Longifolene
- Formula: C15H24
- Molecular weight: 204.3511
- IUPAC Standard InChIKey: PDSNLYSELAIEBU-UHFFFAOYSA-N
- CAS Registry Number: 475-20-7
- Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript. - Other names: 1,4-Methanoazulene, decahydro-4,8,8-trimethyl-9-methylene-, [1S-(1α,3aβ,4α,8aβ)]-; 1,4-Methanoazulene, decahydro-4,8,8-trimethyl-9-methylene-, (1S,3aR,4S,8aS)-(+)-; (+)-Longifolene; D-longifolene; Junipen; Junipene; Kuromatsuen; Kuromatsuene; Longifolen; 1,4-Methanoazulene, decahydro-4,8,8-trimethyl-9-methylene-; (+)-Longifolen; α-Longifolene; 1,4-Methanoazulene, decahydro-4,8,8-trimethyl-9-methylene-, (1S,3aR,4S,8aS)-; (1S,3aR,4S,8aS)-4,8,8-Trimethyl-9-methylenedecahydro-1,4-methanoazulene; 1,4-Methanoazulene, decahydro-4,8,8-trimethyl-9-methylene-, [1S-(1a`,3aa',4a`,8aa')]-; Longifolene (=Junipene); [1S-(1α,3aβ,4α,8aβ)]-decahydro-4,8,8-trimethyl-9-methylene-1,4-methanoazulene
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Normal alkane RI, non-polar column, temperature ramp
Go To: Top, References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-5 | RTX-1 | SPB-1 | HP-5 | DB-5 |
Column length (m) | 30. | 60. | 30. | 30. | 30. |
Carrier gas | Helium | Helium | Helium | Helium | Helium |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.22 | 0.32 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Tstart (C) | 40. | 60. | 30. | 40. | 50. |
Tend (C) | 250. | 230. | 250. | 260. | 250. |
Heat rate (K/min) | 3. | 2. | 4. | 4. | 5. |
Initial hold (min) | 5. | 3. | 2. | ||
Final hold (min) | 20. | 30. | 10. | 5. | |
I | 1404. | 1411. | 1402. | 1402. | 1408. |
Reference | Cao, Li, et al., 2011 | Dib, Djabou, et al., 2010 | Escalona-Arranz, Perez-Roses, et al., 2010 | Miyazawa, Kawauchi, et al., 2010 | Ho, Wang, et al., 2009 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | VF-5 | 5 % Phenyl methyl siloxane | DB-5 | HP-5 | ZB-1 |
Column length (m) | 30. | 60. | 30. | 30. | 30. |
Carrier gas | Helium | Helium | Nitrogen | Helium | Nitrogen |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Tstart (C) | 60. | 90. | 40. | 50. | 45. |
Tend (C) | 300. | 225. | 230. | 300. | 230. |
Heat rate (K/min) | 10. | 3. | 2. | 3. | 3. |
Initial hold (min) | 2. | ||||
Final hold (min) | 10. | 3. | 30. | ||
I | 1430. | 1406. | 1409. | 1397. | 1401. |
Reference | Li and Zhao, 2009 | Retta, Gattuso, et al., 2009 | Scrivanti, Anton, et al., 2009 | Isidorov, Lech, et al., 2008 | Mierendorff, Stahl-Biskup, et al., 2008 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | CP Sil 5 CB | HP-5MS | HP-5 | DB-5MS | HP-5MS |
Column length (m) | 30. | 30. | 30. | 30. | 30. |
Carrier gas | N2 | He | N2 | He | He |
Substrate | |||||
Column diameter (mm) | 0.32 | 0.25 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Tstart (C) | 60. | 60. | 50. | 60. | 60. |
Tend (C) | 300. | 280. | 240. | 240. | 250. |
Heat rate (K/min) | 4. | 3. | 5. | 3. | 2. |
Initial hold (min) | 1. | 8. | |||
Final hold (min) | 4. | 15. | |||
I | 1409. | 1403. | 1402. | 1405. | 1400. |
Reference | Baran, von Reuss, et al., 2007 | Bozin B., Mlmica-Dukic N., et al., 2007 | Cheraif, Ben Jannet, et al., 2007 | Da Silva J.K.R., Sousa P.J.C., et al., 2007 | Ferhat, Tigrine-Kordjani, et al., 2007 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | SE-30 | HP-5 | HP-5 | DB-5 | DB-5MS |
Column length (m) | 30. | 30. | 30. | 30. | 30. |
Carrier gas | He | He | He | He | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Tstart (C) | 40. | 40. | 40. | 50. | 60. |
Tend (C) | 250. | 250. | 240. | 250. | 280. |
Heat rate (K/min) | 5. | 5. | 5. | 3. | 3. |
Initial hold (min) | 5. | 5. | 3. | ||
Final hold (min) | 10. | 10. | 10. | 10. | 30. |
I | 1415. | 1402. | 1398. | 1400. | 1395. |
Reference | Loizzo, Tundis, et al., 2007 | Loizzo, Tundis, et al., 2007 | Wenguang, Wenlai, et al., 2007 | Havlik, Kokoska, et al., 2006 | Maronigiu, Piras, et al., 2006 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-5 | DB-5 | SPB-5 | HP-5 | SPB-5 |
Column length (m) | 30. | 30. | 30. | 60. | |
Carrier gas | Helium | He | He | He | He |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.32 | 0.25 | 0.32 | |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 1. | |
Tstart (C) | 50. | 60. | 50. | 60. | 40. |
Tend (C) | 250. | 280. | 250. | 250. | 230. |
Heat rate (K/min) | 3. | 5. | 5. | 10. | 3. |
Initial hold (min) | 5. | 0.5 | 3. | 2. | 5. |
Final hold (min) | 2. | 15. | 10. | ||
I | 1406. | 1398. | 1402. | 1418. | 1444. |
Reference | Mirza, Navaei, et al., 2006 | Ozel, Gogus, et al., 2006 | Stojanovic, Palic, et al., 2006 | Wang, Yang, et al., 2006 | Cornu, Kondjoyan, et al., 2005 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | CP Sil 8 CB | HP-1 | DB-5MS | HP-5MS | DB-1 |
Column length (m) | 30. | 50. | 30. | 30. | 60. |
Carrier gas | He | He | He | ||
Substrate | |||||
Column diameter (mm) | 0.25 | 0.2 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Tstart (C) | 80. | 60. | 60. | 50. | 50. |
Tend (C) | 200. | 250. | 280. | 250. | 250. |
Heat rate (K/min) | 3. | 2. | 3. | 3. | 4. |
Initial hold (min) | 5. | 60. | 30. | 10. | |
Final hold (min) | 5. | 5. | |||
I | 1437. | 1416. | 1386. | 1410. | 1393. |
Reference | Facey, Porter, et al., 2005 | Fernandez, Lizzani-Cuvelier, et al., 2005 | Marongiu, Piras, et al., 2005 | Melkani, Dev, et al., 2005 | Rasooli and Owlia, 2005 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-1 | DB-5 | HP-5MS | RTX-1 | DB-1 |
Column length (m) | 50. | 30. | 30. | 30. | 60. |
Carrier gas | N2 | He | N2 | He | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.32 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Tstart (C) | 60. | 40. | 60. | 60. | 50. |
Tend (C) | 240. | 230. | 275. | 300. | 250. |
Heat rate (K/min) | 3. | 2. | 4. | 4. | 4. |
Initial hold (min) | |||||
Final hold (min) | |||||
I | 1388. | 1404. | 1400. | 1409. | 1393. |
Reference | Velasco-Negueruela, Pérez-Alonso, et al., 2005 | González, Guerra, et al., 2004 | Hajhashemi V., Ghannadi A., et al., 2004 | Lis, Boczek, et al., 2004 | Rasooli and Razzaghi Abyaneh, 2004 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | HP-1 | DB-5 | HP-5MS | HP-5MS | ZB-1 |
Column length (m) | 30. | 30. | 30. | 30. | 30. |
Carrier gas | He | He | He | He | N2 |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 0.33 | 0.25 | 0.25 | 0.25 | 0.25 |
Tstart (C) | 40. | 60. | 60. | 60. | 45. |
Tend (C) | 260. | 240. | 275. | 280. | 230. |
Heat rate (K/min) | 2. | 3. | 4. | 4. | 3. |
Initial hold (min) | 5. | ||||
Final hold (min) | 20. | ||||
I | 1380. | 1397. | 1401. | 1387. | 1401. |
Reference | Senatore, Napolitano, et al., 2004 | Tellez, Khan, et al., 2004 | Ghannadi, Aghazari, et al., 2003 | Ghasemi, Asghari, et al., 2003 | Mierendorff, Stahl-Biskup, et al., 2003 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-1 | DB-5MS | DB-5 | HP-1 | CP Sil 5 CB |
Column length (m) | 60. | 30. | 30. | 60. | 25. |
Carrier gas | He | He | He | He | He |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | |
Tstart (C) | 50. | 50. | 40. | 50. | 60. |
Tend (C) | 280. | 280. | 250. | 280. | 300. |
Heat rate (K/min) | 4. | 15. | 2. | 4. | 6. |
Initial hold (min) | 2. | 5. | 5. | ||
Final hold (min) | 10. | 60. | |||
I | 1434. | 1408. | 1398. | 1388. | 1398. |
Reference | Ahmadi, Mirza, et al., 2002 | Damon, Hernández, et al., 2002 | Porta, Porcedda, et al., 1999 | Stashenko, Cervantes, et al., 1998 | Bos, Woerdenbag, et al., 1997 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-5 | DB-5 | DB-1 | OV-101 | DB-1 |
Column length (m) | 30. | 30. | 60. | 52. | 60. |
Carrier gas | He | He | Helium | ||
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.26 | 0.32 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | ||
Tstart (C) | 65. | 60. | 70. | 40. | 50. |
Tend (C) | 300. | 300. | 270. | 200. | 250. |
Heat rate (K/min) | 4. | 4. | 2.5 | 3. | 4. |
Initial hold (min) | 2. | 2. | 5. | 0. | 0.1 |
Final hold (min) | 5. | 0. | 5. | ||
I | 1413. | 1396.0 | 1380. | 1400. | 1401. |
Reference | Elias, Simoneit, et al., 1997 | Gawdzik, Mardarowicz, et al., 1996 | Tirado, Stashenko, et al., 1995 | Tkachenko and Zenkevich, 1993 | Binder and Flath, 1989 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary |
---|---|---|---|
Active phase | SE-30 | SE-30 | OV-3 |
Column length (m) | 30. | 30. | 150. |
Carrier gas | He | ||
Substrate | |||
Column diameter (mm) | 0.66 | ||
Phase thickness (μm) | |||
Tstart (C) | 50. | 50. | 20. |
Tend (C) | 240. | 240. | 170. |
Heat rate (K/min) | 4. | 4. | 1. |
Initial hold (min) | 2. | 2. | |
Final hold (min) | 10. | 10. | 120. |
I | 1398. | 1398. | 1420. |
Reference | Ramaswami, Briscese, et al., 1988 | Ramaswami, Briscese, et al., 1986 | Buttery and Ling, 1985 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI |
References
Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
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Notes
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