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2-Cyclopenten-1-one, 3-methyl-2-(2-pentenyl)-, (Z)-


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5 MSDB-5 MSHP-5 MSDB-1-MS
Column length (m) 60.30.25.30.60.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.300.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.50.50.70.30.
Tend (C) 250.180.240.290.200.
Heat rate (K/min) 3.2.3.5.2.
Initial hold (min) 1.   4.
Final hold (min) 20.  10.35.
I 1369.1392.1394.1398.1361.
ReferenceSardashti, Valizadeh, et al., 2013Phungpanya, Thongpoon, et al., 2012Chalchat, Figueredo, et al., 2010Radulovic, Blagojevic, et al., 2010Takeoka, Hobbs, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5 MSHP-5 MSDBP-5DBP-5
Column length (m) 30.30.30.25.25.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.220.22
Tstart (C) 50.50.50.40.40.
Tend (C) 250.280.240.250.250.
Heat rate (K/min) 7.4.3.3.3.
Initial hold (min) 1.  1.1.
Final hold (min) 5.  10.10.
I 1406.1399.1430.1367.1367.
ReferenceZouari, Zouari, et al., 2010Zhao, Zeng, et al., 2009Sarikurkcu, Tepe, et al., 2008Heravi and Sereshti, 2007Sereshti and Samadi, 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5HP-101DB-5HP-5
Column length (m) 30.30.25.30.30.
Carrier gas HeliumHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (mum) 0.250.250.20.250.25
Tstart (C) 60.50.70.40.50.
Tend (C) 280.300.200.240.300.
Heat rate (K/min) 3.5.3.4.5.
Initial hold (min)  5.2. 5.
Final hold (min)  5.15. 5.
I 1393.1394.1382.1392.1394.
ReferenceVagionas, Graikou, et al., 2007Figuérédo, Cabassu, et al., 2006Mastelic, Jerkovic, et al., 2006Sefidkon and Jamzad, 2006Figuérédo, Cabassu, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5HP-5MSHP-5MSDB-5
Column length (m) 30.30.30.30.25.
Carrier gas HeHeHeHeNitrogen
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (mum)   0.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 240.240.275.280.240.
Heat rate (K/min) 3.5.4.3.3.
Initial hold (min)    5. 
Final hold (min)      
I 1392.1374.1399.1400.1394.
ReferenceKhayyat and Karimi, 2005Saeidnia, Gohari, et al., 2005Sajjadi and Ghannadi, 2005Setzer, Noletto, et al., 2005JAvidnia, Mojab, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase ZB-5DB-5HP-5MSHP-5MSHP-5MS
Column length (m) 60.60.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.40.60.60.60.
Tend (C) 260.280.280.280.275.
Heat rate (K/min) 6.4.4.4.4.
Initial hold (min) 4.64.   
Final hold (min) 1.    
I 1415.1395.1393.1396.1394.
ReferenceJürgens and Dötterl, 2004Kalvandi, Sefidkon, et al., 2004Sadeghpour, Asghari, et al., 2004Sajjadi and Shahpiri, 2004Afsharypuor and Jahromy, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-1RTX-1DB-1
Column length (m) 50.50.60.30.60.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.20.20.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.50.40.60.50.
Tend (C) 220.220.280.300.270.
Heat rate (K/min) 3.3.4.4.4.
Initial hold (min) 2.2.5.  
Final hold (min) 10.    
I 1403.1399.1363.1373.1360.
ReferenceJuteau, Jerkovic, et al., 2003Masotti, Juteau, et al., 2003Sefidkon, Jalili, et al., 2002Kalemba, Marschall, et al., 2001Mirza, Ahmadi, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5OV-101DB-1DB-5DB-5
Column length (m) 30.50.60.30.30.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (mum) 0.25 0.250.250.25
Tstart (C) 60.80.50.60.60.
Tend (C) 240.200.220.240.240.
Heat rate (K/min) 3.1.4.3.3.
Initial hold (min)      
Final hold (min)  20.   
I 1394.1378.1377.1394.1394.
ReferenceTellez M., Estell R., et al., 2001Menon, Chacko, et al., 1999Sefidkon and Mirza, 1999Tellez, Canel, et al., 1999El-Sakhawy, El-Tantawy, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase DB-5DB-1
Column length (m) 30.60.
Carrier gas Helium 
Substrate   
Column diameter (mm) 0.250.32
Phase thickness (mum) 0.25 
Tstart (C) 60.50.
Tend (C) 240.250.
Heat rate (K/min) 3.4.
Initial hold (min)  0.1
Final hold (min)  5.
I 1394.1362.
ReferenceTellez, Estell, et al., 1997Flath, Mon, et al., 1983
Comment MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Sardashti, Valizadeh, et al., 2013
Sardashti, A.R.; Valizadeh, J.; Adhami, Y., Variations in the essential oil composition of Peroskia abrotonolides of different growth stage in Baluchestan, Middle-East J. Sci. Res., 2013, 13, 6, 781-784. [all data]

Phungpanya, Thongpoon, et al., 2012
Phungpanya, C.; Thongpoon, C.; Pripdeevech, P.; Machan, T., Analysis of aroma volatiles from fresh leaves of Plectranthus amboinicus using solid phase microextraction (SPME) technique, Pure and Applied Chemistry International Conference 2012 (PACCON 2012), 2012, 16701672. [all data]

Chalchat, Figueredo, et al., 2010
Chalchat, J.-C.; Figueredo, G.; Ozcan, M.M.; Unver, A., Effect of hydrodistillation and microwave distillation extraction methods on chemical composition of essential oil of pickling herb and myrtle plants, South Western J. of Agriculture, 2010, 1, 2, 133-141. [all data]

Radulovic, Blagojevic, et al., 2010
Radulovic, N.; Blagojevic, P.; Palic, R., Comparative study of the leaf volatiles of Arctostaphylos uva-ursi (L.) Spreng. and Vaccinium vitis-idaea L. (Ericaceae), Molecules, 2010, 15, 9, 6168-6185, https://doi.org/10.3390/molecules15096168 . [all data]

Takeoka, Hobbs, et al., 2010
Takeoka, G.R.; Hobbs, C.; Byeoung-Soo, P., Volatile constituents of the aerial parts of Salvia apiana Jepson, J. Essential Oil. Res., 2010, 22, 3, 241-244, https://doi.org/10.1080/10412905.2010.9700314 . [all data]

Zouari, Zouari, et al., 2010
Zouari, S.; Zouari, N.; Fakhfakh, N.; Bougatel, A.; Ayadi, M.A.; Neffati, M., Chemical composition and biological activities of a new essential oil chemotype of Tunisian Artemisia herba alba Asso, J. Medicinal Plants Res., 2010, 4, 10, 871-880. [all data]

Zhao, Zeng, et al., 2009
Zhao, C.; Zeng, Y.; Wan, M.; Li, R.; Liang, Y.; Li, C.; Zeng, Z.; Chau, F.-T., Comparative analysis of essential oils from eight herbal medicines with pungent flavor and cool nature by GC-MS and chemometric resolution methods, J. Sep. Sci., 2009, 32, 4, 660-670, https://doi.org/10.1002/jssc.200800484 . [all data]

Sarikurkcu, Tepe, et al., 2008
Sarikurkcu, C.; Tepe, B.; Daferera, D.; Polissiou, M.; Harmandar, M., Studies on the anioxidant activity of the essential oil and methanol extract of Marrubium globosum subsp. globosum (lamiaceae) by three different chemical assays, Bioresource Technol., 2008, 99, 10, 4239-4246, https://doi.org/10.1016/j.biortech.2007.08.058 . [all data]

Heravi and Sereshti, 2007
Heravi, M.J.; Sereshti, H., Determination of Essential Oil Components of Artemisia haussknechtii Boiss. using Simultaneous Hydrodistillation-Static Headspace Liquid Phase Microextraction - Gas Chromatography Mass Spectrometry, J. Chromatogr. A, 2007, 1160, 1-2, 81-89, https://doi.org/10.1016/j.chroma.2007.05.096 . [all data]

Sereshti and Samadi, 2007
Sereshti, H.; Samadi, S., Comparison of hydrodistillation-headspace liquid phase microextraction techniques with hydrodistillation in determination of essential oils in Artemisia Haussknechtii Boiss, JSUT, 2007, 33, 2, 7-17. [all data]

Vagionas, Graikou, et al., 2007
Vagionas, K.; Graikou, K.; Ngassapa, O.; Runyoro, D.; Chinou, I., Composition and antimicrobial activity of the essential oils of three Satureja species growing in Tansania, Food Chem., 2007, 103, 2, 319-324, https://doi.org/10.1016/j.foodchem.2006.07.051 . [all data]

Figuérédo, Cabassu, et al., 2006
Figuérédo, G.; Cabassu, P.; Chalchat, J.-C.; Pasquier, B., Studies of Mediterranean oregano populations. VIII. Chemical composition of essential oils of oreganos of various origins, Flavour Fragr. J., 2006, 21, 1, 134-139, https://doi.org/10.1002/ffj.1543 . [all data]

Mastelic, Jerkovic, et al., 2006
Mastelic, J.; Jerkovic, I.; Mesic, M., Volatile constituents from flowers, leaves, bark and wood of Prunus mahaleb L., Flavour Fragr. J., 2006, 21, 2, 306-313, https://doi.org/10.1002/ffj.1596 . [all data]

Sefidkon and Jamzad, 2006
Sefidkon, F.; Jamzad, Z., Chemical composition of the essential oil of Gontscharovia popovii from Iran, Flavour Fragr. J., 2006, 21, 4, 619-621, https://doi.org/10.1002/ffj.1628 . [all data]

Figuérédo, Cabassu, et al., 2005
Figuérédo, G.; Cabassu, P.; Chalchat, J.-C.; Pasquier, B., Studies of Mediterranean oregano populations- V. Chemical composition of essential oils of oregano: Origanum syriacum L. var. bevanii (Holmes) Ietswaart, O. syriacum L. var. sinaicum (Boiss.) Ietswaart, and O. syriacum L. var. syriacum from Lebanon and Israel, Flavour Fragr. J., 2005, 20, 164-168. [all data]

Khayyat and Karimi, 2005
Khayyat, M.H.; Karimi, H., Composition of the volatile oils of three different species of Artemisia, Iranian Journal of Pharmaceutical Sciences, 2005, 1, 1, 29-32. [all data]

Saeidnia, Gohari, et al., 2005
Saeidnia, S.; Gohari, A.R.; Yassa, N.; Shafiee, A., Composition of the volatile oil of Achillea conferta DC. from Iran, DARU, 2005, 13, 1, 34-36. [all data]

Sajjadi and Ghannadi, 2005
Sajjadi, S.-E.; Ghannadi, A., Essential oil of the Persian sage, Salvia rhytidea Benth., Acta Pharm. Sin., 2005, 55, 321-326. [all data]

Setzer, Noletto, et al., 2005
Setzer, W.N.; Noletto, J.A.; Lawton, R.O.; Haber, W.A., Leaf essential oil composition of five Zanthoxylum species from Monteverde, Costa Rica, Molecular Diversity, 2005, 9, 1-3, 3-13, https://doi.org/10.1007/s11030-005-1298-6 . [all data]

JAvidnia, Mojab, et al., 2004
JAvidnia, K.; Mojab, F.; Mojahedi, S.A., Chemical constituents of the essential oil of Stachys lavandulifolia Vahl from Iran, Iranian J. Pharm. Res., 2004, 3, 61-63. [all data]

Jürgens and Dötterl, 2004
Jürgens, A.; Dötterl, S., Chemical composition of anther volatiles in Ranunculaceae: genera-specific profiles in Aemone, Aquilegia, Caltha, Pulsatilla, Ranunculus, and Trollius species, American Journal of Botany, 2004, 91, 12, 1969-1980, https://doi.org/10.3732/ajb.91.12.1969 . [all data]

Kalvandi, Sefidkon, et al., 2004
Kalvandi, R.; Sefidkon, F.; Atri, M.; Mirza, M., Analysis of the essential oil of Thymus eriocalyx from Iran, Flavour Fragr. J., 2004, 19, 4, 341-343, https://doi.org/10.1002/ffj.1312 . [all data]

Sadeghpour, Asghari, et al., 2004
Sadeghpour, O.; Asghari, G.; Ardekani, M.R.S., Composition of essential oil of Artemisia persica Boiss. from Iran, Iran. J. Pharm. Res., 2004, 3, 65-67. [all data]

Sajjadi and Shahpiri, 2004
Sajjadi, S.E.; Shahpiri, Z., Chemical composition of the essential oil of Salvia limbata C.A.Mey, DARU, 2004, 12, 3, 94-97. [all data]

Afsharypuor and Jahromy, 2003
Afsharypuor, S.; Jahromy, M.M., Constituents of the essential oil from Tanacetum lingulatum (Boiss.) Bornm., J. Essent. Oil Res., 2003, 15, 2, 74-76, https://doi.org/10.1080/10412905.2003.9712069 . [all data]

Juteau, Jerkovic, et al., 2003
Juteau, F.; Jerkovic, I.; Masotti, V.; Milos, M.; Mastelic, J.; Bessière, J.-M.; Viano, J., Composition and antimicrobial activity of the essential oil of Artemisia absinthium from Croatia and France, Planta Medica, 2003, 69, 2, 158-161, https://doi.org/10.1055/s-2003-37714 . [all data]

Masotti, Juteau, et al., 2003
Masotti, V.; Juteau, F.; Bessière, J.M.; Viano, J., Seasonal and phenological variations of the essential oil from the narrow endemic species Artemisia molinieri and its biological activities, J. Agric. Food Chem., 2003, 51, 24, 7115-7121, https://doi.org/10.1021/jf034621y . [all data]

Sefidkon, Jalili, et al., 2002
Sefidkon, F.; Jalili, A.; Mirhaji, T., Essential oil composition of three Artemisia spp. from Iran, Flavour Fragr. J., 2002, 17, 2, 150-152, https://doi.org/10.1002/ffj.1063 . [all data]

Kalemba, Marschall, et al., 2001
Kalemba, D.; Marschall, H.; Bradesi, P., Constituents of the essential oil of Solidago gigantea Ait. (giant goldenrod), Flavour Fragr. J., 2001, 16, 1, 19-26, https://doi.org/10.1002/1099-1026(200101/02)16:1<19::AID-FFJ940>3.0.CO;2-U . [all data]

Mirza, Ahmadi, et al., 2001
Mirza, M.; Ahmadi, L.; Tayebi, M., Volatile constituents of Hymenocrater incanus Bunge, an Iranian endemic species, Flavour Fragr. J., 2001, 16, 4, 239-240, https://doi.org/10.1002/ffj.983 . [all data]

Tellez M., Estell R., et al., 2001
Tellez M.; Estell R.; Fredrickson E.; Powell J.; Wedge D.; Schrader K.; Kobaisy M., Extracts of Flourensia cernua (L): Volatile constituents and antifungal, antialgal, and antitermite bioactivities, J. Chem. Ecol., 2001, 27, 11, 2263-2273, https://doi.org/10.1023/A:1012283005014 . [all data]

Menon, Chacko, et al., 1999
Menon, A.N.; Chacko, S.; Narayanan, C.S., Free and glycosidically bound volatiles of cardamom (Eletteria cardamomum Maton var. miniscula Burkill), Flavour Fragr. J., 1999, 14, 1, 65-68, https://doi.org/10.1002/(SICI)1099-1026(199901/02)14:1<65::AID-FFJ789>3.0.CO;2-A . [all data]

Sefidkon and Mirza, 1999
Sefidkon, F.; Mirza, M., Chemical composition of the essential oils of two Salvia species from Iran, Salvia virgata Jacq. and Salvia syriaca L., Flavour Fragr. J., 1999, 14, 1, 45-46, https://doi.org/10.1002/(SICI)1099-1026(199901/02)14:1<45::AID-FFJ774>3.0.CO;2-S . [all data]

Tellez, Canel, et al., 1999
Tellez, M.R.; Canel, C.; Rimando, A.M.; Duke, S.O., Differential accumulation of isoprenoids in glanded and glandless Artemisia annua L, Phytochemistry, 1999, 52, 6, 1035-1040, https://doi.org/10.1016/S0031-9422(99)00308-8 . [all data]

El-Sakhawy, El-Tantawy, et al., 1998
El-Sakhawy, F.S.; El-Tantawy, M.E.; Ross, S.A.; El-Sohly, M.A., Composition and antimicrobial activity of the essential oil of Murraya exotica L., Flavour Fragr. J., 1998, 13, 1, 59-62, https://doi.org/10.1002/(SICI)1099-1026(199801/02)13:1<59::AID-FFJ693>3.0.CO;2-L . [all data]

Tellez, Estell, et al., 1997
Tellez, M.R.; Estell, R.E.; Frederickson, E.L.; Havstad, K.M., Essntial oil of Flourensia cernua DC, J. Essent. Oil Res., 1997, 9, 6, 619-624, https://doi.org/10.1080/10412905.1997.9700799 . [all data]

Flath, Mon, et al., 1983
Flath, R.A.; Mon, T.R.; Lorenz, G.; Whitten, C.J.; Mackley, J.W., Volatile components of Acacia sp. blossoms, J. Agric. Food Chem., 1983, 31, 6, 1167-1170, https://doi.org/10.1021/jf00120a008 . [all data]


Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References