Naphthalene, 1,2,3,5,6,8a-hexahydro-4,7-dimethyl-1-(1-methylethyl)-, (1S-cis)-

Formula: C₁₅H₂₄
Molecular weight: 204.3511
IUPAC Standard InChI: InChI=1S/C15H24/c1-10(2)13-8-6-12(4)14-7-5-11(3)9-15(13)14/h9-10,13,15H,5-8H2,1-4H3/t13-,15+/m1/s1
IUPAC Standard InChIKey: FUCYIEXQVQJBKY-HIFRSBDPSA-N
CAS Registry Number: 483-76-1
Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript.
Stereoisomers:
Other names: Cadina-1(10),4-diene; δ-Cadinene, (+)-; (+)-δ-Cadinene; δ-Cadinene; [1S,cis]-Naphthalene,1,2,3,5,6,8a-hexahydro-4,7-dimethyl-1-[1-methylethyl]; (1S,8aR)-1-Isopropyl-4,7-dimethyl-1,2,3,5,6,8a-hexahydronaphthalene; 1,2,3,5,6,8a-Hexahydro-4,7-dimethyl-1-(1-methylethyl)naphthalene
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Other data available:
- Mass spectrum (electron ionization)
- Gas Chromatography
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Normal alkane RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-5 MS	DB-5	HP-5 MS	RTX-1	RTX-1
Column length (m)	30.	30.	60.	60.	60.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.22	0.22
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	60.	60.	40.	60.	60.
T_end (C)	240.	240.	250.	230.	230.
Heat rate (K/min)	3.	3.	3.	2.	2.
Initial hold (min)			1.
Final hold (min)			20.	5.	5.
I	1531.	1523.	1498.	1520.	1520.
Reference	Pinheiro, de Queiros, et al., 2013	Rodriques, Amorim, et al., 2013	Sardashti, Valizadeh, et al., 2013	Bendiabdellah, El Amine Dib, et al., 2012	Bendiabdellah, El Amine Dib, et al., 2012
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5 MS	HP-5 MS	HP-5	HP-5
Column length (m)	30.	30.	30.	25.	25.
Carrier gas	Helium	Helium	Helium	Hydrogen	Hydrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.52	0.52
T_start (C)	100.	40.	50.	40.	40.
T_end (C)	260.	250.	180.	280.	280.
Heat rate (K/min)	10.	3.	2.	4.	4.
Initial hold (min)	1.	1.
Final hold (min)	10.	3.		10.	10.
I	1528.	1522.	1523.	1518.	1518.
Reference	Boukhris, Bouaziz, et al., 2012	Jian-Yu, Zhu, et al., 2012	Phungpanya, Thongpoon, et al., 2012	Velickovic, Ristic, et al., 2012	Velickovic, Ristic, et al., 2012
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5 MS	RTX-1	HP-5 MS	HP-5
Column length (m)	25.	30.	60.	30.	30.
Carrier gas	Hydrogen		Helium	Helium	Helium
Substrate
Column diameter (mm)	0.32	0.25	0.22	0.25	0.25
Phase thickness (μm)	0.52	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	60.	50.	60.
T_end (C)	280.	300.	230.	250.	240.
Heat rate (K/min)	4.	15.	2.	7.	3.
Initial hold (min)		2.		1.
Final hold (min)	10.	10.	45.	5.
I	1518.	1525.	1509.	1518.	1523.
Reference	Velickovic, Ristic, et al., 2012	Xu, Han, et al., 2012	Yapi, Boti, et al., 2012	Zouari, Ayadi, et al., 2012	Bertoli, Lepnardi, et al., 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5	DB-5	VF-5 MS	VF-5 MS
Column length (m)	30.	30.	30.	60.	60.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.32	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	30.	30.
T_end (C)	220.	240.	240.	260.	260.
Heat rate (K/min)	4.	3.	3.	2.	2.
Initial hold (min)	20.	2.
Final hold (min)	20.			28.	28.
I	1517.	1525.	1524.	1522.	1522.
Reference	Feizbakhsh and Naeemy, 2011	Kahriman, Tosun, et al., 2011	Karimi, Farmani, et al., 2011	Leffingwell and Alford, 2011	Leffingwell and Alford, 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-30 MS	CP-Sil 5 CB	DB-5	RTX-5	ZB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Nitrogen	Helium	Nitrogen	Nitrogen
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.32	0.25
Phase thickness (μm)	0.25	0.26	0.25	0.25	0.25
T_start (C)	50.	45.	50.	60.	40.
T_end (C)	250.	280.	300.	210.	200.
Heat rate (K/min)	5.	3.	4.	3.	5.
Initial hold (min)	5.		4.		5.
Final hold (min)	10.	22.	5.
I	1524.	1518.	1509.	1520.	1533.
Reference	Menichini, Tundis, et al., 2011	Mothana, Hasson, et al., 2011	Osorio, Carriazo, et al., 2011	Prasad, Moulekhi, et al., 2011	Vazques, Aimar, et al., 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	ZB-5	HP-5 MS	Elite-5 MS	HP-5	ZB-5 MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Nitrogen	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	30.	40.	50.	60.
T_end (C)	200.	250.	220.	300.	290.
Heat rate (K/min)	5.	5.	4.	50.	5.
Initial hold (min)	5.	3.		5.
Final hold (min)	5.	10.		5.
I	1533.	1559.	1496.	1520.	1519.
Reference	Vazquez, Demmel, et al., 2011	Zarai, Kadri, et al., 2011	Baharum, Bunawan, et al., 2010	Bi Kouame, Bedi, et al., 2010	Boix, Victorio, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	RTX-1	DB-5	SPB-1	BP-1
Column length (m)	30.	60.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Nitrogen
Substrate
Column diameter (mm)	0.252	0.22	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	50.	60.
T_end (C)	240.	230.	250.	250.	220.
Heat rate (K/min)	3.	2.	2.	5.	5.
Initial hold (min)				3.	10.
Final hold (min)		30.		15.	30.
I	1522.	1520.	1523.	1498.	1516.
Reference	Cavar, Maksimovic, et al., 2010	Dib, Djabou, et al., 2010	Ho, Wang, et al., 2010	Lazarevic, Palic, et al., 2010	Mishra, Chaudhary, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	HP-5 MS	HP-5 MS	HP-5 MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	50.	60.	60.	70.
T_end (C)	260.	240.	220.	220.	290.
Heat rate (K/min)	4.	3.	5.	5.	5.
Initial hold (min)		5.	10.	10.
Final hold (min)	5.				10.
I	1529.	1492.	1525.	1525.	1521.
Reference	Miyazawa, Kawauchi, et al., 2010	Monsef-Esfahani, Miri, et al., 2010	Ogunwande, Flamini, et al., 2010	Ogunwande, Flamini, et al., 2010	Radulovic, Blagojevic, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5 MS	HP-5 MS	SLB-5 MS	DB-5
Column length (m)	30.	30.	30.	10.	30.
Carrier gas	Hydrogen	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.10	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.10	0.25
T_start (C)	70.	70.	60.	50.	60.
T_end (C)	290.	290.	220.	250.	240.
Heat rate (K/min)	5.	5.	6.	10.	3.
Initial hold (min)			3.
Final hold (min)		10.
I	1532.	1521.	1516.	1522.	1525.
Reference	Radulovic, Dordevic, et al., 2010	Radulovic, Dordevic, et al., 2010, 2	Safaei-Ghomi and Batooli, 2010	Scandinaro, Tranchida, et al., 2010	Scherer, Wagner, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5 MS	DB-5	DB-1-MS	DB-5	DB-1
Column length (m)	30.	30.	60.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	40.	30.	80.	50.
T_end (C)	240.	240.	200.	240.	220.
Heat rate (K/min)	3.	3.	2.	3.	4.
Initial hold (min)		1.	4.		2.
Final hold (min)			35.	2.	2.
I	1516.	1510.	1507.	1526.	1510.
Reference	Silva, Pott, et al., 2010	de Souza, Lopes, et al., 2010	Takeoka, Hobbs, et al., 2010	Vahirua-Lechat, Mitermite, et al., 2010	Xu, Tang, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-54	SPB-5	DB-5	HP-5 MS	HP-5 MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Nitrogen	Helium	Hydrogen	Helium
Substrate
Column diameter (mm)	0.25	0.53	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.50	0.25	0.25	0.25
T_start (C)	60.	50.	50.	30.	35.
T_end (C)	260.	210.	250.	230.	195.
Heat rate (K/min)	2.	3.	5.	8.	2.
Initial hold (min)	5.	5.	2.	5.	5.
Final hold (min)	999.	45.		10.	30.
I	1518.	1531.	1523.	1539.	1519.
Reference	Dayisoylu and Alma, 2009	Gilani, Shah, et al., 2009	Ho, Wang, et al., 2009	Karlsson, Birgersson, et al., 2009	Kim and Chung, 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5 MS	VF-1 MS	RTX-1	RTX-1	BP-1
Column length (m)	30.	30.	60.	60.	50.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.22	0.22	0.22
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	60.	60.	60.
T_end (C)	250.	280.	230.	230.	220.
Heat rate (K/min)	2.	4.	2.	2.	2.
Initial hold (min)	5.	5.
Final hold (min)		10.	30.	30.	20.
I	1543.	1524.	1515.	1520.	1507.
Reference	Koba, Sanda, et al., 2009	Marchesini, Prada, et al., 2009	Museli, Pau, et al., 2009	Museli, Pau, et al., 2009	Ottavioli, Bighelli, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	5 % Phenyl methyl siloxane	DB-5	DB-5 MS	DB-5
Column length (m)	30.	60.	30.	30.	30.
Carrier gas	Helium	Helium	Nitrogen	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	45.	90.	40.	50.	40.
T_end (C)	250.	225.	230.	220.	240.
Heat rate (K/min)	3.	3.	2.	3.	3.
Initial hold (min)	3.			2.	1.
Final hold (min)	5.	3.		70.
I	1518.	1525.	1523.	1512.	1510.
Reference	Porto, Decorti, et al., 2009	Retta, Gattuso, et al., 2009	Scrivanti, Anton, et al., 2009	Shimizu, Imayoshi, et al., 2009	de Souza, Lopes, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5 MS	HP-5 MS	HP-5 MS	HP-5	HP-5 MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	50.	50.	60.
T_end (C)	250.	300.	280.	280.	280.
Heat rate (K/min)	4.	15.	4.	9.	3.
Initial hold (min)	2.	2.		3.
Final hold (min)	2.	10.		3.
I	1524.	1525.	1527.	1528.	1524.
Reference	Su, Wang, et al., 2009	Xu, Han, et al., 2009	Zhao, Zeng, et al., 2009	Aicha, Ines, et al., 2008	Baziou, Couladis, et al., 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	SE-52	HP-5 MS	HP-5	VF-5MS
Column length (m)	25.	50.	30.	30.	30.
Carrier gas	Nitrogen	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.22	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	50.	50.	240.
T_end (C)	300.	280.	230.	300.	320.
Heat rate (K/min)	6.5	3.	4.	3.	20.
Initial hold (min)	2.		4.		1.
Final hold (min)	7.	20.	10.	30.
I	1519.	1528.	1523.	1518.	1530.
Reference	Chieng, Assim, et al., 2008	Djarri, Medjroubi, et al., 2008	Forero, Quijano, et al., 2008	Isidorov, Lech, et al., 2008	Kowalski, 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SLB-5 MS	DB-5	DB-5 MS	RTX-1	Elite-1
Column length (m)	30.	60.	30.	60.	30.
Carrier gas	Helium	Nitrogen	Helium	He	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.22	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	50.	60.	60.
T_end (C)	250.	250.	300.	230.	246.
Heat rate (K/min)	3.	5.	5.	2.	3.
Initial hold (min)	2.		5.
Final hold (min)	10.	10.	5.	35.
I	1521.	1533.	1517.	1516.	1520.
Reference	Lo Presti, Sciarrone, et al., 2008	Mosayebi, Amin, et al., 2008	Noudogbessi, Yedomonhan, et al., 2008	Paolini, Tomi, et al., 2008	Raj, Baby, et al., 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SLB-5MS	HP-5 MS	BPX-5	RTX-5	HP-5
Column length (m)	10.	30.	7.5	20.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.18	0.25	0.10	0.18	0.25
Phase thickness (μm)	0.18	0.25	10.	0.20	0.32
T_start (C)	40.	50.	60.	50.	60.
T_end (C)	295.	240.	240.	280.	250.
Heat rate (K/min)	10.	3.	3.	4.	5.
Initial hold (min)	1.5			1.	30.
Final hold (min)
I	1517.	1562.	1524.	1536.	1522.
Reference	Risticevic, Carasek, et al., 2008	Sarikurkcu, Tepe, et al., 2008	Shellie, 2008	Skalicka-Wozniak, Los, et al., 2008	Yassa and Akhani, 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	DB-5	DB-5MS	HP-5MS	CP Sil 5 CB
Column length (m)	30.	50.	30.	30.	30.
Carrier gas	Helium	Nitrogen	He	He	N2
Substrate
Column diameter (mm)	0.25	0.20	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.32	0.25	0.25	0.25
T_start (C)	50.	60.	60.	60.	60.
T_end (C)	230.	220.	240.	240.	300.
Heat rate (K/min)	3.	5.	3.	3.	4.
Initial hold (min)	10.	3.
Final hold (min)	10.	5.
I	1524.	1526.	1525.	1539.	1508.
Reference	Adams, Beauchamp, et al., 2007	Amiri, 2007	Andrade, Oliveira, et al., 2007	Argyropoulou, Daferera, et al., 2007	Baran, von Reuss, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5 MS	HP-5	DB-5MS	RTX-5 MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	Helium	N2	He	He
Substrate
Column diameter (mm)	0.26	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	60.	60.
T_end (C)	240.	280.	240.	240.	200.
Heat rate (K/min)	3.	4.	5.	3.	2.
Initial hold (min)		5.	1.		2.
Final hold (min)			4.		10.
I	1523.	1520.	1524.	1522.	1515.
Reference	Bos, Woerdenbag, et al., 2007	Capetanos, Saroglou, et al., 2007	Cheraif, Ben Jannet, et al., 2007	Da Silva J.K.R., Sousa P.J.C., et al., 2007	Edris, Chizzola, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	HP-5MS	HP-5MS	DB-1
Column length (m)	30.	30.	30.	30.	60.
Carrier gas	Helium	Helium	He	He	Nitrogen
Substrate
Column diameter (mm)	0.26	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.26	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	290.	240.	250.	250.	250.
Heat rate (K/min)	3.	4.	2.	2.	4.
Initial hold (min)		2.	8.	8.	1.
Final hold (min)		20.	15.	15.	10.
I	1523.	1526.	1517.	1527.	1523.
Reference	Elfami, Bos, et al., 2007	Farsam, Amanlou, et al., 2007	Ferhat, Meklati, et al., 2007	Ferhat, Tigrine-Kordjani, et al., 2007	Ghasempour, Shirinpour, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Col-Elite 5MS	HP-1	RTX-5 MS	HP-101	BP-1
Column length (m)	30.	30.	30.	25.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.2
T_start (C)	30.	60.	45.	70.	60.
T_end (C)	246.	240.	210.	200.	220.
Heat rate (K/min)	3.	2.	3.	3.	5.
Initial hold (min)				2.
Final hold (min)		20.			6.
I	1534.	1497.	1527.	1480.	1536.
Reference	Gudaityte and Venskutonis R.P., 2007	Hachicha, Skanji, et al., 2007	Hudaib and Aburjai, 2007	Jerkovic, Mastelic, et al., 2007	Kiran, Devi, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	SE-30	HP-5	DB-5MS	AT-5
Column length (m)	30.	30.	30.	30.	60.
Carrier gas	He	He	He	He	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	40.	40.	60.	60.
T_end (C)	300.	250.	250.	280.	260.
Heat rate (K/min)	3.	5.	5.	3.	4.
Initial hold (min)		5.	5.
Final hold (min)		10.	10.	30.
I	1512.	1524.	1522.	1487.	1526.
Reference	Limberger, Scopel, et al., 2007	Loizzo, Tundis, et al., 2007	Loizzo, Tundis, et al., 2007	Marongiu B., Piras A., et al., 2007	Meccia, Rojas, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	ZB-5	DB-1	DB-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He		Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	60.	60.
T_end (C)	240.	220.	260.	300.	220.
Heat rate (K/min)	2.	4.	2.5	3.	4.
Initial hold (min)		5.	1.
Final hold (min)		20.	20.
I	1515.	1521.	1501.	1494.	1525.
Reference	Miyazawa and Tamura, 2007	Mohottalage, Tabacchi, et al., 2007	Monser-Esfahani, Karamkhani, et al., 2007	Moreno, Lima, et al., 2007	Morteza-Semnani, Saeedi, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	HP-5 MS	SPB-1	DB-5
Column length (m)	30.	25.	25.	30.	30.
Carrier gas	He	H2	Helium	He	Hydrogen
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.2	0.25
Phase thickness (μm)	0.32	0.33	0.25	0.2	0.25
T_start (C)	50.	60.	100.	70.	50.
T_end (C)	250.	240.	280.	220.	250.
Heat rate (K/min)	5.	3.	4.	3.	4.
Initial hold (min)			3.
Final hold (min)			5.	15.
I	1520.	1524.	1527.	1508.	1524.
Reference	Nori-Shargh, Raftari, et al., 2007	Oliveira, Leitão, et al., 2007	Phutdhawong, Kawaree, et al., 2007	Pinto, Salgueiro, et al., 2007	Pontes, de Olivera, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-5	BPX-5	BPX-5	BPX-5	DB-1
Column length (m)	30.	50.	50.	50.	60.
Carrier gas	He	He	He	He	Nitrogen
Substrate
Column diameter (mm)	0.25	0.22	0.22	0.22	0.25
Phase thickness (μm)	0.25		1.	1.	0.25
T_start (C)	50.	50.	50.	50.	60.
T_end (C)	250.	300.	300.	300.	250.
Heat rate (K/min)	2.	4.	4.	4.	4.
Initial hold (min)		1.	1.	1.	1.
Final hold (min)		10.	10.	10.	10.
I	1521.	1556.	1545.	1556.	1523.
Reference	Raal, Orav, et al., 2007	Rali, Wossa, et al., 2007	Rali, Wossa, et al., 2007, 2	Rali, Wossa, et al., 2007, 2	Reza, Ebrahim, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5 MS	DB-5	DB-5	DB-5
Column length (m)	60.	30.	30.	30.	30.
Carrier gas	Hydrogen	Helium	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	60.	40.
T_end (C)	260.	220.	240.	320.	210.
Heat rate (K/min)	4.	5.	4.	10.	2.
Initial hold (min)		3.
Final hold (min)	20.	3.		4.	33.
I	1527.	1510.	1526.	1514.	1526.
Reference	Rojas, Velasco, et al., 2007	Safaei-Ghomi, Bamoniri, et al., 2007	Sefidkon, Abbasi, et al., 2007	Smelcerovic, Spiteller, et al., 2007	Sylvestre, Longtin, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Elite-5MS	HP-5MS	HP-5 MS	HP-5MS	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	Helium	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.5	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	60.	40.	40.
T_end (C)	280.	280.	280.	250.	240.
Heat rate (K/min)	4.	3.	3.	3.	5.
Initial hold (min)	5.			5.	3.
Final hold (min)	10.			10.	10.
I	1527.	1480.	1523.	1504.	1521.
Reference	Tava, Pecetti, et al., 2007	Tzakou, Bazos, et al., 2007	Vagionas, Graikou, et al., 2007	Vichi, Riu-Aumatell, et al., 2007	Wenguang, Wenlai, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5MS	DB-5	DB-5	CP Sil 5 CB
Column length (m)	30.	30.	30.	30.	25.
Carrier gas	He	He	He		He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.32	0.25	0.25	0.25
T_start (C)	60.	40.	60.	60.	80.
T_end (C)	250.	260.	300.	300.	270.
Heat rate (K/min)	5.	4.	3.	3.	10.
Initial hold (min)	30.
Final hold (min)
I	1522.	1519.3	1514.	1519.	1520.
Reference	Yassa and Akhani, 2007	Zizovic, Stamenic, et al., 2007	Apel, Sobral, et al., 2006	Apel, Sobral, et al., 2006, 2	Ayoub, Al-Azizi, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	ZB-5	AT-5	BP-1	BP-1
Column length (m)	60.	30.	60.	50.	50.
Carrier gas	He		He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.22	0.22
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	40.	60.	60.	60.
T_end (C)	250.	300.	200.	220.	220.
Heat rate (K/min)	3.	2.	4.	2.	2.
Initial hold (min)
Final hold (min)			20.	20.	20.
I	1532.	1503.	1526.	1511.	1517.
Reference	Bertrand, Comte, et al., 2006	Biondi, Sari, et al., 2006	Borges, Rojas, et al., 2006	Boti, Muselli, et al., 2006	Boti, Yao, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-1	HP-1	HP-1	HP-1
Column length (m)	30.	50.	50.	50.	50.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.2	0.2	0.2	0.2
Phase thickness (μm)	0.25	0.33	0.33	0.5	0.33
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	280.	250.	250.	250.	250.
Heat rate (K/min)	3.	2.	2.	2.	2.
Initial hold (min)		4.	4.		4.
Final hold (min)		30.	30.	120.	30.
I	1524.	1511.	1519.	1520.	1520.
Reference	Bozin, Mimicá-Dukic, et al., 2006	Castel, Fernandez, et al., 2006	Castel, Fernandez, et al., 2006	Castel, Fernandez, et al., 2006, 2	Castel, Fernandez, et al., 2006, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-1	DB-1	DB-5	HP-5MS	DB-5
Column length (m)	30.	60.	30.	30.	30.
Carrier gas	Helium	Nitrogen			Helium
Substrate
Column diameter (mm)	0.20	0.25	0.32	0.25	0.26
Phase thickness (μm)	0.20		0.25	0.25	0.25
T_start (C)	70.	40.	60.	60.	60.
T_end (C)	220.	200.	230.	280.	290.
Heat rate (K/min)	3.	2.	3.	4.	3.
Initial hold (min)		1.
Final hold (min)	15.	9.	15.
I	1508.	1508.	1524.	1521.	1523.
Reference	Cavaleiro, Pinto, et al., 2006	Chen, Sheu, et al., 2006	Damjanovic, Skala, et al., 2006	Ebrahim Sajjadi and Mehregan, 2006	Elfami, Komar, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-1	HP-5	HP-1	DB-5	DB-1
Column length (m)	50.	30.	50.	30.	60.
Carrier gas	He	He	He		He
Substrate
Column diameter (mm)	0.2	0.25	0.2	0.25	0.25
Phase thickness (μm)	0.33	0.25	0.33	0.25	0.25
T_start (C)	60.	50.	60.	40.	60.
T_end (C)	250.	300.	250.	210.	240.
Heat rate (K/min)	2.	5.	2.	2.	5.
Initial hold (min)		5.		2.	2.
Final hold (min)	60.	5.	40.	33.
I	1521.	1517.	1508.	1526.	1504.
Reference	Fernandez, Pintaric, et al., 2006	Figuérédo, Cabassu, et al., 2006	Filippi, Lanfranchi, et al., 2006	Garneau F.X., Collin G., et al., 2006	Gohari, Hadjiakhoondi, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	DB-5	HP-5	DB-5
Column length (m)	30.	60.	30.	30.	30.
Carrier gas	He	He	He	He	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	240.	240.	240.	240.	260.
Heat rate (K/min)	5.	5.	5.	4.	3.
Initial hold (min)	2.	2.	2.
Final hold (min)
I	1523.	1504.	1523.	1524.	1521.
Reference	Gohari, Hadjiakhoondi, et al., 2006	Gohari A.R., Hadjiakhoondi A., et al., 2006	Gohari A.R., Hadjiakhoondi A., et al., 2006	Ibañez and Usubillaga, 2006	Javidnia, Miri, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	HP-5	DB-1	BP-1	CP Sil 5 CB
Column length (m)		30.	60.	50.	30.
Carrier gas	Helium	Helium		He	N2
Substrate
Column diameter (mm)		0.32	0.25	0.22	0.32
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	60.	60.	70.	60.	50.
T_end (C)	220.	260.	230.	220.	300.
Heat rate (K/min)	5.	5.	2.	2.	4.
Initial hold (min)		2.	2.
Final hold (min)	6.	13.	20.	20.
I	1536.	1526.	1512.	1520.	1510.
Reference	Kiran, Bhavani, et al., 2006	Kucuk, Gulec, et al., 2006	Lan Phi N.T., Nishiyama C., et al., 2006	Lesueur, Ban, et al., 2006	Lis and Milczarek, 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	HP-5 MS	HP-5	DB-5	BP-1
Column length (m)	30.	30.	30.	30.	25.
Carrier gas	N2	Nitrogen	N2	Helium	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.3
Phase thickness (μm)	0.25	0.25	0.52	0.25
T_start (C)	50.	50.	50.	50.	70.
T_end (C)	200.	280.	280.	250.	220.
Heat rate (K/min)	5.	5.	5.	3.	4.
Initial hold (min)				5.	2.
Final hold (min)		5.	5.		10.
I	1520.	1508.	1508.	1526.	1523.
Reference	Martin, Joseph, et al., 2006	Marzouk, Mansour, et al., 2006	Marzouk, Neffati, et al., 2006	Mirza, Navaei, et al., 2006	Moody, Gundidza, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	CP-Sil 5 CB	NB-30
Column length (m)	30.	30.	30.	25.	30.
Carrier gas	He	He	He	Hydrogen	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.15	0.25
T_start (C)	60.	60.	60.	50.	50.
T_end (C)	220.	220.	220.	230.	250.
Heat rate (K/min)	4.	4.	4.	3.	2.
Initial hold (min)		5.	5.
Final hold (min)
I	1525.	1527.	1525.	1522.	1518.
Reference	Morteza-Semnani, Akbarzadeh, et al., 2006	Morteza-Semnani K., Akbarzadeh M., et al., 2006	Morteza-Semnani K., Saeedi M., et al., 2006	Olawore, Usman, et al., 2006	Orav, Raal, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	HP-5MS	HP-5	DB-5
Column length (m)	25.	50.	30.	30.	30.
Carrier gas	N2	N2	He	He	Hydrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.15	0.25	0.25	0.25	0.25
T_start (C)	50.	95.	40.	60.	70.
T_end (C)	200.	240.	260.	220.	280.
Heat rate (K/min)	4.	4.	4.	5.	4.
Initial hold (min)	3.			10.	4.
Final hold (min)
I	1520.	1516.	1529.	1522.	1522.
Reference	Ouamba, Ouabonzi, et al., 2006	Pala-Paul J., Perez-Alonso M.J., et al., 2006	Petrovic, Ristic, et al., 2006	Pintore G., Chessa M., et al., 2006	Pino, Marbot, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	HP-5	HP-5	DB-5
Column length (m)	30.	30.	30.	25.	30.
Carrier gas	Hydrogen	Hydrogen	H2	H2	Hydrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	70.	70.	50.	60.	120.
T_end (C)	280.	280.	280.	240.	180.
Heat rate (K/min)	4.	4.	4.	3.	2.
Initial hold (min)	4.	4.	2.
Final hold (min)			10.
I	1524.	1529.	1524.	1527.	1508.
Reference	Pino, Marbot, et al., 2006	Pino, Marbot, et al., 2006	Pino, Sauri-Duch, et al., 2006	Potzernheim, Bizzo, et al., 2006	Pripdeevech, Wongpornchai, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	DB-5	DB-5	DB-5	ZB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas		He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	60.	60.	40.
T_end (C)	250.	200.	200.	260.	300.
Heat rate (K/min)	10.	2.	2.	5.	2.
Initial hold (min)	5.
Final hold (min)		60.	60.
I	1532.	1525.	1523.	1534.	1503.
Reference	Robinson, 2006	Rout, Naik, et al., 2006	Rout, Naik, et al., 2006	Sabulal, Dan, et al., 2006	Sari M., Biondi D.M., et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-1	CP Sil 5 CB	CP Sil 5 CB	SPB-5
Column length (m)	25.	60.	25.	25.	60.
Carrier gas	N2	Helium	H2		He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.33	0.25			1.
T_start (C)	30.	60.	50.	50.	40.
T_end (C)	280.	250.	230.	230.	230.
Heat rate (K/min)	3.	5.	3.	3.	3.
Initial hold (min)					5.
Final hold (min)		10.			2.
I	1536.	1515.	1517.	1518.	1551.
Reference	Shafi, Jose, et al., 2006	Sonboli, Mirjalili, et al., 2006	Tesso, König, et al., 2006	Tesso, Kubeczka, et al., 2006	Tornambe, Cornu, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	HP-5	HP-5	SPB-1
Column length (m)	30.	50.	25.	30.	50.
Carrier gas	N2	N2	H2	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.52	0.25	0.33
T_start (C)	60.	90.	50.	60.	50.
T_end (C)	240.	240.	280.	250.	220.
Heat rate (K/min)	4.	4.	2.5	10.	4.
Initial hold (min)			5.	2.	1.
Final hold (min)				10.	10.
I	1505.	1509.	1530.	1540.	1510.
Reference	Trilles, Bombarda, et al., 2006	Velasco-Negueruela, Pérez-Alonso, et al., 2006	Wang, Kong, et al., 2006	Wang, Yang, et al., 2006	Wong, Lim, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	DB-5	HP-1	DB-5MS	DB-5
Column length (m)	30.	30.	50.	30.	50.
Carrier gas	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.25	0.3
Phase thickness (μm)	0.25	0.25	0.5	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	275.	210.	250.	240.	240.
Heat rate (K/min)	4.	3.	2.	3.	2.
Initial hold (min)		5.
Final hold (min)			60.
I	1526.	1522.	1514.	1525.	1521.
Reference	Asadipour, Mehrabani, et al., 2005	Askari and Sefidkon, 2005	Bendimerad and Bendiab, 2005	Busman, Zoghbi, et al., 2005	Chagonda and Chalchat, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	Methyl Silicone	SPB-5
Column length (m)	25.	30.	30.	60.	60.
Carrier gas		He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.3	0.32
Phase thickness (μm)	0.15	0.25	0.25		1.
T_start (C)	40.	60.	60.	50.	40.
T_end (C)	220.	240.	240.	240.	230.
Heat rate (K/min)	3.	3.	3.	3.	3.
Initial hold (min)	5.				5.
Final hold (min)
I	1515.	1527.	1525.	1516.	1551.
Reference	Chagonda and Chalchat, 2005, 2	Chaverri and Cicció, 2005	Chaverri and Cicció, 2005	Chalchat and Özcan, 2005	Cornu, Kondjoyan, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BPX-5	ZB-5	HP-5	CP Sil 8 CB	DB-1
Column length (m)	25.	60.	25.	30.	60.
Carrier gas	He	He	He	He	N2
Substrate
Column diameter (mm)	0.22	0.25	0.2	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.33	0.25	0.25
T_start (C)	50.	40.	60.	80.	60.
T_end (C)	320.	250.	240.	200.	250.
Heat rate (K/min)	5.	6.	3.	3.	5.
Initial hold (min)	5.	7.		5.
Final hold (min)		1.	7.	5.	10.
I	1522.	1543.	1520.	1530.	1525.
Reference	Dickschat, Martens, et al., 2005	Dötterl, Wolfe, et al., 2005	Duarte, Figueira, et al., 2005	Facey, Porter, et al., 2005	Fakhari A.R., Sonboli A., et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-1	HP-5	HP-5MS	HP-5MS
Column length (m)	30.	50.	30.	30.	25.
Carrier gas	He		He	He	He
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	60.	50.
T_end (C)	300.	250.	300.	200.	250.
Heat rate (K/min)	3.	2.	5.	4.	3.
Initial hold (min)	3.	60.	5.	30.	3.
Final hold (min)			5.		10.
I	1508.	1513.	1517.	1514.	1525.
Reference	Ferraz, Limberger, et al., 2005	Fernandez, Lizzani-Cuvelier, et al., 2005	Figuérédo, Cabassu, et al., 2005	Gauvin and Smadja, 2005	Ghasemi Y., Faridi P., et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RSL-200	HP-5	DB-1	DB-1	DB-5
Column length (m)	30.	25.	30.	60.	30.
Carrier gas		H2	He	He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.52	0.25	0.25	0.25
T_start (C)	40.	40.	50.	50.	35.
T_end (C)	280.	240.	265.	250.	280.
Heat rate (K/min)	6.	4.	2.5	4.	4.
Initial hold (min)	2.		1.	5.	2.
Final hold (min)	10.		20.
I	1522.	1520.	1512.	1522.	1530.
Reference	Jirovetz, Buchbauer, et al., 2005	Jovanovic, Kitic, et al., 2005	Khanavi, Ghasemian, et al., 2005	Khajeh, Yamini, et al., 2005	Kowalski and Wolski, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	DB-5	DB-5MS	DB-5MS
Column length (m)	30.	60.	30.	30.	30.
Carrier gas	Helium	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	35.	30.	60.	60.	60.
T_end (C)	280.	260.	230.	280.	280.
Heat rate (K/min)	4.	2.	3.	3.	3.
Initial hold (min)	2.	2.		30.	30.
Final hold (min)		28.
I	1530.	1529.2	1517.	1490.	1492.
Reference	Kowalski, 2005	Leffingwell and Alford, 2005	Limberger, Sobral, et al., 2005	Marongiu, Piras, et al., 2005	Marongiu, Piras, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	CP Sil 5 CB	CP Sil 5 CB	HP-5
Column length (m)	30.	30.	25.	25.	30.
Carrier gas	He	He			He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.15	0.15	0.25
T_start (C)	60.	60.	50.	50.	70.
T_end (C)	220.	220.	230.	230.	240.
Heat rate (K/min)	4.	4.	3.	3.	5.
Initial hold (min)	5.	4.
Final hold (min)
I	1523.	1525.	1522.	1522.	1524.
Reference	Morteza-Semnani, Akbarzadeh, et al., 2005	Morteza-Semnani and Saeedi, 2005	Ogunwande, Olawore, et al., 2005	Olawore, Ogunwande, et al., 2005	Oyedeji, Yani, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	RTX-5 MS	HP-5MS	SPB-5	CP Sil 5 CB
Column length (m)	50.	30.	30.	30.	30.
Carrier gas	N2	He		He	He
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	95.	50.	60.	60.	40.
T_end (C)	240.	280.	280.	250.	220.
Heat rate (K/min)	4.	8.	3.	4.	4.
Initial hold (min)		2.		2.	1.
Final hold (min)		2.		20.
I	1522.	1535.	1523.	1524.	1523.
Reference	Pala-Paul, Perez-Alonso, et al., 2005	Pellati, Benvenuti, et al., 2005	Petrakis, Roussis, et al., 2005	Pino, Marbot, et al., 2005	Rohloff and Bones, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	DB-5	HP-5	HP-5MS	HP-5MS
Column length (m)	30.	25.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	40.	60.	60.	60.	60.
T_end (C)	220.	200.	240.	280.	275.
Heat rate (K/min)	4.	2.	5.	4.	4.
Initial hold (min)	1.
Final hold (min)		80.
I	1523.	1521.	1523.	1522.	1521.
Reference	Rohloff and Bones, 2005	Rout, Misra, et al., 2005	Saeidnia, Gohari, et al., 2005	Sajjadi S.E. and Eskandari B., 2005	Sajjadi and Ghannadi, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	DB-5	DB-5	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	60.	50.	40.	40.	60.
T_end (C)	220.	265.	240.	260.	280.
Heat rate (K/min)	3.	2.5	4.	2.	3.
Initial hold (min)	4.	1.		5.	5.
Final hold (min)		20.		20.
I	1527.	1498.	1522.	1518.	1523.
Reference	Salehi, Sefidkon, et al., 2005	Sarkhail, Amin, et al., 2005	Sefidkon and Jamzad, 2005	Senatore, Apostolides Arnold, et al., 2005	Setzer, Noletto, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	PE-5	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	H2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	300.	300.	300.	230.	280.
Heat rate (K/min)	3.	3.	3.	5.	3.
Initial hold (min)				2.
Final hold (min)				4.
I	1515.	1515.	1515.	1517.	1523.
Reference	Simoes-Pires C.A., Debenedetti S., et al., 2005	Simoes-Pires C.A., Debenedetti S., et al., 2005	Simoes-Pires C.A., Debenedetti S., et al., 2005	Singh, Raina, et al., 2005	Slavkovska, Couladis, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	RTX-1	DB-1	BP-1	DB-5
Column length (m)	60.	60.	60.	30.	30.
Carrier gas	He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	40.
T_end (C)	250.	25.	250.	220.	210.
Heat rate (K/min)	5.	5.	5.	5.	2.
Initial hold (min)					2.
Final hold (min)	10.	10.	10.	15.	33.
I	1523.	1520.	1517.	1523.	1530.
Reference	Sonboli A., Fakhari A.R., et al., 2005	Sonboli, Salehi, et al., 2005	Sonboli, Salehi, et al., 2005, 2	Srivastava, Srivastava, et al., 2005	Stevanovic, Garneau, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 8 CB	RTX-5	HP-5 MS	HP-5MS	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He		He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)		0.25	0.50	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	290.	220.	260.	280.	280.
Heat rate (K/min)	3.	3.	3.	3.	3.
Initial hold (min)	5.
Final hold (min)			20.
I	1519.	1523.	1518.	1484.	1495.
Reference	Suárez, Vásquez, et al., 2005	Szafranek, Chrapkowska, et al., 2005	Topçu, Barla, et al., 2005	Tzakou, Bazos, et al., 2005	Tzakou and Constantinidis, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5	DB-1	HP-5MS	DB-5
Column length (m)	30.	30.	50.	30.	30.
Carrier gas	Helium	Helium			H2
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	40.	60.	40.	50.
T_end (C)	240.	300.	240.	220.	290.
Heat rate (K/min)	3.	4.	3.	3.	4.
Initial hold (min)				5.
Final hold (min)		5.		10.
I	1523.	1512.	1497.	1504.	1515.
Reference	Urdampilleta, Amat, et al., 2005	Utsunomia, Kawata, et al., 2005	Velasco-Negueruela, Pérez-Alonso, et al., 2005	Vichi, Riu-Aumatell, et al., 2005	Abreu, Reis, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	BP-1	DB-5	DB-1	SPB-5
Column length (m)	30.	50.	30.	30.	60.
Carrier gas	N2		He	N2	He
Substrate
Column diameter (mm)	0.25	0.22	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	1.
T_start (C)	50.	60.	60.	50.	60.
T_end (C)	200.	220.	240.	200.	200.
Heat rate (K/min)	5.	2.	2.	5.	4.
Initial hold (min)
Final hold (min)		20.			30.
I	1515.	1514.	1523.	1519.	1537.
Reference	Agnaniet, Menut, et al., 2004	Blanc, Muselli, et al., 2004	Cicció, 2004	Fekam Boyom, Fotio, et al., 2004	Gauvin, Ravaomanarivo, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	DB-5	RTX-1	SE-54
Column length (m)	30.	25.	25.	30.	30.
Carrier gas	N2		Nitrogen	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	60.	60.	60.
T_end (C)	230.	180.	240.	300.	260.
Heat rate (K/min)	2.	3.	3.	4.	2.
Initial hold (min)		10.			5.
Final hold (min)		10.
I	1524.	1522.	1526.	1516.	1511.
Reference	González, Guerra, et al., 2004	bin Jantan, Ayop, et al., 2004	JAvidnia, Mojab, et al., 2004	Kalemba and Thiem, 2004	Kilic, Hafizoglu, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5MS	DB-5	RTX-1	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	40.
T_end (C)	300.	240.	300.	300.	210.
Heat rate (K/min)	3.	3.	3.	4.	2.
Initial hold (min)					2.
Final hold (min)					33.
I	1497.	1525.	1517.	1515.	1527.
Reference	Lago, de Ávila, et al., 2004	paz Lima, Silva, et al., 2004	Limberger, Sobral, et al., 2004	Lis, Boczek, et al., 2004	Lopez Arze, Collin, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5MS	HP-5MS	DB-5MS	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	280.	280.	280.	280.	275.
Heat rate (K/min)	3.	3.	3.	3.	4.
Initial hold (min)
Final hold (min)				30.
I	1521.	1519.	1509.	1481.	1527.
Reference	Malencic, Couladis, et al., 2004	Malencic, Couladis, et al., 2004	Malencic, Couladis, et al., 2004	Marongiu, Porcedda, et al., 2004	Mehrabani, Asadipour, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	DB-5	DB-5	DB-1	NB-30
Column length (m)	30.	30.	50.	60.	50.
Carrier gas	He	Helium	Helium	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.25			0.25	0.25
T_start (C)	60.	60.	60.	50.	50.
T_end (C)	280.	240.	240.	270.	250.
Heat rate (K/min)	3.	2.	2.	4.	2.
Initial hold (min)
Final hold (min)		999.	999.
I	1524.	1512.	1512.	1512.	1519.
Reference	Mimica-Dukic, Bozin, et al., 2004	Miyazawa, Fuhita, et al., 2004	Miyazawa, Fujita, et al., 2004	Nik, Mirza, et al., 2004	Orav, Stulova, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	NB-30	DB-5	DB-1	NB-30	DB-5
Column length (m)	50.	30.	50.	50.	30.
Carrier gas	He	He	N2	He	He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.20	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	35.	95.	50.	35.
T_end (C)	250.	220.	240.	250.	220.
Heat rate (K/min)	2.	3.	4.	2.	2.5
Initial hold (min)
Final hold (min)					6.
I	1517.	1524.	1503.	1518.	1523.
Reference	Orav, Stulova, et al., 2004	Palá-Paúl, Brophy, et al., 2004	Palá-Paúl, Velasco-Negueruela, et al., 2004	Raal, Paaver, et al., 2004	Rohloff, Mordal, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-1	DB-5	HP-5	DB-5
Column length (m)	30.	30.	30.	25.	30.
Carrier gas	He	He	He	H2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.33	0.25	0.52	0.25
T_start (C)	50.	40.	40.	40.	60.
T_end (C)	265.	260.	250.	240.	300.
Heat rate (K/min)	2.5	2.	2.	4.	3.
Initial hold (min)	1.	5.	5.
Final hold (min)	20.	20.	20.
I	1498.	1504.	1521.	1524.	1515.
Reference	Sarkhail, Amin, et al., 2004	Senatore, Napolitano, et al., 2004	Senatore, Rigano, et al., 2004	Simic, Sokovic, et al., 2004	Suyenaga, Apel, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	CP Sil 5 CB	DB-5	HP-5	HP-5
Column length (m)	30.	20.	30.	30.	30.
Carrier gas	He	He	He	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	100.	60.	60.	100.
T_end (C)	240.	270.	300.	220.	240.
Heat rate (K/min)	3.	8.	3.	5.	5.
Initial hold (min)		2.		10.	2.
Final hold (min)					5.
I	1520.	1512.	1522.	1526.	1524.
Reference	Tellez, Khan, et al., 2004	Thappa, Bakshi, et al., 2004	Tirillini, Pellegrino, et al., 2004	Bertoli, Menichini, et al., 2003	Chaves, Lago, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	RTX-5Sil	HP-5MS	HP-1	DB-1
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	70.	60.	70.	50.
T_end (C)	280.	200.	220.	200.	200.
Heat rate (K/min)	3.	4.	5.	10.	5.
Initial hold (min)			20.
Final hold (min)		10.	20.
I	1522.	1519.	1532.	1519.	1505.
Reference	Couladis, Özcan, et al., 2003	Dudai, Larkov, et al., 2003	Feizbaksh, Saber Tehrani, et al., 2003	Fekam Boyom, Amvam Zollo, et al., 2003	Fekam Boyom, Ngouana, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5MS	Methyl Silicone	RSL-200	RSL-200
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	H2	H2
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.32	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	40.	40.
T_end (C)	275.	280.	250.	280.	280.
Heat rate (K/min)	4.	4.	2.	6.	6.
Initial hold (min)			2.	5.	5.
Final hold (min)			5.	5.	5.
I	1523.	1524.	1518.	1518.	1515.
Reference	Ghannadi, Aghazari, et al., 2003	Ghasemi, Asghari, et al., 2003	Jayaprakasha, Rao, et al., 2003	Jirovetz, Buchbauer, et al., 2003	Jirovetz, Buchbauer, et al., 2003, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	CP Sil 5 CB	CP Sil 5 CB	DB-5	DB-5MS
Column length (m)	50.	25.	25.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.39	0.25	0.25
T_start (C)	50.	35.	60.	60.	60.
T_end (C)	220.	280.	220.	250.	240.
Heat rate (K/min)	3.	5.	5.	3.	3.
Initial hold (min)	2.	2.5
Final hold (min)	10.
I	1520.	1510.	1518.	1518.	1524.
Reference	Juteau, Jerkovic, et al., 2003	Kanjilal, Kotoky, et al., 2003	Khanavi, Hadjiakhoondi, et al., 2003	Limberger, Simões-Pires, et al., 2003	Maia, Taveira, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	DB-5	CP Sil 5 CB
Column length (m)	30.	30.	30.	50.	25.
Carrier gas	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.2	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.39
T_start (C)	60.	60.	60.	50.	60.
T_end (C)	280.	280.	280.	220.	220.
Heat rate (K/min)	3.	3.	3.	3.	5.
Initial hold (min)				2.
Final hold (min)	30.	30.	30.
I	1505.	1512.	1514.	1524.	1518.
Reference	Marongiu, Porcedda, et al., 2003	Marongiu, Porcedda, et al., 2003	Marongiu, Porcedda, et al., 2003	Masotti, Juteau, et al., 2003	Mazloomifar, Saber-Tehrani, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5	DB-5	OV-101	CP Sil 5 CB
Column length (m)	60.	30.	30.	50.	25.
Carrier gas	He	Helium	He	He	H2
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.2	0.25
Phase thickness (μm)	0.25		0.25	0.5	0.15
T_start (C)	50.	70.	60.	50.	50.
T_end (C)	270.	210.	275.	250.	230.
Heat rate (K/min)	4.	2.	4.	2.	3.
Initial hold (min)			5.
Final hold (min)		60.
I	1513.	1517.	1521.	1512.	1507.
Reference	Mirza, Nik, et al., 2003	Mookdasanit, Tamura, et al., 2003	Morteza-Semnani and Saeedi, 2003	Orav, Kailas, et al., 2003	Oyedeji, Ekundayo, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	DB-5	HP-5	DB-1
Column length (m)	50.	30.	30.	30.	60.
Carrier gas	N2	H2	H2	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	95.	60.	60.	60.	50.
T_end (C)	240.	280.	280.	280.	250.
Heat rate (K/min)	4.	4.	4.	3.	4.
Initial hold (min)		10.	10.
Final hold (min)		40.	40.
I	1516.	1525.	1525.	1503.	1510.
Reference	Perez-Alonso, Velasco-Negueruela, et al., 2003	Pino, Marbot, et al., 2003	Pino, Marbot, et al., 2003	Pitarokili, Tzakou, et al., 2003	Pourmortazavi, Sefidkon, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	NB-30	DB-1	DB-5	HP-5	HP-5
Column length (m)	50.	60.	30.	30.	30.
Carrier gas	He	He	N2	He	He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.5	0.25	0.25	0.25	0.25
T_start (C)	50.	40.	40.	60.	60.
T_end (C)	250.	220.	230.	280.	280.
Heat rate (K/min)	2.	4.	2.	4.	4.
Initial hold (min)
Final hold (min)
I	1516.	1514.	1524.	1524.	1521.
Reference	Raal, Arak, et al., 2003	Rasooli and Mirmostafa, 2003	Rotman, Ahumada, et al., 2003	Sajjadi and Mehregan, 2003	Sajjadi and Mehregan, 2003, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	DB-5	HP-5	HP-5
Column length (m)	30.	60.	30.	60.	60.
Carrier gas		He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	50.	60.	40.	40.
T_end (C)	260.	280.	240.	250.	250.
Heat rate (K/min)	2.	4.	3.	5.	5.
Initial hold (min)	5.			15.	15.
Final hold (min)
I	1520.	1510.	1524.	1524.	1524.
Reference	Senatore and Bruno, 2003	Shahmir, Ahmadi, et al., 2003	da Silva, Luz, et al., 2003	Stashenko, Jaramillo, et al., 2003	Stashenko, Jaramillo, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5MS	HP-5	HP-5	HP-5	HP-5
Column length (m)	30.	25.	25.	25.	25.
Carrier gas	He	H2	H2	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.32	0.32	0.32	0.32
Phase thickness (μm)	0.25	0.53	0.53	0.53	0.53
T_start (C)	60.	40.	40.	40.	40.
T_end (C)	240.	280.	280.	280.	280.
Heat rate (K/min)	3.	4.	4.	4.	4.
Initial hold (min)
Final hold (min)
I	1522.	1519.	1523.	1519.	1520.
Reference	Taveira, de Lima, et al., 2003	Velickovic, Randjelovic, et al., 2003	Velickovic, Randjelovic, et al., 2003	Velickovic, Ristic, et al., 2003	Velickovic, Ristic, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	HP-5	HP-5	DB-5
Column length (m)	25.	25.	25.	30.	30.
Carrier gas	Helium	Helium	Helium	He	He
Substrate
Column diameter (mm)	0.32	0.32	0.32	0.25	0.25
Phase thickness (μm)	0.53	0.53	0.53	0.32	0.25
T_start (C)	40.	40.	40.	60.	60.
T_end (C)	280.	280.	280.	250.	240.
Heat rate (K/min)	4.	4.	4.	5.	3.
Initial hold (min)				30.
Final hold (min)
I	1520.	1521.	1523.	1530.	1523.
Reference	Velickovic, Ristic, et al., 2003	Velickovic, Ristic, et al., 2003	Velickovic, Ristic, et al., 2003	Yassa, Akhani, et al., 2003	Zoghbi, Andrade, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	DB-5	OV-101	HP-1
Column length (m)	25.	60.	30.	25.	30.
Carrier gas	N2	He	He		He
Substrate
Column diameter (mm)	0.25	0.25	0.249	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25		0.25
T_start (C)	50.	50.	60.	50.	70.
T_end (C)	250.	280.	300.	200.	220.
Heat rate (K/min)	4.	4.	3.	5.	3.
Initial hold (min)
Final hold (min)	10.		5.		15.
I	1524.	1510.	1521.	1519.	1508.
Reference	Zrira, Elamrani, et al., 2003	Ahmadi, Mirza, et al., 2002	Bos, Koulman, et al., 2002	Boyom, Keumedjio, et al., 2002	Cavaleiro, Salgueiro, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	5 % Phenyl methyl siloxane	DB-5MS	DB-5MS	BP-1	BPX-5
Column length (m)	30.	30.	30.	25.
Carrier gas	He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.50
Phase thickness (μm)	0.25	0.25	0.25	0.25
T_start (C)	75.	60.	60.	60.	40.
T_end (C)	200.	280.	280.	220.	260.
Heat rate (K/min)	3.	3.	3.	5.	5.
Initial hold (min)	4.
Final hold (min)	8.			10.
I	1523.	1520.	1520.	1514.	1531.
Reference	Cicció and Gómez-Laurito, 2002	Congiu, Falconieri, et al., 2002	Congiu, Falconieri, et al., 2002	Das, Ram, et al., 2002	Diaz and Kite, 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	PTE-5	SE-30	RSL-200
Column length (m)	30.	30.	60.	50.	30.
Carrier gas	He	H2	H2	He	H2
Substrate
Column diameter (mm)	0.25	0.32	0.32	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.30	0.25	0.25
T_start (C)	60.	40.	60.	70.	40.
T_end (C)	240.	245.	285.	240.	280.
Heat rate (K/min)	3.	3.	4.3	4.	6.
Initial hold (min)		20.			5.
Final hold (min)					5.
I	1526.	1497.	1524.	1517.	1519.
Reference	Flamini, Ertugrul, et al., 2002	Gancel, Ollé, et al., 2002	Gudzic, Djokovic, et al., 2002	Iñigo, Palá-Paúl, et al., 2002	Jirovetz, Buchbauer, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RSL-200	CP Sil 8 CB	DB-5	DB-1	DB-5
Column length (m)	30.	30.	30.	25.	30.
Carrier gas	H2	He		He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.23	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.20	0.25
T_start (C)	40.	50.	40.	50.	60.
T_end (C)	280.	220.	210.	200.	240.
Heat rate (K/min)	6.	3.	2.	3.	3.
Initial hold (min)	2.	2.	2.	3.
Final hold (min)	10.		33.	30.
I	1519.	1524.	1529.	1527.	1521.
Reference	Jirovetz, Smith, et al., 2002	Juteau, Masotti, et al., 2002	Kabouss, Charrouf, et al., 2002	Khallouki, Younos, et al., 2002	Kobaisy, Tellez, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	OV-101	HP-5	DB-5
Column length (m)	30.	30.	25.	30.	30.
Carrier gas	He	He	He		He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.32	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	35.	35.	50.	100.	60.
T_end (C)	280.	280.	200.	240.	250.
Heat rate (K/min)	3.	4.	5.	5.	3.
Initial hold (min)	2.	2.		2.
Final hold (min)	15.	15.		5.
I	1530.	1531.	1518.	1519.	1517.
Reference	Krauze-Baranowska, Mardarowicz, et al., 2002	Krauze-Baranowska, Mardarowicz, et al., 2002, 2	Kuiate, Bessière, et al., 2002	Lago, Reis, et al., 2002	Limberger, Simões-Pires, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-5	DB-5	DB-5MS	OV-101
Column length (m)	30.	25.	30.	30.	25.
Carrier gas		N2	He	He	He
Substrate
Column diameter (mm)	0.25	0.23	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.15	0.25	0.25
T_start (C)	60.	50.	60.	60.	50.
T_end (C)	275.	250.	240.	240.	200.
Heat rate (K/min)	4.	3.	3.	3.	5.
Initial hold (min)	4.
Final hold (min)
I	1517.	1520.	1526.	1527.	1521.
Reference	Lockwood, Asghari, et al., 2002	Mahmout, Bessière, et al., 2002	Maia, da Silva, et al., 2002	Maia, Zoghbi, et al., 2002	Menut, Bessière, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	OV-101	DB-5MS	DB-5	DB-1
Column length (m)	30.	50.	30.	25.	60.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.2	0.32	0.2	0.25
Phase thickness (μm)	0.25	0.5	0.25
T_start (C)	60.	50.	40.	60.	40.
T_end (C)	250.	250.	280.	220.	250.
Heat rate (K/min)	4.	2.	4.	3.	4.
Initial hold (min)	10.
Final hold (min)			5.
I	1528.	1509.	1522.	1522.	1506.
Reference	Norouzi-Arasi, Yavari, et al., 2002	Orav, Kailas, et al., 2002	Phutdhawong, Korth, et al., 2002	Schwob, Bessière, et al., 2002	Sefidkon, Dabiri, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5	DB-5MS	DB-5	DB-1
Column length (m)	50.	30.	30.	30.	60.
Carrier gas	N2	H2	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.248
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	40.	60.	60.	60.
T_end (C)	240.	280.	270.	240.	220.
Heat rate (K/min)	3.	4.	3.	3.	3.
Initial hold (min)					5.
Final hold (min)					22.
I	1497.	1524.	1525.	1524.	1520.
Reference	Velasco-Negueruela, Pérez-Alonso, et al., 2002	Velickovic, Randjelovic, et al., 2002	Zoghbi, Andrade, et al., 2002	Zoghbi, Andrade, et al., 2002, 2	Bailac, Dellacasa, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-5	DB-1	DB-1	HP-5	HP-5
Column length (m)	60.	60.	60.	30.	30.
Carrier gas	He	He	He	N2	N2
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	40.	40.	40.	60.	60.
T_end (C)	220.	280.	280.	220.	220.
Heat rate (K/min)	3.	4.	4.	5.	5.
Initial hold (min)	5.	5.	5.	10.	10.
Final hold (min)	15.
I	1526.	1511.	1511.	1523.	1524.
Reference	Cornu, Carnat, et al., 2001	Dabiri and Sefidkon, 2001	Dabiri and Sefidkon, 2001	Flamini, Cioni, et al., 2001	Gallori, Flamini, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	Optima-5	RTX-1	DB-5MS	DB-1
Column length (m)	30.	30.	30.	30.	60.
Carrier gas	N2	He	N2	He	He
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.25		0.25	0.25	0.25
T_start (C)	60.	50.	60.	60.	50.
T_end (C)	220.	250.	300.	240.	270.
Heat rate (K/min)	5.	3.	4.	3.	4.
Initial hold (min)		3.
Final hold (min)				30.
I	1518.	1527.	1516.	1515.	1509.
Reference	Gupta, Mallavarapu, et al., 2001	Jacquemond-Collet, Bessière, et al., 2001	Kalemba, Marschall, et al., 2001	Marongiu, Porcedda, et al., 2001	Mirza, Ahmadi, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	OV-101	DB-5	DB-1	DB-5
Column length (m)	50.	50.	30.	30.	60.
Carrier gas	He	He	He	N2	He
Substrate
Column diameter (mm)	0.2	0.2	0.25	0.25	0.25
Phase thickness (μm)			0.25	0.25
T_start (C)	50.	50.	60.	80.	50.
T_end (C)	250.	250.	270.	225.	250.
Heat rate (K/min)	2.	2.	3.	4.	3.
Initial hold (min)					5.
Final hold (min)
I	1509.	1508.	1523.	1504.	1524.
Reference	Orav and Kann, 2001	Orav and Kann, 2001	Palmeira, Conserva, et al., 2001	Palá-Paúl, Pérez-Alonso, et al., 2001	Rousis, Papadogianni, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	CP Sil 5 CB	CP-Sil 5 CB	DB-5	OV-101
Column length (m)	30.	25.	25.	30.	50.
Carrier gas	H2	He	Nitrogen	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.39	0.39	0.25
T_start (C)	60.	60.	60.	60.	80.
T_end (C)	285.	220.	220.	240.	200.
Heat rate (K/min)	3.	5.	5.	3.	2.
Initial hold (min)
Final hold (min)
I	1520.	1522.	1522.	1522.	1517.
Reference	Santos-Gomes and Fernandes-Ferreira, 2001	Sayyah, Kamalinejad, et al., 2001	Sayyah, Kamalinejad, et al., 2001, 2	Tellez M., Estell R., et al., 2001	Yang, 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	DB-1	HP-5	DB-1	RSL-200
Column length (m)	50.	60.	30.	30.	60.
Carrier gas	N2	N2	H2		H2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.32
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	80.	60.	40.	45.	40.
T_end (C)	200.	220.	280.	300.	250.
Heat rate (K/min)	2.	3.	3.	15.	6.
Initial hold (min)		5.	10.	2.
Final hold (min)		22.	10.	5.
I	1517.	1528.	1523.	1505.	1516.
Reference	Yang, 2001, 2	Bailac, Dellacasa, et al., 2000	Bicalho, Pereira, et al., 2000	Hedin, McKibben, et al., 2000	Jirovetz, Puschmann, et al., 2000
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-1	HP-5	OV-101	DB-5
Column length (m)	25.	60.	30.	50.	30.
Carrier gas	Nitrogen	He	He	Nitrogen	He
Substrate
Column diameter (mm)	0.50	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25		0.25
T_start (C)	60.	60.	40.	40.	60.
T_end (C)	220.	200.	240.	200.	240.
Heat rate (K/min)	5.	4.	3.	2.	3.
Initial hold (min)		5.	5.	10.
Final hold (min)		25.
I	1512.	1517.	1533.	1516.	1523.
Reference	Mallavarapu, Rao, et al., 2000	Meccia, Rojas, et al., 2000	Novak, Novak, et al., 2000	Tamura, Boonbumrung, et al., 2000	Tellez, Dayan, et al., 2000
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	OV-101	OV-101	RTX-1	Ultra-2
Column length (m)	25.	25.	52.	30.	50.
Carrier gas	H2	N2	Helium	N2
Substrate
Column diameter (mm)	0.25	0.25	0.26	0.25	0.32
Phase thickness (μm)	0.15		0.13	0.25
T_start (C)	50.	50.	50.	60.	32.
T_end (C)	320.	200.	220.	300.	250.
Heat rate (K/min)	3.	5.	3.	4.	4.
Initial hold (min)			0.		5.
Final hold (min)			0.
I	1507.	1518.	1517.	1518.	1512.
Reference	Asekun and Ekundayo, 1999	Ayedoun, Adéoti, et al., 1999	Dzumayev, Tkachenko, et al., 1999	Kalemba, 1999	Khalilov L.M., Khalilova A.Z., et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	OV-101	CBP-1	HP-1	BP-1
Column length (m)	25.	25.	25.	25.	25.
Carrier gas	He		He	H2	N2
Substrate
Column diameter (mm)	0.25	0.32	0.3	0.32	0.50
Phase thickness (μm)	0.25			0.17	0.25
T_start (C)	50.	50.	60.	40.	60.
T_end (C)	290.	200.	240.	260.	220.
Heat rate (K/min)	4.	5.	4.	3.	5.
Initial hold (min)				5.
Final hold (min)					10.
I	1521.	1518.	1517.	1506.	1514.
Reference	Koulman, 1999	Kuiate, Zollo, et al., 1999	Labuckas, Zygadlo, et al., 1999	Lopes, Koketsu, et al., 1999	Mallavarapu, Kulkarni, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-1	CP Sil 5 CB	DB-1	SE-30	CP Sil 5 CB
Column length (m)	25.	25.	50.	30.	25.
Carrier gas	H2	He	He	Helium	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25		0.25	0.20	0.39
T_start (C)	40.	50.	70.	60.	60.
T_end (C)	220.	230.	240.	200.	220.
Heat rate (K/min)	3.	3.	4.	3.	5.
Initial hold (min)	5.			4.	5.
Final hold (min)	5.				20.
I	1501.	1531.	1504.	1541.	1516.
Reference	Oberhofer, Nikiforov, et al., 1999	Oyedeji, Olawore, et al., 1999	Palá-Paúl, Pérez-Alonso, et al., 1999	Prikhod'ko, Klyuev, et al., 1999	Rustaiyan, Masoudi, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	DB-1	DB-5	OV-101
Column length (m)	60.	30.	60.	30.	50.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.22
Phase thickness (μm)	0.25	0.25	0.25	0.25	1.
T_start (C)	40.	40.	50.	60.	100.
T_end (C)	280.	220.	220.	240.	220.
Heat rate (K/min)	4.	4.	4.	3.	1.
Initial hold (min)	5.	5.			1.
Final hold (min)
I	1511.	1526.	1526.	1523.	1508.
Reference	Sefidkon, Dabiri, et al., 1999	Sefidkon and Khajavi, 1999	Sefidkon and Mirza, 1999	Tellez, Canel, et al., 1999	Camciuc, Bessière, et al., 1998
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-5	DB-5	SE-30	OV-1	DB-5
Column length (m)	50.	30.	25.	50.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.2	0.32	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	60.	60.	60.	50.	60.
T_end (C)	240.	240.	180.	250.	240.
Heat rate (K/min)	3.	3.	3.	10.	3.
Initial hold (min)			10.	5.
Final hold (min)	20.			20.
I	1530.	1520.	1524.	1516.	1527.
Reference	Doneanu and Anitescu, 1998	El-Sakhawy, El-Tantawy, et al., 1998	Jantan, Ahmad, et al., 1998	Kökdil, Kurucu, et al., 1998	Maia, Zohhbi, et al., 1998
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-101	HP-5	HP-1	OV-101	CP Sil 5 CB
Column length (m)	25.	25.	60.	25.	25.
Carrier gas	He	He	He		N2
Substrate
Column diameter (mm)	0.2	0.2	0.25	0.32	0.32
Phase thickness (μm)	0.2	0.33	0.25		0.25
T_start (C)	70.	70.	50.	50.	50.
T_end (C)	200.	290.	280.	200.	290.
Heat rate (K/min)	3.	3.	4.	5.	4.
Initial hold (min)	2.	8.	5.
Final hold (min)	10.	20.
I	1504.	1529.	1497.	1518.	1507.
Reference	Milso, Mastelic, et al., 1998	Poiana, Sicari, et al., 1998	Stashenko, Cervantes, et al., 1998	Zollo, Biyiti, et al., 1998	Bos, Woerdenbag, et al., 1997
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	DB-5	OV-1	OV-1	DB-1
Column length (m)	25.	30.	30.	30.
Carrier gas	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25
T_start (C)	60.	65.	40.	40.	80.
T_end (C)	300.	300.	270.	270.	220.
Heat rate (K/min)	6.	4.	2.	2.	6.
Initial hold (min)		2.	4.	4.
Final hold (min)
I	1507.	1528.	1514.	1501.	1505.
Reference	Bos, Woerdenbag, et al., 1997, 2	Elias, Simoneit, et al., 1997	Kökdil, Kurucu, et al., 1997	Kökdil, Tanker, et al., 1997	Salgueiro, Vila, et al., 1997
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	CBP-1	HP-1	OV-101
Column length (m)	30.	30.	25.	23.	50.
Carrier gas	Helium	He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.22	0.32	0.25
Phase thickness (μm)	0.25			0.17	0.17
T_start (C)	60.	60.	60.	60.	50.
T_end (C)	240.	240.	240.	250.	220.
Heat rate (K/min)	3.	4.	5.	5.	5.
Initial hold (min)				3.
Final hold (min)				30.
I	1523.	1521.	1517.	1510.	1526.
Reference	Tellez, Estell, et al., 1997	Zunino, Novillo-Newton, et al., 1997	Zygadlo, Ariza-Espinar, et al., 1997	Ayedoun, Adeoti, et al., 1996	Chacko, Jayalekshmy, et al., 1996
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	DB-1	DB-1	HP-1	SPB-1
Column length (m)	50.	60.	60.	25.	50.
Carrier gas	He	He	He	Helium	He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.32	0.2
Phase thickness (μm)		0.50	0.25	0.25	0.33
T_start (C)	50.	50.	50.	60.	40.
T_end (C)	250.	250.	250.	220.	200.
Heat rate (K/min)	2.	8.	2.5	4.	3.
Initial hold (min)		1.	5.	2.	3.
Final hold (min)		6.		20.	30.
I	1510.	1528.	1522.	1510.	1512.
Reference	Orav, Kailas, et al., 1996	Sagrero-Nieves and Bartley, 1996	Stashenko, Puertas, et al., 1996	Thanh, Dung, et al., 1996	Wong and Lai, 1996
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	DB-1	OV-1	OV-1
Column length (m)	60.	60.	60.	50.	50.
Carrier gas	He	He	He	N2	N2
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.27	0.27
Phase thickness (μm)	0.25	0.25	0.25	0.2	0.2
T_start (C)	80.	50.	70.	80.	80.
T_end (C)	210.	250.	270.	240.	240.
Heat rate (K/min)	4.	3.5	2.5	3.	3.
Initial hold (min)		5.	5.
Final hold (min)
I	1512.	1515.	1511.	1515.	1529.
Reference	Nishimura, 1995	Stashenko, Torres, et al., 1995	Tirado, Stashenko, et al., 1995	Ramanoelina, Viano, et al., 1994	Ramanoelina, Viano, et al., 1994
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-101	Methyl Silicone	Methyl Silicone	CP Sil 5 CB	DB-1
Column length (m)	50.	50.	50.	25.	30.
Carrier gas	H2	N2	N2		He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.3	0.17	0.17		0.25
T_start (C)	65.	80.	80.	60.	50.
T_end (C)	300.	200.	200.	280.	240.
Heat rate (K/min)	2.	2.	3.	5.	5.
Initial hold (min)	5.				3.
Final hold (min)
I	1508.	1524.	1523.	1518.	1516.
Reference	Demarne and van der Walt, 1993	Gopalakrishnan, Menon, et al., 1993	Gopalakrishnan, Menon, et al., 1993	Kaul, Singh, et al., 1993	Shiota, 1993
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	SE-54	DB-1	DB-1	DB-1
Column length (m)	30.	30.	30.	60.	60.
Carrier gas	He	Hydrogen	N2
Substrate
Column diameter (mm)	0.25	0.25		0.32	0.32
Phase thickness (μm)	0.25	0.25
T_start (C)	50.	60.	80.	50.	50.
T_end (C)	240.	250.	220.	230.	230.
Heat rate (K/min)	5.	2.	4.	4.	4.
Initial hold (min)	3.	5.
Final hold (min)		2.		10.	10.
I	1519.	1517.	1501.	1513.	1513.
Reference	Shiota, 1993	Kollmannsberger, Nitz, et al., 1992	Velasco-Negueruela, Pérez Alonso, et al., 1991	Binder, Benson, et al., 1990	Binder, Turner, et al., 1990
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 8 CB	RSL-150	BP-1	OV-101	OV-101
Column length (m)	25.	30.	25.	50.	50.
Carrier gas				N2	N2
Substrate
Column diameter (mm)	0.20	0.32	0.33	0.25	0.25
Phase thickness (μm)		0.20
T_start (C)	60.	30.	45.	80.	80.
T_end (C)	230.	200.	180.	200.	200.
Heat rate (K/min)	3.	3.	3.	2.	2.
Initial hold (min)	10.		3.
Final hold (min)
I	1550.	1515.	1506.	1516.	1516.
Reference	Jantan and Goh, 1990	Ronse and De Pooter, 1990	Wyllie, Brophy, et al., 1990	Yang and Sugisawa, 1990	Yang and Sugisawa, 1990
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	BP-1	SE-30	OV-101	OV-101
Column length (m)	60.	50.	40.	50.	50.
Carrier gas		H2	He	N2	N2
Substrate
Column diameter (mm)	0.32	0.30	0.50	0.25	0.25
Phase thickness (μm)			0.75
T_start (C)	50.	40.	30.	80.	80.
T_end (C)	250.	250.	220.	200.	200.
Heat rate (K/min)	4.	10.	3.	2.	2.
Initial hold (min)	0.1	1.
Final hold (min)	5.
I	1512.	1520.	1510.	1517.	1516.
Reference	Binder and Flath, 1989	Brophy, Davies, et al., 1989	de Pooter, de Buyck, et al., 1989	Sugisawa, Yamamoto, et al., 1989	Sugisawa, Yang, et al., 1989
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	DB-1	DB-1	SE-54	OV-1
Column length (m)	50.	60.	60.	25.	50.
Carrier gas	N2	He	He	N2	He
Substrate
Column diameter (mm)	0.25	0.32	0.32	0.25	0.20
Phase thickness (μm)					0.20
T_start (C)	80.	30.	30.	60.	30.
T_end (C)	200.	210.	210.	260.	220.
Heat rate (K/min)	2.	2.	2.	6.	2.
Initial hold (min)		4.	4.	2.
Final hold (min)
I	1516.	1508.	1513.	1533.	1512.
Reference	Sugisawa, Yang, et al., 1989	Takeoka and Butter, 1989	Takeoka and Butter, 1989	Bestmann, Classen, et al., 1988	de Pooter, Nicolai, et al., 1988
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-30	OV-101	OV-101	OV-101	DB-1
Column length (m)	30.	50.	50.	50.	10.
Carrier gas					H2
Substrate
Column diameter (mm)		0.30	0.30	0.30	0.25
Phase thickness (μm)					0.25
T_start (C)	50.	40.	40.	40.	50.
T_end (C)	240.	230.	230.	230.	250.
Heat rate (K/min)	4.	3.5	3.5	3.5	5.
Initial hold (min)	2.	5.	5.	5.
Final hold (min)	10.
I	1510.	1514.	1527.	1535.	1515.
Reference	Ramaswami, Briscese, et al., 1988	Nykanen, 1986	Nykanen, 1986	Nykanen, 1986	Perry, Baxter, et al., 1986
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-1	OV-101	OV-101	OV-101	SE-30
Column length (m)	40.	30.	30.	30.	30.
Carrier gas	He	He	He	He
Substrate
Column diameter (mm)	0.5	0.5	0.5	0.5
Phase thickness (μm)	0.75	0.8	0.8	0.8
T_start (C)	30.	40.	40.	40.	50.
T_end (C)	220.	220.	220.	220.	240.
Heat rate (K/min)	3.	2.	2.	2.	4.
Initial hold (min)					2.
Final hold (min)					10.
I	1512.	1511.	1511.	1511.	1510.
Reference	de Pooter, de Buyck, et al., 1986	De Pooter and Schamp, 1986	De Pooter and Schamp, 1986	De Pooter and Schamp, 1986	Ramaswami, Briscese, et al., 1986
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary
Active phase	OV-3	SE-30+Igepal	SE-30+Igepal
Column length (m)	150.	100.	100.
Carrier gas
Substrate
Column diameter (mm)	0.66	0.25	0.25
Phase thickness (μm)
T_start (C)	20.	70.	70.
T_end (C)	170.	170.	170.
Heat rate (K/min)	1.	1.	1.
Initial hold (min)
Final hold (min)
I	1540.	1518.	1519.
Reference	Buttery, Xu, et al., 1985	Shibamoto and Jennings, 1977	Shibamoto and Jennings, 1977
Comment	MSDC-RI	MSDC-RI	MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

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Cicció and Gómez-Laurito, 2002
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Diaz and Kite, 2002
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Juteau, Masotti, et al., 2002
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Kobaisy, Tellez, et al., 2002
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Lago, Reis, et al., 2002
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Maia, Zoghbi, et al., 2002
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Cornu, A.; Carnat, A.-P.; Martin, B.; Coulon, J.-B.; Lamaison, J.-L.; Berdagué, J.-L., Solid-phase microextraction of volatile components from natural grassland plants, J. Agric. Food Chem., 2001, 49, 1, 203-209, https://doi.org/10.1021/jf0008341 . [all data]

Dabiri and Sefidkon, 2001
Dabiri, M.; Sefidkon, F., Analysis of the essential oil from aerial parts of Perovskia atriplicifolia Benth. at different stages of plant growth, Flavour Fragr. J., 2001, 16, 6, 435-438, https://doi.org/10.1002/ffj.988 . [all data]

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Gupta, Mallavarapu, et al., 2001
Gupta, R.; Mallavarapu, G.R.; Banerjee, S.; Kumar, S., Characteristics of an isomenthone-rich somaclonal mutant isolated in a geraniol-rich rose-scented geranium accession of Pelargonium graveolens, Flavour Fragr. J., 2001, 16, 5, 319-324, https://doi.org/10.1002/ffj.1002 . [all data]

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Jacquemond-Collet, I.; Bessière, J.-M.; Hannedouche, S.; Bertrand, C.; Fourasté, I.; Moulis, C., Identification of the alkaloids of Galipea officinalis by gas chromatography-mass spectrometry, Phytochem. Anal., 2001, 12, 5, 312-319, https://doi.org/10.1002/pca.594 . [all data]

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Kalemba, D.; Marschall, H.; Bradesi, P., Constituents of the essential oil of Solidago gigantea Ait. (giant goldenrod), Flavour Fragr. J., 2001, 16, 1, 19-26, https://doi.org/10.1002/1099-1026(200101/02)16:1<19::AID-FFJ940>3.0.CO;2-U . [all data]

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Marongiu, B.; Porcedda, S.; Porta, G.D.; Reverchon, E., Extraction and isolation of Salvia desoleana and Mentha spicata subsp. insularis essential oils by supercritical CO₂, Flavour Fragr. J., 2001, 16, 5, 384-388, https://doi.org/10.1002/ffj.1021 . [all data]

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Mirza, M.; Ahmadi, L.; Tayebi, M., Volatile constituents of Hymenocrater incanus Bunge, an Iranian endemic species, Flavour Fragr. J., 2001, 16, 4, 239-240, https://doi.org/10.1002/ffj.983 . [all data]

Orav and Kann, 2001
Orav, A.; Kann, J., Determination of peppermint and orange aroma compounds in food and beverages, Proc. Est. Acad. Sci. Chem., 2001, 50, 4, 217-225. [all data]

Palmeira, Conserva, et al., 2001
Palmeira, S.F., Jr.; Conserva, L.M.; Andrade, E.H.A.; Guilhon, G.M.S.P., Analysis by GC-MS of the hexane extract of the aerial parts of Aristolochia acutifolia Duchtr., Flavour Fragr. J., 2001, 16, 2, 85-88, https://doi.org/10.1002/1099-1026(200103/04)16:2<85::AID-FFJ948>3.0.CO;2-2 . [all data]

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Palá-Paúl, J.; Pérez-Alonso, M.J.; Velasco-Negueruela, A.; Palá-Paúl, R.; Sanz, J.; Conejero, Fco., Seasonal variation in chemical constituents of Santolina rosmarinifolia L. ssp. rosmarinifolia, Biochem. Syst. Ecol., 2001, 29, 7, 663-672, https://doi.org/10.1016/S0305-1978(01)00032-1 . [all data]

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Santos-Gomes and Fernandes-Ferreira, 2001
Santos-Gomes, P.C.; Fernandes-Ferreira, M., Organ- and season-dependent variation in the essential oil composition of Salvia officinalis L. cultivated at two different sites, J. Agric. Food Chem., 2001, 49, 6, 2908-2916, https://doi.org/10.1021/jf001102b . [all data]

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Yang, 2001
Yang, R., Analysis of the volatile components in peel oil of Yuzu by gas chromatography/mass spectrometry, Chin. J. Anal. Chem., 2001, 29, 3, 313-316. [all data]

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Bailac, P.N.; Dellacasa, A.D.; Bernasconi, H.O.; Firpo, N.H.; Ponzi, M.I., Composicion del aceite esencial y actividad antimicrobiana de eupatorium patens, Bol. Soc. Chil. Quim., 2000, 45, 207-211. [all data]

Bicalho, Pereira, et al., 2000
Bicalho, B.; Pereira, A.S.; Aquino Neto, F.R.; Pinto, A.C.; Rezende, C.M., Application of high-temperature gas chromatography-mass spectrometry to the investigation of glycosidically bound components related to cashew applie (Anacardium occidentale L. Var. nanum) volatiles, J. Agric. Food Chem., 2000, 48, 4, 1167-1174, https://doi.org/10.1021/jf9909252 . [all data]

Hedin, McKibben, et al., 2000
Hedin, P.A.; McKibben, G.H.; Dollar, D.A., Role of ground trash volatiles in the selection of hibernation sites by boll weevils, J. Agric. Food Chem., 2000, 48, 8, 3673-3676, https://doi.org/10.1021/jf991001h . [all data]

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Mallavarapu, G.R.; Rao, L.; Ramesh, S., Volatile constituents of the leaf and fruit oils of Murraya koenigii Spreng., L. Ess. Oil Res., 2000, 12, 6, 766-768, https://doi.org/10.1080/10412905.2000.9712211 . [all data]

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Novak, Novak, et al., 2000
Novak, J.; Novak, S.; Bitsch, C.; Franz, C.M., Essential oil composition of underground parts of Valeriana celtica ssp. from Austria and Italy, Flavour Fragr. J., 2000, 15, 1, 40-42, https://doi.org/10.1002/(SICI)1099-1026(200001/02)15:1<40::AID-FFJ863>3.0.CO;2-B . [all data]

Tamura, Boonbumrung, et al., 2000
Tamura, H.; Boonbumrung, S.; Yoshizawa, T.; Varanyanond, W., Volatile components of the essential oil in the pulp of four yellow mangoes (Mangifera indica L.) in Thailand, Food Sci. Technol. Res., 2000, 6, 1, 68-73, https://doi.org/10.3136/fstr.6.68 . [all data]

Tellez, Dayan, et al., 2000
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Asekun and Ekundayo, 1999
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Ramaswami, Briscese, et al., 1988
Ramaswami, S.K.; Briscese, P.; Gargiullo, R.J.; von Geldern, T., Sesquiterpene hydrocarbons: from mass confusion to orderly line-up in Flavors and Fragrances: A World Perspective. Proceedings of the 10th International Congress of Essential Oils, Fragrances and Flavors, Lawrence,B.M.; Mookherjee,B.D.; Willis,B.J., ed(s)., Elsevier, New York, 1988, 951-980. [all data]

Nykanen, 1986
Nykanen, I., High Resolution Gas Chromatographic - Mass Spectrometric determination of the Flavour Composition of Wild Majoram (Origanum vulgare L.) Cultivated in Finland, Z. Lebensm Unters Forsch, 1986, 183, 4, 267-272, https://doi.org/10.1007/BF01087742 . [all data]

Perry, Baxter, et al., 1986
Perry, N.B.; Baxter, A.J.; Brennan, N.J.; van Klink, J.W., Dalmatian Sage. PArt 1. Differing oil yields and compositions from flowering and non-flowering accessions, Flavour Fragr. J., 1986, 11, 4, 231-238, https://doi.org/10.1002/(SICI)1099-1026(199607)11:4<231::AID-FFJ572>3.0.CO;2-0 . [all data]

de Pooter, de Buyck, et al., 1986
de Pooter, H.L.; de Buyck, L.F.; Schamp, N.M.; Aboutabl, E.; De Bruyn, A.; Husain, S.Z., The Volatile Fraction of Senecio glaucus subsp. coronopifolius, Flavour Fragr. J., 1986, 1, 4-5, 159-163, https://doi.org/10.1002/ffj.2730010406 . [all data]

De Pooter and Schamp, 1986
De Pooter, H.L.; Schamp, N.M., Comparison of the Volatile Composition of Some Calamintha/Satureja Species, Prog. Essnt. Oil. Res., 1986, 139-150. [all data]

Ramaswami, Briscese, et al., 1986
Ramaswami, S.K.; Briscese, P.; Gargiullo, R.J.; von Geldern, T., Sesquiterpene hydrocarbons: from mass confusion to orderly line-up in Flavors and Fragrances: A World Perspective, Lawrence,B.M.; Mookherjee,B.D.; Willis,B.J., ed(s)., Proceedings of the 10th International Congress of Essential Oils, Fragrances, and Flavors, Washington, DC, 1986, 951-959. [all data]

Buttery, Xu, et al., 1985
Buttery, R.G.; Xu, C.; Ling, L.C., Volatile components of wheat leaves (and stems): Possible insect attractants, J. Agric. Food Chem., 1985, 33, 1, 115-117, https://doi.org/10.1021/jf00061a033 . [all data]

Shibamoto and Jennings, 1977
Shibamoto, T.; Jennings, W.G., The volatile composition of the leaf oil of California Juniper (J. californica Carr.) in Proceedings of VII International Congress of Essential Oils, October 7-11, 1977, Kyoto, Japan, 1977, 413-418. [all data]

Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References

Symbols used in this document:

T_end Final temperature

T_start Initial temperature
Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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