.3.2.
Initial hold (min)  5.5.  
Final hold (min) 22. 5.  
I 1592.1595.1598.1600.1601.
ReferenceMothana, Hasson, et al., 2011Vazques, Aimar, et al., 2011Vazquez, Demmel, et al., 2011Cavar, Maksimovic, et al., 2010Ho, Wang, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1HP-5 MSCP-Sil 5 CBDB-5HP-1
Column length (m)  30.30.30.25.
Carrier gas NitrogenHeliumNitrogenHelium 
Substrate      
Column diameter (mm)  0.250.250.250.32
Phase thickness (mum)  0.250.250.250.17
Tstart (C) 60.60.50.50.50.
Tend (C) 220.220.200.250.260.
Heat rate (K/min) 5.5.5.5.1.
Initial hold (min) 10.10. 2.5.
Final hold (min) 30.   5.
I 1585.1595.1611.1601.1585.
ReferenceMishra, Chaudhary, et al., 2010Ogunwande, Flamini, et al., 2010Hnawia, Menut, et al., 2009Ho, Wang, et al., 2009Wetwiayaklung, Thavanapong, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5VF-5MSHP-5DB-5DB-5
Column length (m) 25.30.30.50.30.
Carrier gas NitrogenHeliumHeliumNitrogenHe
Substrate      
Column diameter (mm) 0.220.250.320.200.26
Phase thickness (mum) 0.250.250.250.320.25
Tstart (C) 50.240.100.60.60.
Tend (C) 300.320.240.220.240.
Heat rate (K/min) 6.520.5.5.3.
Initial hold (min) 2.1.2.3. 
Final hold (min) 7. 5.5. 
I 1587.1608.1595.1615.1596.
ReferenceChieng, Assim, et al., 2008Kowalski, 2008Lago, Romoff, et al., 2008Amiri, 2007Bos, Woerdenbag, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-5DB-5DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeliumHeHydrogenHe
Substrate      
Column diameter (mm) 0.250.260.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.50.50.
Tend (C) 240.290.300.250.240.
Heat rate (K/min) 3.3.3.4.4.
Initial hold (min)      
Final hold (min)      
I 1600.1596.1595.1591.1596.
ReferenceDa Silva J.K.R., Sousa P.J.C., et al., 2007Elfami, Bos, et al., 2007Limberger, Scopel, et al., 2007Pontes, de Olivera, et al., 2007Sefidkon, Abbasi, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5AT-5BP-1HP-5HP-5MS
Column length (m) 30.60.50.30.30.
Carrier gas  He He 
Substrate      
Column diameter (mm) 0.250.250.220.320.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 300.200.220.246.280.
Heat rate (K/min) 3.4.2.3.4.
Initial hold (min)      
Final hold (min)  20.20.  
I 1597.1596.1587.1601.1597.
ReferenceApel, Sobral, et al., 2006Borges, Rojas, et al., 2006Boti, Yao, et al., 2006Coronel, Cerda-Garcia-Rojas, et al., 2006Ebrahim Sajjadi and Mehregan, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5CP Sil 5 CBHP-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas Helium  HeHydrogen
Substrate      
Column diameter (mm) 0.260.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.40.40.60.70.
Tend (C) 290.210.220.220.280.
Heat rate (K/min) 3.2.3.5.4.
Initial hold (min)  2. 10.4.
Final hold (min)  33.3.  
I 1596.1592.1625.1602.1595.
ReferenceElfami, Komar, et al., 2006Garneau F.X., Collin G., et al., 2006Hymete, Rohloff, et al., 2006Pintore G., Chessa M., et al., 2006Pino, Marbot, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1Methyl SiliconeDB-5HP-5
Column length (m) 30.60.25.30.30.
Carrier gas HeHeliumN2N2He
Substrate      
Column diameter (mm) 0.250.250.30.250.25
Phase thickness (mum) 0.250.250.150.250.25
Tstart (C) 60.60.50.60.60.
Tend (C) 200.250.210.240.250.
Heat rate (K/min) 2.5.2.4.10.
Initial hold (min)   5. 2.
Final hold (min) 60.10.  10.
I 1594.1626.1619.1599.1618.
ReferenceRout, Naik, et al., 2006Sonboli, Mirjalili, et al., 2006Tonzibo, Coffy, et al., 2006Trilles, Bombarda, et al., 2006Wang, Yang, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5MSDB-5HP-5DB-1
Column length (m) 60.25.30.30.50.
Carrier gas N2HeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.25 0.250.250.25
Tstart (C) 60.50.60.70.95.
Tend (C) 250.250.230.240.240.
Heat rate (K/min) 5.3.3.5.4.
Initial hold (min)  3.   
Final hold (min) 10.10.   
I 1600.1599.1584.1626.1595.
ReferenceFakhari A.R., Sonboli A., et al., 2005Ghasemi Y., Faridi P., et al., 2005Limberger, Sobral, et al., 2005Oyedeji, Yani, et al., 2005Pala-Paul, Perez-Alonso, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5PE-5RTX-1DB-5MS
Column length (m) 30.30.30.60.30.
Carrier gas  HeH2HeHe
Substrate      
Column diameter (mm) 0.20.250.320.250.25
Phase thickness (mum)  0.250.250.250.25
Tstart (C) 60.60.60.60.80.
Tend (C) 280.220.230.250.250.
Heat rate (K/min) 3.3.5.5.5.
Initial hold (min)  4.2. 2.
Final hold (min)   4.10.9.
I 1601.1600.1605.1623.1596.
ReferencePetrakis, Roussis, et al., 2005Salehi, Sefidkon, et al., 2005Singh, Raina, et al., 2005Sonboli A., Fakhari A.R., et al., 2005Watanabe Y., Mihara R., et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-5MSDB-5DB-5HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas N2He HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.40.60.60.
Tend (C) 200.240.210.240.280.
Heat rate (K/min) 5.3.2.3.3.
Initial hold (min)   2.  
Final hold (min)   33.  
I 1594.1595.1593.1592.1593.
ReferenceAgnaniet, Menut, et al., 2004paz Lima, Silva, et al., 2004Lopez Arze, Collin, et al., 2004Tellez, Khan, et al., 2004Couladis, Özcan, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RSL-200RSL-200DB-5HP-5HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas H2H2HeHeHe
Substrate      
Column diameter (mm) 0.320.320.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.40.60.60.60.
Tend (C) 280.280.250.280.275.
Heat rate (K/min) 6.6.3.3.4.
Initial hold (min) 5.5.   
Final hold (min) 5.5.   
I 1591.1605.1590.1574.1599.
ReferenceJirovetz, Buchbauer, et al., 2003Jirovetz, Buchbauer, et al., 2003, 2Limberger, Simões-Pires, et al., 2003Pitarokili, Tzakou, et al., 2003Sadraei, Ghannadi, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-5HP-5RSL-200RSL-200
Column length (m) 25.30.30.30.30.
Carrier gas  N2N2H2H2
Substrate      
Column diameter (mm) 0.320.250.250.320.32
Phase thickness (mum)  0.250.250.250.25
Tstart (C) 50.50.50.40.50.
Tend (C) 200.250.250.280.280.
Heat rate (K/min) 5.4.4.6.6.
Initial hold (min)   5.5.5.
Final hold (min)    5.5.
I 1592.1595.1595.1589.1598.
ReferenceBoyom, Keumedjio, et al., 2002Farah, Fechtal, et al., 2002Farah, Fechtal. M., et al., 2002Jirovetz, Buchbauer, et al., 2002Jirovetz, Ngassoum, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5DB-1HP-5
Column length (m) 30.30.30.60.30.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.40.60.
Tend (C) 250.220.300.280.220.
Heat rate (K/min) 3.4.2.4.5.
Initial hold (min)  5. 5.10.
Final hold (min)      
I 1584.1601.1593.1580.1596.
ReferenceLimberger, Simões-Pires, et al., 2002Morteza-Semnani, Saeedi, et al., 2002Ruberto, Biondi, et al., 2002Sefidkon, Jalili, et al., 2002Flamini, Cioni, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1SE-30DB-5DB-5
Column length (m) 60.30.30.30.30.
Carrier gas HeHeN2HeHelium
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (mum)   0.250.250.25
Tstart (C) 50.60.60.40.60.
Tend (C) 250.240.220.250.240.
Heat rate (K/min) 3.3.4.2.3.
Initial hold (min) 5. 10.5. 
Final hold (min)    60. 
I 1595.1603.01584.1571.1599.
ReferenceRousis, Papadogianni, et al., 2001Santos, Moreira, et al., 2001Jassbi, Ahmad, et al., 1999Porta, Porcedda, et al., 1999Santos, Andrade, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase OV-101HP-1OV-101
Column length (m) 25.23.50.
Carrier gas  HeN2
Substrate    
Column diameter (mm) 0.320.320.25
Phase thickness (mum)  0.170.17
Tstart (C) 50.60.50.
Tend (C) 200.250.220.
Heat rate (K/min) 5.5.5.
Initial hold (min)  3. 
Final hold (min)  30. 
I 1592.1580.1604.
ReferenceZollo, Biyiti, et al., 1998Ayedoun, Adeoti, et al., 1996Chacko, Jayalekshmy, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Phungpanya, Thongpoon, et al., 2012
Phungpanya, C.; Thongpoon, C.; Pripdeevech, P.; Machan, T., Analysis of aroma volatiles from fresh leaves of Plectranthus amboinicus using solid phase microextraction (SPME) technique, Pure and Applied Chemistry International Conference 2012 (PACCON 2012), 2012, 16701672. [all data]

Silva, Suzuki, et al., 2012
Silva, P.S.; Suzuki, E.Y.; Moreira, A.P.; Raposo, N.R.B.; Alves, T.M.A.; Viccini, L.F., Stachytarpheta gesnerioides Cham.: chemical composition of hexane fraction and essential oil, antioxidant and antimicrobial activities, Boletin Latinoamericano y del Caribe de Plantas Medicinales y Aromaticas, 2012, 11, 6, 542-548. [all data]

Karimi, Farmani, et al., 2011
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Mothana, Hasson, et al., 2011
Mothana, R.A.A.; Hasson, S.S.; Schultze, W.; Mowitz, A.; Lindequist, U., Phytochemical composition and in vitro antimicrobial and antioxidant activities of essential oils of three endemic Soqotraen Boswellia species, Food Chem., 2011, 126, 3, 1149-1154, https://doi.org/10.1016/j.foodchem.2010.11.150 . [all data]

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Cavar, Maksimovic, et al., 2010
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Ho, Wang, et al., 2010
Ho, C.-L.; Wang, E.I.-C.; Yu, H.-T.; Yu, H.-M.; Su, Y.-C., Composition amd antioxidant activities of essential oils of different tissues from Cryptomeria japonica D. Don, Quarterly J. Chin. Forestry, 2010, 32, 1, 63-76. [all data]

Mishra, Chaudhary, et al., 2010
Mishra, R.K.; Chaudhary, S.; Pandey, R.; Gupta, S.; Mallavarapu, G.R.; Kumar, S., Analysis of linalool content in the inflorescence (flower) essential oil and leaf oil of Lippia alba cultivar Kavach, J. Essen. Oil Res., 2010, 22, 1, 3-7, https://doi.org/10.1080/10412905.2010.9700253 . [all data]

Ogunwande, Flamini, et al., 2010
Ogunwande, I.A.; Flamini, G.; Cioni, P.L.; Omikorede, O.; Azeez, R.A.; Ayodele, A.A.; Kamil, Y.O., Aromatic plants growing in Nigeria: essential oil constituents of Cassia alata (Linn.) Roxb. and Helianthus annuus L., Rec. Nat. Prod., 2010, 4, 4, 211-217. [all data]

Hnawia, Menut, et al., 2009
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Ho, Wang, et al., 2009
Ho, C.-L.; Wang, E.I.-C.; Su, Y.-C., Essential oil compositions and bioactivities of the various parts of Cinnamomum camphora Sieb. var. linallolifera Fujuta, Journal title only in Chinese, 2009, 31, 2, 77-96. [all data]

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Chieng, Assim, et al., 2008
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Limberger, Scopel, et al., 2007
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Pontes, de Olivera, et al., 2007
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Sefidkon, Abbasi, et al., 2007
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Apel, Sobral, et al., 2006
Apel, M.A.; Sobral, M.; Zuanazzi, J.A.S.; Henriques, A.T., Essential oil composition of Calycorectes australis and Calycorectes psidiiflorus (Myrtaceae), Flavour Fragr. J., 2006, 21, 4, 656-658, https://doi.org/10.1002/ffj.1640 . [all data]

Borges, Rojas, et al., 2006
Borges, R.; Rojas, L.B.; Cegarra, J.A.; Usubillaga, A., Study of the essential oils from the leaves and flowers of Lepechinia conferta (Benth) Epl., Flavour Fragr. J., 2006, 21, 1, 155-157, https://doi.org/10.1002/ffj.1550 . [all data]

Boti, Yao, et al., 2006
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Coronel, Cerda-Garcia-Rojas, et al., 2006
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Ebrahim Sajjadi and Mehregan, 2006
Ebrahim Sajjadi, S.; Mehregan, I., Volatile constituents of flowers and leaves of Anthemis hyalina, Chem. Nat. Compd. (Engl. Transl.), 2006, 42, 5, 531-533, https://doi.org/10.1007/s10600-006-0207-2 . [all data]

Elfami, Komar, et al., 2006
Elfami, R.B.; Komar, R.; Woerdenbag, H.J.; Kayser, P.; Quax, W.J., Essential oil constituents of Piper cubeba from Indonesia, 2006, retrieved from http://dissertations.ub.rug.nl/FILES/facultiew/science/2006/elfahmi/05c5.pdf. [all data]

Garneau F.X., Collin G., et al., 2006
Garneau F.X.; Collin G.; Gagnon H.; Jean F.I.; Strobl H.; Pichette A., The essential oil composition of Devil's Club, Oplopanax horridus J. E. Smith Miq., Flavour Fragr. J., 2006, 21, 5, 792-794, https://doi.org/10.1002/ffj.1716 . [all data]

Hymete, Rohloff, et al., 2006
Hymete, A.; Rohloff, J.; Iversen, T.-H., Essential oil from seeds and husks of Aframomum corrorima from Ethiopia, Flavour Fragr. J., 2006, 21, 4, 642-644, https://doi.org/10.1002/ffj.1634 . [all data]

Pintore G., Chessa M., et al., 2006
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Notes

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