1H-Cycloprop[e]azulene, 1a,2,3,4,4a,5,6,7b-octahydro-1,1,4,7-tetramethyl-, [1aR-(1aα,4α,4aβ,7bα)]-

Normal alkane RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSDP-5DP-5HP-5 MSHP-5 MS
Column length (m) 60.30.30.30.30.
Carrier gas HeliumHeliumHelium Helium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.80.80.60.50.
Tend (C) 250.300.300.300.250.
Heat rate (K/min) 3.4.4.15.7.
Initial hold (min) 1.1.1.2.1.
Final hold (min) 20.40.40.10.5.
I 1411.1419.1419.1408.1412.
ReferenceSardashti, Valizadeh, et al., 2013Vijayakumar, Duraipandiyan, et al., 2012Vijayakumar, Duraipandiyan, et al., 2012Xu, Han, et al., 2012Zouari, Ayadi, et al., 2012
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSHP-5 MSDB-5HP-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHydrogen
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.60.50.70.
Tend (C) 270.180.240.240.290.
Heat rate (K/min) 3.2.3.3.5.
Initial hold (min)    5. 
Final hold (min)      
I 1393.1397.1409.1410.1419.
ReferenceCui, Yang, et al., 2011Hammami, Kamoun, et al., 2011Karimi, Farmani, et al., 2011Monsef-Esfahani, Miri, et al., 2010Radulovic, Dordevic, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSDB-5 MSDB-1-MSDB-5DB-5
Column length (m) 30.30.60.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.30.40.35.
Tend (C) 220.240.200.250.220.
Heat rate (K/min) 6.3.2.10.3.
Initial hold (min) 3. 4.1. 
Final hold (min)   35.3.40.
I 1412.1407.1399.1400.1398.
ReferenceSafaei-Ghomi and Batooli, 2010Silva, Pott, et al., 2010Takeoka, Hobbs, et al., 2010Yang, Zhang, et al., 2010El-Massry, El-Ghorab, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5RTX-1RTX-1DB-5 MSHP-5 MS
Column length (m) 30.60.60.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.220.220.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 70.60.60.40.60.
Tend (C) 240.230.230.250.300.
Heat rate (K/min) 5.2.2.4.15.
Initial hold (min)    2.2.
Final hold (min)  30.30.2.10.
I 1431.1408.1413.1412.1408.
ReferenceLawal and Oyedelji, 2009Museli, Pau, et al., 2009Museli, Pau, et al., 2009Su, Wang, et al., 2009Xu, Han, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSRTX-1BPX-5HP-5 MSHP-5
Column length (m) 30.60.7.530.30.
Carrier gas HeliumHeHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.220.100.250.25
Phase thickness (μm) 0.250.2510.0.250.32
Tstart (C) 50.60.60.60.60.
Tend (C) 280.230.240.280.250.
Heat rate (K/min) 4.2.3.10.5.
Initial hold (min)    1.30.
Final hold (min)  35. 7. 
I 1411.1411.1409.1417.1410.
ReferenceZhao, Zeng, et al., 2009Paolini, Tomi, et al., 2008Shellie, 2008Szarka, Hethelyi, et al., 2008Yassa and Akhani, 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5MSHP-1DB-5SPB-1
Column length (m) 50.30.30.30.30.
Carrier gas NitrogenHeHeHeHe
Substrate      
Column diameter (mm) 0.200.250.250.250.2
Phase thickness (μm) 0.320.250.250.250.2
Tstart (C) 60.60.60.60.70.
Tend (C) 220.240.240.300.220.
Heat rate (K/min) 5.3.2.3.3.
Initial hold (min) 3.    
Final hold (min) 5. 20. 15.
I 1406.1410.1378.1400.1402.
ReferenceAmiri, 2007Da Silva J.K.R., Sousa P.J.C., et al., 2007Hachicha, Skanji, et al., 2007Limberger, Scopel, et al., 2007Pinto, Salgueiro, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5HP-5 MSHP-5 MSHP-5 MSHP-5
Column length (m) 30.60.30.30.30.
Carrier gas HeHydrogenHeliumHeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.32
Tstart (C) 50.60.60.60.60.
Tend (C) 250.260.280.280.250.
Heat rate (K/min) 2.4.3.3.5.
Initial hold (min)     30.
Final hold (min)  20.   
I 1414.1411.1406.1410.1410.
ReferenceRaal, Orav, et al., 2007Rojas, Velasco, et al., 2007Tsokou, Georgopoulos, et al., 2007Vagionas, Graikou, et al., 2007Yassa and Akhani, 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5ZB-5AT-5HP-1DB-1
Column length (m) 30.30.60.50.60.
Carrier gas   HeHeNitrogen
Substrate      
Column diameter (mm) 0.250.250.250.20.25
Phase thickness (μm) 0.250.250.250.33 
Tstart (C) 60.40.60.60.40.
Tend (C) 300.300.200.250.200.
Heat rate (K/min) 3.2.4.2.2.
Initial hold (min)    4.1.
Final hold (min)   20.30.9.
I 1403.1394.1410.1414.1403.
ReferenceApel, Sobral, et al., 2006Biondi, Sari, et al., 2006Borges, Rojas, et al., 2006Castel, Fernandez, et al., 2006Chen, Sheu, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5CP Sil 5 CBHP-5HP-5MSHP-5
Column length (m) 30.30.30.30.30.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.40.60.60.100.
Tend (C) 300.220.240.260.240.
Heat rate (K/min) 5.3.4.4.5.
Initial hold (min) 5.   2.
Final hold (min) 5.3.  5.
I 1407.1410.1409.1409.1409.
ReferenceFiguérédo, Cabassu, et al., 2006Hymete, Rohloff, et al., 2006Ibañez and Usubillaga, 2006Ibanez and Usubillaga, 2006Lago, Soares, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1SPB-5SPB-5DB-5DB-5
Column length (m) 50. 60.30.30.
Carrier gas N2HeHeN2He
Substrate      
Column diameter (mm) 0.25 0.320.250.25
Phase thickness (μm) 0.25 1.0.250.25
Tstart (C) 95.50.40.60.40.
Tend (C) 240.250.230.240.250.
Heat rate (K/min) 4.5.3.4.4.
Initial hold (min)  3.5.  
Final hold (min)  15.2.  
I 1411.1409.1445.1406.1395.
ReferencePala-Paul J., Perez-Alonso M.J., et al., 2006Stojanovic, Palic, et al., 2006Tornambe, Cornu, et al., 2006Trilles, Bombarda, et al., 2006Yadegarinia, Gachkar, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5BPX-5DB-5DB-1HP-5MS
Column length (m) 60.25.30.50.30.
Carrier gas HeHeHeN2 
Substrate      
Column diameter (mm) 0.320.220.250.250.2
Phase thickness (μm) 1.0.250.250.25 
Tstart (C) 40.50.60.95.60.
Tend (C) 230.320.220.240.280.
Heat rate (K/min) 3.5.4.4.3.
Initial hold (min) 5.5.4.  
Final hold (min)      
I 1445.1413.1412.1406.1410.
ReferenceCornu, Kondjoyan, et al., 2005Dickschat, Martens, et al., 2005Morteza-Semnani and Saeedi, 2005Pala-Paul, Perez-Alonso, et al., 2005Petrakis, Roussis, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSCP Sil 8 CBRTX-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 280.280.290.220.280.
Heat rate (K/min) 4.3.3.3.3.
Initial hold (min)   5.  
Final hold (min)      
I 1406.1414.1416.1409.1376.
ReferenceSajjadi S.E. and Eskandari B., 2005Slavkovska, Couladis, et al., 2005Suárez, Vásquez, et al., 2005Szafranek, Chrapkowska, et al., 2005Tzakou and Constantinidis, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5RTX-1DB-5
Column length (m) 30.30.25.30.30.
Carrier gas H2N2NitrogenN2He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.40.60.60.35.
Tend (C) 290.230.240.300.220.
Heat rate (K/min) 4.2.3.4.2.5
Initial hold (min)      
Final hold (min)     6.
I 1404.1403.1406.1411.1410.
ReferenceAbreu, Reis, et al., 2004González, Guerra, et al., 2004JAvidnia, Mojab, et al., 2004Kalemba and Thiem, 2004Rohloff, Mordal, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Methyl SiliconeHP-5 MSHP-1DB-5HP-5
Column length (m) 60.30.30.30.30.
Carrier gas HeHeliumHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.2490.25
Phase thickness (μm) 0.250.250.330.250.25
Tstart (C) 60.60.40.60.60.
Tend (C) 200.200.260.300.220.
Heat rate (K/min) 4.4.2.3.5.
Initial hold (min) 1.1.5. 10.
Final hold (min) 20.20.20.  
I 1405.1405.1382.1409.1399.
ReferenceRojas, Usubillaga, et al., 2004Royas, Usubillaga, et al., 2004Senatore, Napolitano, et al., 2004Woerdenbag, Windono, et al., 2004Bertoli, Menichini, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1RSL-200RSL-200DB-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas N2H2H2H2He
Substrate      
Column diameter (mm) 0.250.320.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.40.40.60.60.
Tend (C) 200.280.280.280.280.
Heat rate (K/min) 5.6.6.4.3.
Initial hold (min)  5.5.10. 
Final hold (min)  5.5.40. 
I 1404.1409.1405.1409.1390.
ReferenceFekam Boyom, Ngouana, et al., 2003Jirovetz, Buchbauer, et al., 2003Jirovetz, Buchbauer, et al., 2003, 2Pino, Marbot, et al., 2003Pitarokili, Tzakou, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5HP-5HP-5DB-5
Column length (m) 60.25.25.25.30.
Carrier gas HeHeliumHeliumHeliumHe
Substrate      
Column diameter (mm) 0.250.320.320.320.25
Phase thickness (μm) 0.250.530.530.530.25
Tstart (C) 50.40.40.40.60.
Tend (C) 250.280.280.280.240.
Heat rate (K/min) 4.4.4.4.3.
Initial hold (min)      
Final hold (min)      
I 1406.1405.1407.1410.1411.
ReferencePourmortazavi, Sefidkon, et al., 2003Velickovic, Ristic, et al., 2003Velickovic, Ristic, et al., 2003Velickovic, Ristic, et al., 2003Flamini, Ertugrul, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase PTE-5SE-30RSL-200DB-5DB-5
Column length (m) 60.50.30.30.30.
Carrier gas H2HeH2HeHe
Substrate      
Column diameter (mm) 0.320.250.320.250.25
Phase thickness (μm) 0.300.250.250.250.25
Tstart (C) 60.70.40.60.60.
Tend (C) 285.240.280.240.240.
Heat rate (K/min) 4.34.6.3.3.
Initial hold (min)   5.  
Final hold (min)   5.  
I 1409.1414.1412.1407.1409.
ReferenceGudzic, Djokovic, et al., 2002Iñigo, Palá-Paúl, et al., 2002Jirovetz, Buchbauer, et al., 2002Kobaisy, Tellez, et al., 2002Maia, da Silva, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-5MSDB-5DB-1DB-1
Column length (m) 30.30.30.60.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.40.40.
Tend (C) 240.270.240.280.280.
Heat rate (K/min) 3.3.3.4.4.
Initial hold (min)    5.5.
Final hold (min)      
I 1412.1410.1411.1400.1407.
ReferenceMaia, Zoghbi, et al., 2002Zoghbi, Andrade, et al., 2002Zoghbi, Andrade, et al., 2002, 2Dabiri and Sefidkon, 2001Dabiri and Sefidkon, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5Optima-5RSL-200RTX-1DB-5
Column length (m) 30.30.30.30.60.
Carrier gas N2HeH2N2He
Substrate      
Column diameter (mm) 0.250.20.320.250.25
Phase thickness (μm) 0.25 0.250.25 
Tstart (C) 60.50.40.60.50.
Tend (C) 220.250.280.300.250.
Heat rate (K/min) 5.3.6.4.3.
Initial hold (min) 10.3.5. 5.
Final hold (min)   5.  
I 1409.1410.1408.1411.1409.
ReferenceGallori, Flamini, et al., 2001Jacquemond-Collet, Bessière, et al., 2001Jirovetz L., Buchbauer G., et al., 2001Kalemba, Marschall, et al., 2001Rousis, Papadogianni, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-1CP Sil 5 CBDB-5DB-5
Column length (m) 25.60.25.30.30.
Carrier gas N2N2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm)  0.25 0.250.25
Tstart (C) 50.75.50.40.40.
Tend (C) 200.220.230.250.220.
Heat rate (K/min) 5.4.3.2.4.
Initial hold (min)  1. 5.5.
Final hold (min)  8. 60. 
I 1411.1388.1399.1416.1406.
ReferenceAyedoun, Adéoti, et al., 1999Bailac, Dellacasa, et al., 1999Oyedeji, Olawore, et al., 1999Porta, Porcedda, et al., 1999Sefidkon and Khajavi, 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5CBP-1HP-1OV-101
Column length (m) 30.30.30.60.25.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.25 0.25 
Tstart (C) 60.60.60.50.50.
Tend (C) 240.240.240.280.200.
Heat rate (K/min) 3.3.4.4.5.
Initial hold (min)    5. 
Final hold (min)      
I 1410.1411.1410.1422.1411.
ReferenceZoghbi, Andrade, et al., 1999El-Sakhawy, El-Tantawy, et al., 1998Lamarque, Maestri, et al., 1998Stashenko, Cervantes, et al., 1998Zollo, Biyiti, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5CBP-1OV-1SE-54
Column length (m)  30.25.50.30.
Carrier gas  HeHeN2Hydrogen
Substrate      
Column diameter (mm)  0.250.220.270.25
Phase thickness (μm)    0.20.25
Tstart (C) 80.60.60.80.60.
Tend (C) 220.240.240.240.250.
Heat rate (K/min) 6.4.5.3.2.
Initial hold (min)     5.
Final hold (min)     2.
I 1400.1403.1410.1406.1402.
ReferenceSalgueiro, Vila, et al., 1997Zunino, Novillo-Newton, et al., 1997Zygadlo, Ariza-Espinar, et al., 1997Ramanoelina, Viano, et al., 1994Kollmannsberger, Nitz, et al., 1992
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1BP-1DB-1DB-1
Column length (m) 60.60.50.60.60.
Carrier gas   H2HeHe
Substrate      
Column diameter (mm) 0.320.320.300.320.32
Phase thickness (μm)      
Tstart (C) 50.50.40.30.30.
Tend (C) 230.250.250.210.210.
Heat rate (K/min) 4.4.10.2.2.
Initial hold (min)  0.11.4.4.
Final hold (min) 10.5.   
I 1407.1407.1414.1399.1401.
ReferenceBinder, Benson, et al., 1990Binder and Flath, 1989Brophy, Davies, et al., 1989Takeoka and Butter, 1989Takeoka and Butter, 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase SE-30OV-101SE-30
Column length (m) 30.50.30.
Carrier gas    
Substrate    
Column diameter (mm)  0.30 
Phase thickness (μm)    
Tstart (C) 50.40.50.
Tend (C) 240.230.240.
Heat rate (K/min) 4.3.54.
Initial hold (min) 2.5.2.
Final hold (min) 10. 10.
I 1400.1408.1400.
ReferenceRamaswami, Briscese, et al., 1988Nykanen, 1986Ramaswami, Briscese, et al., 1986
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Sardashti, Valizadeh, et al., 2013
Sardashti, A.R.; Valizadeh, J.; Adhami, Y., Variations in the essential oil composition of Peroskia abrotonolides of different growth stage in Baluchestan, Middle-East J. Sci. Res., 2013, 13, 6, 781-784. [all data]

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Safaei-Ghomi, J.; Batooli, H., Determination of bioactive molecules from flowers, leaves, stems and roots of Perovskia abrotanoides Karel growing in central Iran by nano scale injection, Digest J. Nanomaterials Biostructures, 2010, 5, 2, 551-556. [all data]

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Notes

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