1,3-Benzodioxole, 4,5-dimethoxy-6-(2-propenyl)-


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Optima-5DB-5HP-5HP-5MSBPX-5
Column length (m) 30.30.30.30.50.
Carrier gas HeliumNitrogenHeliumHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.22
Phase thickness (μm) 0.250.250.320.251.
Tstart (C) 60.40.60.60.50.
Tend (C) 246.250.250.250.300.
Heat rate (K/min) 3.3.5.2.4.
Initial hold (min) 1.1.30.8.1.
Final hold (min)  10. 15.10.
I 1625.1620.1620.1622.1662.
ReferenceAl-Qudah, Muhaidat, et al., 2012Rahimi-Nasrabadi, Gholivand, et al., 2009Yassa and Akhani, 2008Ferhat, Meklati, et al., 2007Rali, Wossa, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5DB-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeN2N2HeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.320.250.250.250.25
Tstart (C) 60.50.50.60.40.
Tend (C) 250.280.280.260.240.
Heat rate (K/min) 5.9.9.3.4.
Initial hold (min) 30.3.3.  
Final hold (min)  3.3. 5.
I 1620.1586.1608.1625.1611.
ReferenceYassa and Akhani, 2007Abdelwahed, Hayder, et al., 2006Abdelwahed, Hayder, et al., 2006Javidnia, Miri, et al., 2006Miyazawa and Kawata, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBHP-5MSDB-5HP-5MSMethyl Silicone
Column length (m) 30.30.30.30.60.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.32 0.250.25
Tstart (C) 60.60.40.60.60.
Tend (C) 250.250.240.280.200.
Heat rate (K/min) 5.5.4.3.4.
Initial hold (min)  3. 5.1.
Final hold (min) 10.   20.
I 1603.1634.1620.1625.1620.
ReferenceJassbi, Mehrdad, et al., 2005Pourmortazavi, Ghadiri, et al., 2005Sefidkon and Jamzad, 2005Setzer, Noletto, et al., 2005Rojas, Usubillaga, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSRSL-200DB-5MSDB-1HP-5
Column length (m) 30.30.30.50.30.
Carrier gas HeliumH2HeN2He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.32
Tstart (C) 60.40.60.90.60.
Tend (C) 200.280.240.240.250.
Heat rate (K/min) 4.6.3.4.5.
Initial hold (min) 1.2.  30.
Final hold (min) 20.10.   
I 1620.1602.1624.1582.1628.
ReferenceRoyas, Usubillaga, et al., 2004Jirovetz, Buchbauer, et al., 2003Maia, Taveira, et al., 2003Velasco-Negueruela, Pérez-Alonso, et al., 2003Yassa, Akhani, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5RSL-200DB-5DB-5MSDB-1
Column length (m) 30.30.30.30.30.
Carrier gas HeH2HeHeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.40.60.60.40.
Tend (C) 240.280.240.270.260.
Heat rate (K/min) 3.6.3.3.2.
Initial hold (min)  5.  5.
Final hold (min)  5.  2.
I 1620.1608.1625.1622.1597.
ReferenceZoghbi, Andrade, et al., 2003Jirovetz, Buchbauer, et al., 2002Maia, da Silva, et al., 2002Zoghbi, Andrade, et al., 2002Senatore, Napolitano, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase OV-101DB-5MSDB-5
Column length (m) 50.30.30.
Carrier gas HeHeHe
Substrate    
Column diameter (mm) 0.250.250.25
Phase thickness (μm) 0.250.250.25
Tstart (C) 70.60.60.
Tend (C) 220.240.240.
Heat rate (K/min) 2.3.3.
Initial hold (min) 5.  
Final hold (min)    
I 1595.1624.1628.
ReferencePateira, Nogueira, et al., 1999Zoghbi, Andrade, et al., 1999Maia, Zohhbi, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Al-Qudah, Muhaidat, et al., 2012
Al-Qudah, M.A.; Muhaidat, R.; Trawenh, I.N.; Jaber, H.I.; Abu Zarga, M.H.; Abu Orabi, S.T., Volatile constituents of leaves and bulbs of Gynandriris Sisyrinchicum and their antimicrobial activities, Jordan J. Chem., 2012, 7, 3, 287-295. [all data]

Rahimi-Nasrabadi, Gholivand, et al., 2009
Rahimi-Nasrabadi, M.; Gholivand, M.B.; Batooli, H.; Vatanara, A., Chemical composition of the essential oil from leaves and flowering aerial parts of Psammogeton canscens (DC). Vake from Iran, J. Medicinal Plants, 2009, 8, 31, 82-86. [all data]

Yassa and Akhani, 2008
Yassa, N.; Akhani, H., The essential oils composition in two species of the genus Eriocycla Lindl. (Apiaceae) from Iran, 2008, retrieved from http://biology.ut.ac.ir/members/akhani/PdfReprintNumber/27.pdf. [all data]

Ferhat, Meklati, et al., 2007
Ferhat, M.A.; Meklati, B.Y.; Chemat, F., Comparison of different isolation methods of essential oil from Citrus fruits: cold pressing, hydrodistillation and microwave dry distillation, Flavour Fragr. J., 2007, 22, 6, 494-504, https://doi.org/10.1002/ffj.1829 . [all data]

Rali, Wossa, et al., 2007
Rali, T.; Wossa, S.W.; Leach, D.N.; Waterman, P.G., Volatile chemical constituents of Piper aduncum L and Piper gibbilimbum C. DC (Piperaceae) from Papua New Guinea, Molecules, 2007, 12, 3, 389-394, https://doi.org/10.3390/12030389 . [all data]

Yassa and Akhani, 2007
Yassa, N.; Akhani, H., The essential oils composition in two species of the genus Eriocycla Lindl. (Apiaceae) from Iran, 2007, retrieved from http://biology.ut.ac.ir/members/akhani/PdfReprintNumber/27.pdf. [all data]

Abdelwahed, Hayder, et al., 2006
Abdelwahed, A.; Hayder, N.; Kilani, S.; Mahmoud, A.; Chibani, J.; Hammami, M.; Chekir-Ghedira, L.; Ghedira, K., Chemical composition and antimicrobial activity of essential oils from Tunisian Pituranthos tortuosus (Coss.) Maire, Flavour Fragr. J., 2006, 21, 1, 129-133, https://doi.org/10.1002/ffj.1542 . [all data]

Javidnia, Miri, et al., 2006
Javidnia, K.; Miri, R.; Kamalinejad, M.; Mehdipour, A.R., Composition of the essential oil of Diplotaenia cachrydifolia Boiss. from Iran, J. Ess. Oil Res., 2006, 18, 1, 86-87, https://doi.org/10.1080/10412905.2006.9699393 . [all data]

Miyazawa and Kawata, 2006
Miyazawa, M.; Kawata, J., Identification of the Key Aroma Compounds in Dried Roots of Rubia cordifolia, L. Oleo Sci., 2006, 55, 1, 37-39, https://doi.org/10.5650/jos.55.37 . [all data]

Jassbi, Mehrdad, et al., 2005
Jassbi, A.R.; Mehrdad, M.; Soleimani, M.; Mirzaeian, M.; Sonboli, A., Chemical composition of the essential oils of Bunium elegans and Bunium caroides, Chem. Nat. Compd. (Engl. Transl.), 2005, 41, 4, 415-417, https://doi.org/10.1007/s10600-005-0165-0 . [all data]

Pourmortazavi, Ghadiri, et al., 2005
Pourmortazavi, S.M.; Ghadiri, M.; Hajimirsadeghi, S.S., Supercritical fluid extraction of volatile components from Bunium persicum Boiss. (black cumin) and Mespilus germanica L. (medlar) seeds, J. Food Comp. Anal., 2005, 18, 5, 439-446, https://doi.org/10.1016/j.jfca.2004.01.003 . [all data]

Sefidkon and Jamzad, 2005
Sefidkon, F.; Jamzad, Z., Chemical composition of the essential oil of three Iranian Satureja species (S. mutica, S. macrantha and S. intermedia), Food Chem., 2005, 91, 1, 1-4, https://doi.org/10.1016/j.foodchem.2004.01.027 . [all data]

Setzer, Noletto, et al., 2005
Setzer, W.N.; Noletto, J.A.; Lawton, R.O.; Haber, W.A., Leaf essential oil composition of five Zanthoxylum species from Monteverde, Costa Rica, Molecular Diversity, 2005, 9, 1-3, 3-13, https://doi.org/10.1007/s11030-005-1298-6 . [all data]

Rojas, Usubillaga, et al., 2004
Rojas, L.B.; Usubillaga, A.; Cegarra, J.A.; Borregales, E.; Carrero, Y., Composición Química y actividad antimicótica de el aceite Esenchial ede la Lepechinia schiedeane (Schlecht) vatke, Rev. Fac. Farm., 2004, 46, 1, 27-30. [all data]

Royas, Usubillaga, et al., 2004
Royas, L.B.; Usubillaga, A.; Cegarra, J.A.; Borreagales, E.; Carrero, S., Composicion Quimica y Actividad Antimicotica de el Aceite Esensial de la Lepechinia schiedeana (Schlecht) Vatke, Revista de la Facultad de Farmacia, 2004, 46, 1, 27-30. [all data]

Jirovetz, Buchbauer, et al., 2003
Jirovetz, L.; Buchbauer, G.; Stoyanova, A.S.; Georgiev, E.V.; Damianova, S.T., Composition, quality control, and antimicrobial activity of the essential oil of long-time stored dill (Anethum graveolens L.) seeds from Bulgaria, J. Agric. Food Chem., 2003, 51, 13, 3854-3857, https://doi.org/10.1021/jf030004y . [all data]

Maia, Taveira, et al., 2003
Maia, J.G.S.; Taveira, F.S.N.; Andrade, E.H.A.; da Silva, M.H.L.; Zoghbi, M.G.B., Essential oils of Lippia grandis Schau., Flavour Fragr. J., 2003, 18, 5, 417-420, https://doi.org/10.1002/ffj.1241 . [all data]

Velasco-Negueruela, Pérez-Alonso, et al., 2003
Velasco-Negueruela, A.; Pérez-Alonso, M.J.; Pérez de Paz, P.L.; Palá-Paúl, J.; Sanz, J., Analysis by gas chromatography-mass spectrometry of the essential oils from the aerial parts of Rutheopsis herbanica (Bolle) Hans. Kunk., gathered in Fuerteventura (Canary Islands), J. Chromatogr. A, 2003, 984, 1, 159-162, https://doi.org/10.1016/S0021-9673(02)01742-9 . [all data]

Yassa, Akhani, et al., 2003
Yassa, N.; Akhani, H.; Aqaahmadi, M.; Salimian, M., Essential oils from two endemic species of Apiaceae from Iran, Z. Naturforsch. C:, 2003, 58, 459-463. [all data]

Zoghbi, Andrade, et al., 2003
Zoghbi, M.G.B.; Andrade, E.H.A.; da Silva, M.H.; Carreira, L.M.M.; Maia, J.G.S., Essential oils from three Myrcia species, Flavour Fragr. J., 2003, 18, 5, 421-424, https://doi.org/10.1002/ffj.1242 . [all data]

Jirovetz, Buchbauer, et al., 2002
Jirovetz, L.; Buchbauer, G.; Ngassoum, M.B.; Geissler, M., Aroma compound analysis of Piper nigrum and Piper guineense essential oils from Cameroon using solid-phase microextraction-gas chromatography, solid-phase microextraction-gas chromatography-mass spectrometry and olfactometry, J. Chromatogr. A, 2002, 976, 1-2, 265-275, https://doi.org/10.1016/S0021-9673(02)00376-X . [all data]

Maia, da Silva, et al., 2002
Maia, J.G.S.; da Silva, M.H.L.; Andrade, E.H.A.; Zoghbi, M.G.B.; Carreira, L.M.M., Essential oils from Astronium urundeuva (Allemao) Engl. and A. fraxinifolium Schott ex Spreng., Flavour Fragr. J., 2002, 17, 1, 72-74, https://doi.org/10.1002/ffj.1046 . [all data]

Zoghbi, Andrade, et al., 2002
Zoghbi, M.G.B.; Andrade, E.H.A.; Maia, J.G.S., Volatile constituents from Adenocalymma alliaceum Miers and Petiveria alliacea L., two medicinal herbs of the Amazon, Flavour Fragr. J., 2002, 17, 2, 133-135, https://doi.org/10.1002/ffj.1051 . [all data]

Senatore, Napolitano, et al., 2000
Senatore, F.; Napolitano, F.; Ozcan, M., Composition and antibacterial activity of the essential oil from Crithmum maritimum L. (Apiaceae) growing wild in Turkey, Flavour Fragr. J., 2000, 15, 3, 186-189, https://doi.org/10.1002/1099-1026(200005/06)15:3<186::AID-FFJ889>3.0.CO;2-I . [all data]

Pateira, Nogueira, et al., 1999
Pateira, L.; Nogueira, T.; Antunes, A.; Venancio, F.; Tavares, R.; Capelo, J., Two chemotypes of Crithmum maritimum L. from Portugal, Flavour Fragr. J., 1999, 14, 5, 333-343, https://doi.org/10.1002/(SICI)1099-1026(199909/10)14:5<333::AID-FFJ839>3.0.CO;2-V . [all data]

Zoghbi, Andrade, et al., 1999
Zoghbi, M.G.B.; Andrade, E.H.A.; Maia, J.G.S., Volatile constituents from leaves and flowers of Alpinia speciosa K. Schum. and A. purpurata (Viell.) Schum., Flavour Fragr. J., 1999, 14, 6, 411-414, https://doi.org/10.1002/(SICI)1099-1026(199911/12)14:6<411::AID-FFJ854>3.0.CO;2-U . [all data]

Maia, Zohhbi, et al., 1998
Maia, J.G.S.; Zohhbi, M.G.B.; Andrade, E.H.A.; Santos, A.S.; da Silva, M.H.L.; Luz, A.I.R.; Bastos, C.N., Constituents of the essential oil of Piper aduncum L. growing wild in the Amazon region, Flavour Fragr. J., 1998, 13, 4, 269-272, https://doi.org/10.1002/(SICI)1099-1026(1998070)13:4<269::AID-FFJ744>3.0.CO;2-A . [all data]


Notes

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