Naphthalene, 1,2,3,5,6,8a-hexahydro-4,7-dimethyl-1-(1-methylethyl)-, (1S-cis)-

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Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSBP-1CP-Sil PONA GBBP-1DB-5
Column length (m) 30.50.100.50.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.220.250.220.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.140.60.60.
Tend (C) 250.220.230.220.240.
Heat rate (K/min) 2.2.5.2.3.
Initial hold (min) 8. 10.  
Final hold (min) 30.20.25.20. 
I 1521.1514.1537.1512.1524.
ReferenceBenkaci-Ali, Baaliouamer, et al., 2007Boti, Koukoua, et al., 2007Cunicao, Lopes, et al., 2007Duquesnoy, Castola, et al., 2007Flamini, Cioni, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSBP-1DB-5DB-5Methyl Silicone
Column length (m) 30.50.30.30.30.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.250.220.250.220.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.80.
Tend (C) 280.220.240.240.220.
Heat rate (K/min) 3.2.3.3.2.
Initial hold (min)    2. 
Final hold (min)  20.  15.
I 1518.1515.1524.1520.1519.
ReferenceKundakovic, Fokialakis, et al., 2007Lesueur, de Rocca Serra, et al., 2007Maccioni, Baldini, et al., 2007Martins, Santos, et al., 2007Melo, Corrêa, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1RTX-1RTX-1HP-101HP-101
Column length (m) 60.60.60.25.25.
Carrier gas HeHeHeHeliumHe
Substrate      
Column diameter (mm) 0.220.220.220.200.2
Phase thickness (μm) 0.250.250.250.200.2
Tstart (C) 60.60.60.70.70.
Tend (C) 230.230.230.200.200.
Heat rate (K/min) 2.2.2.3.3.
Initial hold (min)    2.2.
Final hold (min) 30.35.35.15.15.
I 1513.1516.1516.1505.1486.
ReferenceMuselli, Rossi, et al., 2007Paolini J., Costa J., et al., 2007Paolini, Muselli, et al., 2007Politeo, Jukic, et al., 2007Politeo, Jukic, et al., 2007, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5SPB-1HP-5MSDB-5HP-5MS
Column length (m) 30.30.30.25.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.50.60.60.60.
Tend (C) 250.250.280.200.280.
Heat rate (K/min) 4.5.4.2.4.
Initial hold (min) 4.3.5. 5.
Final hold (min) 10.15. 60. 
I 1523.1498.1524.1520.1524.
ReferenceQuijano, Salamanca, et al., 2007Radulovic, Lazarevic, et al., 2007Radulovic, Lazarevic, et al., 2007Rout, Rao, et al., 2007Saroglou, Marin, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5ZB-5DB-5HP-5MSHP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 55.50.60.60.80.
Tend (C) 240.250.240.280.300.
Heat rate (K/min) 3.3.3.3.4.
Initial hold (min) 2.    
Final hold (min) 15.    
I 1521.1524.1524.1519.1528.
ReferenceSilva, Barbosa, et al., 2007Simoniatto, Bonani, et al., 2007Telascrea, de Araujo, et al., 2007Vagionas, Ngassapa, et al., 2007Zeng, Zhao, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSBP-1SPB-1DB-5DB-5
Column length (m) 30.50.30.30.30.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.250.220.250.20.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.50.50.60.
Tend (C) 280.220.250.250.240.
Heat rate (K/min) 3.2.5.5.3.
Initial hold (min)   3.3. 
Final hold (min)  20.15.15. 
I 1498.1515.1500.1505.1524.
ReferenceBasta, Tzakou, et al., 2006Blanc, Bradesi, et al., 2006Blagojevic, Radulovic, et al., 2006Blagojevic, Radulovic, et al., 2006Block, Flamini, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1RTX-1HP-5MSMega 5MSDB-5
Column length (m) 50.60.30.60.30.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.220.220.250.250.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 220.230.280.240.240.
Heat rate (K/min) 2.2.3.3.3.
Initial hold (min)     3.
Final hold (min) 20.45.  5.
I 1508.1515.1524.1511.1524.
ReferenceBoti, Bighelli, et al., 2006Cavalli, Tomi, et al., 2006Chorianopoulos N., Evergets E., et al., 2006Condurso, Verzera, et al., 2006Dob, Dahmane, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5BP-1DB-5HP-5BP-1
Column length (m) 30.50.50.30.50.
Carrier gas N2HeN2N2He
Substrate      
Column diameter (mm) 0.250.220.20.250.22
Phase thickness (μm) 0.250.250.320.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 240.220.220.220.220.
Heat rate (K/min) 3.2.5.5.2.
Initial hold (min) 3. 3.10. 
Final hold (min) 3.20.5. 20.
I 1520.1514.1524.1522.1517.
ReferenceDob, Dahmane, et al., 2006, 2Duquesnoy, Dinh, et al., 2006Esmaeili, Nematollahi, et al., 2006Flamini, Tebano, et al., 2006Gonny, Cavaleiro, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5DB-1HP-5MSHP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.50.60.60.
Tend (C) 250.260.220.280.250.
Heat rate (K/min) 3.3.4.3.10.
Initial hold (min)     2.
Final hold (min)     10.
I 1526.1525.1519.1524.1530.
ReferenceJavidnia, Miri, et al., 2006Javidnia K., Miri R., et al., 2006Kuiate, Bessière, et al., 2006Kukic J., Petrovic S., et al., 2006Liu J.M., Nan P., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5RTX-1HP-5MSDB-5HP-5
Column length (m) 50.60.30.30.60.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.20.220.250.320.25
Phase thickness (μm) 0.320.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 220.230.280.280.250.
Heat rate (K/min) 5.2.3.3.3.
Initial hold (min) 3.    
Final hold (min) 5.35.   
I 1524.1511.1493.1515.1533.
ReferenceMasoudi, Esmaeili, et al., 2006Paolini J., Desjobert J.M., et al., 2006Pavlovic, Kovacevic, et al., 2006Pavlovic, Tzakou, et al., 2006Perraudin, Popovici, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1SPB-1DB-1HP-5OV-1
Column length (m) 30.30.30.25.25.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (μm) 0.20.250.250.250.25
Tstart (C) 70.50.60.60.50.
Tend (C) 220.250.240.240.220.
Heat rate (K/min) 3.5.4.4.3.
Initial hold (min)  3.  1.
Final hold (min) 15.15.  5.
I 1508.1499.1522.1528.1523.
ReferencePinto, Pina-Vaz, et al., 2006Radulovic, Mananjarasoa, et al., 2006Rezazadeh, Hamedani, et al., 2006Rezazadeh, Hamedani, et al., 2006Rubiolo P., Matteodo M., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1HP-5MSHP-5MSDB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (μm) 0.20.250.250.250.25
Tstart (C) 70.60.60.50.50.
Tend (C) 220.280.300.250.250.
Heat rate (K/min) 3.4.3.5.5.
Initial hold (min)  5. 2.2.
Final hold (min) 15.    
I 1508.1515.1520.1523.1523.
ReferenceSalgueiro L.R., Pinto E., et al., 2006Saroglou, Dorizas, et al., 2006Silva-Brandão, Solferini, et al., 2006Su, Ho, et al., 2006Su, Ho, et al., 2006, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5HP-5MSCP Sil 5 CBCP Sil 5 CB
Column length (m) 30.30.30.25.25.
Carrier gas H2HeHeH2He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.25 0.4
Tstart (C) 50.40.80.80.80.
Tend (C) 285.300.300.270.270.
Heat rate (K/min) 4.34.4.10.10.
Initial hold (min)  5.   
Final hold (min)      
I 1524.1521.1526.71520.1520.
ReferenceVujisic L., Vuckovic I., et al., 2006Vundac, Pfeifhofer, et al., 2006Zhao C.X., Li, et al., 2006Ziegenbein, Hanssen, et al., 2006Ziegenbein, Hanssen, et al., 2006, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1SPB-1DB-5BP-1SE-54
Column length (m) 30.30.30.50.50.
Carrier gas N2HeHeHeH2
Substrate      
Column diameter (mm) 0.250.250.20.220.25
Phase thickness (μm) 0.250.250.250.250.27
Tstart (C) 50.50.50.60.50.
Tend (C) 200.250.250.220.300.
Heat rate (K/min) 5.5.5.2.5.
Initial hold (min)  3.3.  
Final hold (min)  15.15.20. 
I 1519.1498.1526.1514.1524.
ReferenceAgnaniet, Makani, et al., 2005Boskovic, Radulovic, et al., 2005Boskovic, Radulovic, et al., 2005Boti J.B., Koukoua G., et al., 2005Brantner, Pfeifhofer, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5RTX-1DB-1DB-1DB-1
Column length (m) 30.60.30.30.30.
Carrier gas N2 N2N2 
Substrate      
Column diameter (mm) 0.250.220.320.320.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.50.50.50.
Tend (C) 220.220.260.260.250.
Heat rate (K/min) 5.2.2.2.2.
Initial hold (min) 10. 3.3.8.
Final hold (min)  20.5.5. 
I 1524.1515.1498.1513.1505.
ReferenceCelik, Gokturk, et al., 2005Cozzani, Muselli, et al., 2005Dob, Berramdane, et al., 2005Dob, Berramdane, et al., 2005, 2Dob, Dahmane, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase MDN-5DB-1BP-1HP-5HP-5
Column length (m) 30.30.50.30.30.
Carrier gas HeHeHeN2N2
Substrate      
Column diameter (mm) 0.250.250.220.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.40.60.60.60.
Tend (C) 250.260.220.220.220.
Heat rate (K/min) 3.2.2.5.5.
Initial hold (min)  5. 10.10.
Final hold (min)  20.20.  
I 1515.1514.1514.1524.1521.
ReferenceDugo, Mondello, et al., 2005de Feo, Urrunaga Soria, et al., 2005Ferrari, Tomi, et al., 2005Flamini, Luigi Cioni, et al., 2005Flamini, Luigi Cioni, et al., 2005, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-1DB-5HP-5HP-5
Column length (m) 50.25.25.30.30.
Carrier gas H2 N2HeHe
Substrate      
Column diameter (mm) 0.220.250.250.250.25
Phase thickness (μm) 0.130.250.250.250.25
Tstart (C) 40.60.75.60.60.
Tend (C) 300.180.210.260.260.
Heat rate (K/min) 4.3.3.3.3.
Initial hold (min)  10.10.  
Final hold (min) 10.10.1.  
I 1508.1522.1524.1526.1526.
ReferenceIdzojtic, Kajba, et al., 2005bin Jantan, Yalvema, et al., 2005bin Jantan, Yalvema, et al., 2005, 2Javidnia, Miri, et al., 2005Javidnia, Miri, et al., 2005, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1HP-5MSDB-5MSDB-1BP-1
Column length (m) 60.30.60.30.50.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.220.250.250.250.22
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.40.50.60.
Tend (C) 230.250.200.200.230.
Heat rate (K/min) 2.4.2.5.2.
Initial hold (min)  2.   
Final hold (min) 35.20.20. 35.
I 1516.1523.1519.1520.1515.
ReferencePaolini, Costa, et al., 2005Pino, Mesa, et al., 2005Seo and Baek, 2005Tchoumbougnang, Zollo, et al., 2005Vellutini, Baldovini, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSHP-5MSHP-5MSSPB-1
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 80.80.80.60.70.
Tend (C) 290.290.290.280.220.
Heat rate (K/min) 2.4.6.3.3.
Initial hold (min)      
Final hold (min)     15.
I 1527.51527.1530.81519.1508.
ReferenceZhao, Liang, et al., 2005Zhao, Liang, et al., 2005Zhao, Liang, et al., 2005Aligiannis, Kalpoutzakis, et al., 2004Antunes, Sevinate-Pinto, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5SPB-1HP-5HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas N2N2He He
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (μm) 0.250.250.20.250.25
Tstart (C) 60.60.70.60.60.
Tend (C) 220.220.220.220.280.
Heat rate (K/min) 5.5.3.5.3.
Initial hold (min) 10.10. 10. 
Final hold (min)   15.  
I 1524.1524.1506.1523.1524.
ReferenceBertoli, Menichini, et al., 2004Bertoli, Pistelli, et al., 2004Cavaleiro, Salgueiro, et al., 2004Ceccarini, Macchia, et al., 2004Chorianopoulos, Kalpoutzakis, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1HP-5DB-5DB-5HP-5
Column length (m) 25.30.30.30.30.
Carrier gas HeHeN2N2He
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.170.250.250.250.25
Tstart (C) 50.60.60.60.50.
Tend (C) 200.240.240.240.290.
Heat rate (K/min) 3.3.3.3.4.
Initial hold (min)      
Final hold (min)      
I 1493.1524.1524.1524.1524.
ReferenceFernández-Ocaña, Gómez-Rodríguez, et al., 2004Flamini, Bader, et al., 2004Flamini, Cioni, et al., 2004Flamini, Cioni, et al., 2004Flach A., Dondon R.C., et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5BP-1HP-5MSHP-5HP-5
Column length (m) 30.50.30.30.30.
Carrier gas N2 HeHeHe
Substrate      
Column diameter (mm) 0.250.220.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.40.60.
Tend (C) 220.220.280.250.260.
Heat rate (K/min) 5.2.4.3.3.
Initial hold (min) 10. 5.  
Final hold (min)  20.   
I 1525.1518.1524.1522.1526.
ReferenceFlamini, Luigi Cioni, et al., 2004Gonny, Bradesi, et al., 2004Grujic-Jovanovic, Skaltsa, et al., 2004Isidorov, Krajewska, et al., 2004Javidnia, Miri, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5MSDB-5MSSPB-1HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.20.25
Phase thickness (μm)  0.250.250.20.25
Tstart (C) 60.60.40.70.50.
Tend (C) 260.280.280.220.300.
Heat rate (K/min) 3.4.4.3.5.
Initial hold (min)  5.2. 5.
Final hold (min)    15. 
I 1522.1523.1526.1508.1530.
ReferenceJavidnia, Miri, et al., 2004, 2Karioti, Hadjipavlou-Litina, et al., 2004Mardarowicz, Wianowska, et al., 2004Moldão-Martins, Beirão-da-Costa, et al., 2004Mumm, Tiemann, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RSL-200Methyl SiliconeSPB-5DB-5HP-5MS
Column length (m) 30.50.30.30.30.
Carrier gas H2HeHeHeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.25 0.250.250.25
Tstart (C) 40.50.60.50.50.
Tend (C) 280.240.250.290.250.
Heat rate (K/min) 6.3.4.4.3.
Initial hold (min) 5. 2.  
Final hold (min) 5. 20.  
I 1553.1520.1524.1524.1524.
ReferenceNgassoum, Ousmaila, et al., 2004Özcan and Chalchat, 2004Pino, Marbot, et al., 2004Reis, Pansarim, et al., 2004Salido, Valenzuela, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5BP-1Optima 5DB-5MS
Column length (m) 25.50.50.25.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.20.20.220.250.25
Phase thickness (μm) 0.330.20.250.250.25
Tstart (C) 60.35.60.60.40.
Tend (C) 240.250.220.280.200.
Heat rate (K/min) 3.3.2.3.4.
Initial hold (min)  15.  5.
Final hold (min) 7.40.20.20.20.
I 1524.1524.1514.1512.1524.
ReferenceSartoratto, Machado, et al., 2004Stashenko, Jaramillo, et al., 2004Tam, Thuam, et al., 2004Vérité, Nacer, et al., 2004Yu, Kim, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-5MSDB-5BPX-5HP-5
Column length (m) 30.30.25.30.30.
Carrier gas HeHeN2N2N2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.40.75.75.60.
Tend (C) 200.200.210.210.220.
Heat rate (K/min) 4.4.3.3.5.
Initial hold (min) 5.5.10.10.10.
Final hold (min) 20.20.1.1. 
I 1524.1518.1522.1526.1524.
ReferenceYu, Kim, et al., 2004, 2Zheng, Kim, et al., 2004bin Ahmad and bin Jantan, 2003bin Ahmad and bin Jantan, 2003, 2Angelini, Carpanese, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5BP-1OV-1HP-5
Column length (m) 30.30.50.25.30.
Carrier gas HeHeHeH2He
Substrate      
Column diameter (mm) 0.250.250.220.250.25
Phase thickness (μm) 0.250.250.250.30.25
Tstart (C) 60.60.60.50.60.
Tend (C) 240.240.230.200.280.
Heat rate (K/min) 3.3.2.3.3.
Initial hold (min)    1. 
Final hold (min) 30. 35.20. 
I 1523.1525.1510.1503.1524.
ReferenceBader, Caponi, et al., 2003Bader, Flamini, et al., 2003Bianchini, Tomi, et al., 2003Bicchi, Rubiolo, et al., 2003Bougatsos, Meyer, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5HP-5SPB-1RTX-1
Column length (m) 30.30.30.30.60.
Carrier gas N2N2N2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.20.22
Phase thickness (μm) 0.250.250.250.20.25
Tstart (C) 50.60.60.70.60.
Tend (C) 200.220.220.220.230.
Heat rate (K/min) 5.5.5.3.2.
Initial hold (min)  10.10.  
Final hold (min) 0.  15.45.
I 1519.1523.1523.1508.1516.
ReferenceBoyom, Assembe, et al., 2003Campeol, Flamini, et al., 2003Campeol, Flamini, et al., 2003Cavaleiro, Salgueiro, et al., 2003Cavalli, Tomi, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Ultra-2HP-5HP-5DB-1DB-1
Column length (m) 25.30.30.30.30.
Carrier gas H2N2N2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.330.250.250.250.25
Tstart (C) 40.60.60.40.40.
Tend (C) 280.220.220.250.250.
Heat rate (K/min) 3.5.5.2.2.
Initial hold (min) 2.10.10.5.5.
Final hold (min) 10.  20. 
I 1524.1524.1524.1500.1514.
ReferenceCeva-Antunes, Bizzo, et al., 2003Dural, Bagci, et al., 2003Ertugrul, Dural, et al., 2003de Feo, Bruno, et al., 2003de Feo, Urrunaga Soria, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5HP-5HP-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeN2N2N2He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 240.220.220.220.280.
Heat rate (K/min) 3.5.5.5.3.
Initial hold (min)  10.10.10. 
Final hold (min)      
I 1525.1525.1523.1525.1524.
ReferenceFlamini, Cioni, et al., 2003Flamini, Luigi Cioni, et al., 2003Flamini, Luigi Cioni, et al., 2003, 2Flamini, Luigi Cioni, et al., 2003, 3Fokialakis, Melliou, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-5HP-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas   HeHeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.5 0.250.250.25
Tstart (C) 40.25.75.60.60.
Tend (C) 265.150.230.280.240.
Heat rate (K/min) 7.3.3.4.3.
Initial hold (min)  5.10.5. 
Final hold (min) 5. 20.  
I 1530.1524.1520.1524.1524.
ReferenceHögnadóttir and Rouseff, 2003Isidorov, Vinogorova, et al., 2003Jantan, Ling, et al., 2003Karioti, Skaltsa, et al., 2003Macchioni, Cioni, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5MSDB-1HP-1BPX-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.330.25
Tstart (C) 60.50.40.40.60.
Tend (C) 280.250.270.260.240.
Heat rate (K/min) 3.3.2.2.3.
Initial hold (min)   5.5.2.
Final hold (min)   20.20. 
I 1524.1524.1501.1520.1525.
ReferenceNgassapa, Runyoro, et al., 2003Salido, Altarejos, et al., 2003Senatore, Lentini, et al., 2003Senatore, Rigano, et al., 2003Shellie, Marriott, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5HP-5HP-5HP-5SPB-1
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.20
Phase thickness (μm) 0.250.250.250.250.20
Tstart (C) 45.40.60.60.70.
Tend (C) 250.240.280.280.220.
Heat rate (K/min) 3.3.4.3.3.
Initial hold (min) 6. 5.  
Final hold (min)     15.
I 1529.1525.1524.1523.1507.
ReferenceShellie, Marriott, et al., 2003, 2Shellie and Marriott, 2003Skaltsa, Demetzos, et al., 2003Tsiri, Kretsi, et al., 2003Cavaleiro, Salgueiro, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSDB-5DB-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas He  HeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.50.60.60.
Tend (C) 300.280.280.240.220.
Heat rate (K/min) 3.3.3.3.5.
Initial hold (min)  5.5. 10.
Final hold (min)      
I 1524.1524.1524.1523.1525.
ReferenceCouladis, Chinou, et al., 2002Demetzos, Angelopoulou, et al., 2002Economakis, Skaltsa, et al., 2002Flamini, Cioni, et al., 2002Flamini, Cioni, et al., 2002, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5CP Sil 5 CBRTX-5 MSDB-1SE-30
Column length (m) 30.50.30.25.25.
Carrier gas  H2HeN2N2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.150.25 0.25
Tstart (C) 60.40.45.60.60.
Tend (C) 280.300.180.180.180.
Heat rate (K/min) 3.4.2.53.3.
Initial hold (min) 5.3.10.10.10.
Final hold (min)    10.10.
I 1524.1523.1523.1516.1516.
ReferenceFokialakis, Magiatis, et al., 2002Heinrich, Pfeifhofer, et al., 2002Hudaib, Speroni, et al., 2002bin Jantan and bin Ahmad, 2002bin Jantan, Ayop, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-5RTX-5HP-1
Column length (m) 30.30.25.30.24.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.25 0.250.17
Tstart (C) 60.60.70.45.60.
Tend (C) 260.280.260.300.250.
Heat rate (K/min) 4.3.4.3.4.
Initial hold (min)    6.2.
Final hold (min)    10.20.
I 1524.1518.1524.1529.1510.
ReferenceJavidnia, Miri, et al., 2002Kovacevic, Pavlovic, et al., 2002Miri, Ramezani, et al., 2002Mondello, Zappia, et al., 2002Nath, Sarma, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5CP Sil 5 CBCP Sil 5 CBHP-5RTX-5
Column length (m) 30.30.50.30.30.
Carrier gas HeH2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.250.40.250.25
Tstart (C) 60.60.60.60.45.
Tend (C) 250.280.280.280.250.
Heat rate (K/min) 4.2.3.3.3.
Initial hold (min) 2.10.10. 6.
Final hold (min) 20.40.60.  
I 1524.1518.1518.1506.1522.
ReferencePino, Marbot, et al., 2002Pino, Marbot, et al., 2002, 2Pino, Marbot, et al., 2002, 3Pitarokili, Couladis, et al., 2002Shellie, Mondello, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5HP-5HP-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.50
Tstart (C) 60.60.60.60.60.
Tend (C) 280.300.260.380.280.
Heat rate (K/min) 3.5.3.3.3.
Initial hold (min) 5.3.   
Final hold (min)   10.  
I 1520.1528.1524.1515.1524.
ReferenceAligiannis, Kalpoutzakis, et al., 2001Bortolomeazzi, Berno, et al., 2001Couladis, Baziou, et al., 2001Couladis, Tsortanidou, et al., 2001Couladis, Tzakou, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1HP-5RTX-5 MSRTX-5 MSDB-5
Column length (m) 60.50.30.30.30.
Carrier gas HeHeHeHeH2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.50.70.70.60.
Tend (C) 250.250.210.210.240.
Heat rate (K/min) 2.52.54.4.3.
Initial hold (min) 5.5.10.10. 
Final hold (min)   10.10. 
I 1518.1524.1528.1528.1525.
ReferenceGuilliard, Delgado, et al., 2001Guilliard, Delgado, et al., 2001Hudaib, Grazia Bellardi, et al., 2001Hudaib, Grazia Bellardi, et al., 2001Nogueira, Bittrich, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBBP-1BP-1HP-5MSHP-5
Column length (m) 50.50.50.30.30.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.320.220.220.250.25
Phase thickness (μm) 0.40.250.250.25 
Tstart (C) 60.60.60.50.50.
Tend (C) 280.220.220.250.200.
Heat rate (K/min) 3.2.2.3.4.
Initial hold (min) 10.   1.
Final hold (min) 60.20.20.  
I 1511.1517.1516.1524.1530.
ReferencePino, Marbot, et al., 2001Rezzi, Bighelli, et al., 2001Rezzi, Cavaleiro, et al., 2001Salido, Altarejos, et al., 2001Shalit, Katzir, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSBPX-5HP-5DB-5HP-5
Column length (m) 30.50.30.30.30.
Carrier gas HeH2HeHeHe
Substrate      
Column diameter (mm) 0.250.220.200.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.40.
Tend (C) 280.180.180.300.200.
Heat rate (K/min) 4.4.4.5.2.
Initial hold (min) 5.5.8.3.5.
Final hold (min)  5.2. 20.
I 1524.1537.1524.1528.1518.
ReferenceSkaltsa, Mavrommati, et al., 2001Zabaras and Wyllie, 2001Alonzo, Bosco, et al., 2000Bortolomeazzi, Pizzale, et al., 2000Kim, Thuy, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5BP-1BP-1DB-5DB-5
Column length (m) 30.50.50.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.220.220.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.60.60.60.60.
Tend (C) 280.230.230.240.240.
Heat rate (K/min) 4.2.2.3.3.
Initial hold (min) 5.  2.2.
Final hold (min)  35.35.  
I 1518.1516.1516.1524.1524.
ReferenceLazari, Skaltsa, et al., 2000Lota, de Rocca Serra, et al., 2000Lota, de Rocca Serra, et al., 2000Maia, de Paula, et al., 2000Maia, de Paula, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5OV-101HP-101CP Sil 5 CB
Column length (m) 30.30.25.25.50.
Carrier gas HeHeN2HeH2
Substrate      
Column diameter (mm) 0.250.250.250.20.22
Phase thickness (μm) 0.250.25 0.20.13
Tstart (C) 60.60.50.70.40.
Tend (C) 240.240.200.200.300.
Heat rate (K/min) 3.3.5.3.4.
Initial hold (min) 2.2. 2. 
Final hold (min)    10.10.
I 1524.1524.1518.1503.1522.
ReferenceMaia, de Paula, et al., 2000Maia, de Paula, et al., 2000Menut, Bessiere, et al., 2000Milos and Radonic, 2000Pfeifhofer, 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5Mega 5MSCBP-1HP-5OV-101
Column length (m) 30.30.30.30.25.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.25 0.25 
Tstart (C) 50.40.60.50.50.
Tend (C) 280.240.240.280.200.
Heat rate (K/min) 4.3.4.4.5.
Initial hold (min) 5.2. 5. 
Final hold (min)      
I 1524.1511.1517.1524.1517.
ReferenceSkaltsa, Lazari, et al., 2000Verzera, Trozzi, et al., 2000Zunino, Lopez, et al., 2000Lazari, Skaltsa, et al., 1999Menut, Bessiere, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1HP-1Methyl SiliconeCP Sil 5 CB
Column length (m) 60.30.60.50.25.
Carrier gas He HeN2He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.17 
Tstart (C) 50.50.50.80.60.
Tend (C) 220.220.250.200.260.
Heat rate (K/min) 4.3.2.52.5.
Initial hold (min)  3.5.  
Final hold (min)      
I 1522.1502.1497.1520.1518.
ReferenceMirza and Sefidkon, 1999Muselli, Hoi, et al., 1999Stashenko, Cervantes, et al., 1999Sumathykutty, Rao, et al., 1999Weyerstahl, Marschall, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1DB-5OV-1BP-1BP-1
Column length (m) 25.30.25.50.50.
Carrier gas  H2H2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.220.22
Phase thickness (μm) 0.30.250.30.250.25
Tstart (C) 50.60.50.60.60.
Tend (C) 200.240.200.230.230.
Heat rate (K/min) 3.3.3.2.2.
Initial hold (min) 1. 1.  
Final hold (min) 20. 20.35.35.
I 1498.1524.1503.1516.1508.
ReferenceBicchi, Rubiolo, et al., 1998Nogueira, Marsaioli, et al., 1998Bicchi, Fresia, et al., 1997Mariotti, Costa, et al., 1997Mariotti, Tomi, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1Methyl SiliconeDB-1HP-101
Column length (m) 60.60.25.30.50.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.240.250.20.200.25
Phase thickness (μm)  0.250.30.20 
Tstart (C) 50.50.40.70.70.
Tend (C) 280.250.200.200.200.
Heat rate (K/min) 5.3.52.4.3.
Initial hold (min) 3.5. 5. 
Final hold (min)      
I 1520.1518.1529.1522.1531.
ReferenceTzakou, Roussis, et al., 1997Stashenko, Prada, et al., 1996Píry, Príbela, et al., 1995Stashenko, Wiame, et al., 1995Chung, Eiserich, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101DB-5OV-101CP Sil 5 CB
Column length (m) 50.50.60.50.25.
Carrier gas N2N2HeH2N2
Substrate      
Column diameter (mm) 0.250.250.320.320.22
Phase thickness (μm)   1.  
Tstart (C) 80.80.40.50.70.
Tend (C) 200.200.220.200.295.
Heat rate (K/min) 2.2.3.2.4.
Initial hold (min)      
Final hold (min)      
I 1516.1517.1538.1522.1527.
ReferenceYang, Sugisawa, et al., 1992Yang, Sugisawa, et al., 1992Le Quere and Latrasse, 1990Pieribattesti, Smadja, et al., 1988Montanarella, Bos, et al., 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Benkaci-Ali, Baaliouamer, et al., 2007
Benkaci-Ali, F.; Baaliouamer, A.; Meklati, B.Y.; Chemat, F., Chemical composition of seed essential oils from Algerian Nigella sativa extracted by microwave and hydrodistillation, Flavour Fragr. J., 2007, 22, 2, 148-153, https://doi.org/10.1002/ffj.1773 . [all data]

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Melo, R.M.; Corrêa, V.F.S.; Amorim, A.C.L.; Miranda, A.L.P.; Rezende, C.M., Identification of Impact Aroma Compounds in Eugenia uniflora L. (Brazilian Pitanga) Leaf Essential Oil, J. Braz. Chem. Soc., 2007, 18, 1, 179-183, https://doi.org/10.1590/S0103-50532007000100020 . [all data]

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Paolini J., Costa J., et al., 2007
Paolini J.; Costa J.; Bernardini A.F., Analysis of the essential oil from the roots of Eupatorium cannabinum subsp corsicum (L.) by GC, GC-MS and C-13-NMR, Phytochem. Anal., 2007, 18, 3, 235-244, https://doi.org/10.1002/pca.977 . [all data]

Paolini, Muselli, et al., 2007
Paolini, J.; Muselli, A.; Bernardini, A.-F.; Bighelli, A.; Casanova, J.; Costa, J., Thymol derivatives from essential oil of Doronicum corsicum L., Flavour Fragr. J., 2007, 22, 6, 479-487, https://doi.org/10.1002/ffj.1824 . [all data]

Politeo, Jukic, et al., 2007
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Flamini, G.; Cioni, P.L.; Morelli, I.; Ceccarini, L.; Andolfi, L.; Macchia, M., Composition of the essential oil of Medicago marina L. from the coastal dunes of Tuscany, Italy, Flavour Fragr. J., 2003, 18, 5, 460-462, https://doi.org/10.1002/ffj.1253 . [all data]

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Högnadóttir, Á.; Rouseff, R.L., Identification of aroma active compounds in organce essence oil using gas chromatography-olfactometry and gas chromatography-mass spectrometry, J. Chromatogr. A, 2003, 998, 1-2, 201-211, https://doi.org/10.1016/S0021-9673(03)00524-7 . [all data]

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Jantan, I.; Ling, Y.E.; Romli, S.; Ayop, N.; Ahmad, A.S., A comparative study of the constituents of the essential oils of three Cinnamomum species from Malaysia, J. Essent. Oil Res., 2003, 15, 6, 387-391, https://doi.org/10.1080/10412905.2003.9698618 . [all data]

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Macchioni, F.; Cioni, P.L.; Flamini, G.; Morelli, I.; Maccioni, S.; Ansaldi, M., Chemical composition of essential oils from needles, branches and cones of Pinus pinea, P. halepensis, P. pinaster and P. nigra from central Italy, Flavour Fragr. J., 2003, 18, 2, 139-143, https://doi.org/10.1002/ffj.1178 . [all data]

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Ngassapa, O.; Runyoro, D.K.B.; Harvala, E.; Chinou, I.B., Composition and antimicrobial activity of essential oils of two populations of Tanzanian Lippia javanica (Burm. f.) Spreng. (Verbenaceae), Flavour Fragr. J., 2003, 18, 3, 221-224, https://doi.org/10.1002/ffj.1195 . [all data]

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Senatore, F.; Lentini, F.; Venza, F.; Bruno, M.; Napolitano, F., Composition and antibacterial activity of the essential oil of Anisochilus carnosus (Linn. fil.) Benth., a Tamil plant acclimatized in Sicily, Flavour Fragr. J., 2003, 18, 3, 202-204, https://doi.org/10.1002/ffj.1183 . [all data]

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Shellie, R.A.; Marriott, P.J., Comprehensive two-dimensional gas chromatography-mass spectrometry analysis of Pelargonium graveolens essential oil using rapid scanning quadrupole mass spectrometry, Analyst, 2003, 128, 7, 879-883, https://doi.org/10.1039/b304371a . [all data]

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Milos and Radonic, 2000
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Pfeifhofer, 2000
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Mirza and Sefidkon, 1999
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Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References