2-Naphthalenemethanol, 1,2,3,4,4a,5,6,8a-octahydro-α,α,4a,8-tetramethyl-, [2R-(2α,4aα,8aβ)]-


Normal alkane RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5 MSRTX-1HP-5DB-5
Column length (m) 60.30.60.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.220.2520.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.50.60.60.50.
Tend (C) 250.180.230.240.250.
Heat rate (K/min) 3.2.2.3.2.
Initial hold (min) 1.    
Final hold (min) 20. 45.  
I 1656.1653.1629.1650.1654.
ReferenceSardashti, Valizadeh, et al., 2013Phungpanya, Thongpoon, et al., 2012Yapi, Boti, et al., 2012Cavar, Maksimovic, et al., 2010Ho, Wang, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSCP-Sil 5 CBDB-5HP-55 % Phenyl methyl siloxane
Column length (m) 30.30.30.25.60.
Carrier gas HeliumNitrogenHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.200.25
Phase thickness (μm) 0.250.250.250.330.25
Tstart (C) 70.50.50.60.90.
Tend (C) 290.200.250.240.225.
Heat rate (K/min) 5.5.5.3.3.
Initial hold (min)   2.  
Final hold (min) 10.  7.3.
I 1659.1673.1654.1656.1655.
ReferenceRadulovic, Blagojevic, et al., 2010Hnawia, Menut, et al., 2009Ho, Wang, et al., 2009Maridass, 2009Retta, Gattuso, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5 MSCP Sil 5 CBHP-5MSHP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumN2HeHelium
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.250.250.250.26
Tstart (C) 50.50.60.50.60.
Tend (C) 280.230.300.280.240.
Heat rate (K/min) 4.3.4.5.4.
Initial hold (min)  10. 4.2.
Final hold (min)  10. 10.20.
I 1656.1652.1649.1656.1657.
ReferenceZhao, Zeng, et al., 2009Adams, Beauchamp, et al., 2007Baran, von Reuss, et al., 2007Cho, Abd El-Aty, et al., 2007Farsam, Amanlou, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-101DB-5Methyl SiliconeDB-1DB-5
Column length (m) 25.30.50.50.30.
Carrier gas HeHeliumHeliumHeHe
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (μm) 0.20.25 0.250.25
Tstart (C) 70.60.50.95.50.
Tend (C) 200.220.240.240.265.
Heat rate (K/min) 3.4.3.4.2.5
Initial hold (min) 2.   1.
Final hold (min)     20.
I 1612.1654.1671.1643.1659.
ReferenceJerkovic, Mastelic, et al., 2007Morteza-Semnani, Saeedi, et al., 2007Ozcan and Chalchat, 2007Pala-Paul, Brophy, et al., 2007Bazargani, Almasirad, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase AT-5BP-1HP-5DB-5DB-5
Column length (m) 60.50.30.30.30.
Carrier gas He He Helium
Substrate      
Column diameter (mm) 0.250.220.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.40.60.
Tend (C) 200.220.246.210.260.
Heat rate (K/min) 4.2.3.2.3.
Initial hold (min)    2. 
Final hold (min) 20.20. 33. 
I 1655.1644.1653.1655.1656.
ReferenceBorges, Rojas, et al., 2006Boti, Yao, et al., 2006Coronel, Cerda-Garcia-Rojas, et al., 2006Garneau F.X., Collin G., et al., 2006Javidnia, Miri, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-1BP-1CP Sil 5 CBDB-5
Column length (m) 30.60.50.30.30.
Carrier gas He HeN2He
Substrate      
Column diameter (mm) 0.250.250.220.320.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.70.60.50.60.
Tend (C) 280.230.220.300.220.
Heat rate (K/min) 5.2.2.4.4.
Initial hold (min) 4.2.  5.
Final hold (min) 10.20.20.  
I 1656.1638.1644.1631.1655.
ReferenceKim, Abd El-Aty, et al., 2006Lan Phi N.T., Nishiyama C., et al., 2006Lesueur, Ban, et al., 2006Lis and Milczarek, 2006Morteza-Semnani K., Saeedi M., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase PE-5DB-5HP-5MSDB-5HP-5
Column length (m) 50.30.30.30.25.
Carrier gas HeHydrogen N2H2
Substrate      
Column diameter (mm) 0.320.250.250.250.32
Phase thickness (μm) 0.250.250.250.250.52
Tstart (C) 100.70.50.60.50.
Tend (C) 280.280.250.240.280.
Heat rate (K/min) 3.4.10.4.2.5
Initial hold (min) 1.4.5. 5.
Final hold (min)      
I 1652.1652.1670.1652.1654.
ReferencePandey-Rai S., Mallavarapu G.R., et al., 2006Pino, Marbot, et al., 2006Robinson, 2006Trilles, Bombarda, et al., 2006Wang, Kong, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-1HP-5DB-5HP-5MS
Column length (m) 30.25.25.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (μm) 0.250.250.330.250.25
Tstart (C) 60.50.60.60.60.
Tend (C) 250.250.240.300.200.
Heat rate (K/min) 10.3.3.3.4.
Initial hold (min) 2.3. 3.30.
Final hold (min) 10. 7.  
I 1677.1658.1649.1652.1649.
ReferenceWang, Yang, et al., 2006Cégiéla-Carlioz, Bessière, et al., 2005Duarte, Figueira, et al., 2005Ferraz, Limberger, et al., 2005Gauvin and Smadja, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5HP-5MSPE-5RTX-1
Column length (m) 25.30.30.30.60.
Carrier gas HeHeHeH2He
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 50.60.60.60.60.
Tend (C) 250.220.280.230.250.
Heat rate (K/min) 3.4.4.5.5.
Initial hold (min) 3.4. 2. 
Final hold (min) 10.  4.10.
I 1654.1653.1650.1658.1654.
ReferenceGhasemi Y., Faridi P., et al., 2005Morteza-Semnani and Saeedi, 2005Sajjadi, 2005Singh, Raina, et al., 2005Sonboli A., Fakhari A.R., et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1CP Sil 8 CBDB-5MSSPB-5DB-5
Column length (m) 60.30.30.60.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.25 0.251.0.25
Tstart (C) 60.60.80.60.60.
Tend (C) 25.290.250.200.300.
Heat rate (K/min) 5.3.5.4.3.
Initial hold (min)  5.2.  
Final hold (min) 10. 9.30. 
I 1647.1637.1664.1668.1616.
ReferenceSonboli, Salehi, et al., 2005Suárez, Vásquez, et al., 2005Watanabe Y., Mihara R., et al., 2005Gauvin, Ravaomanarivo, et al., 2004Lago, de Ávila, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1DB-5DB-5HP-5MSDB-1
Column length (m) 30.30.30.30.30.
Carrier gas N2 HeHeN2
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.40.60.60.50.
Tend (C) 300.210.240.280.200.
Heat rate (K/min) 4.2.3.3.5.
Initial hold (min)  2.   
Final hold (min)  33.   
I 1648.1650.1650.1654.1643.
ReferenceLis, Boczek, et al., 2004Lopez Arze, Collin, et al., 2004Tellez, Khan, et al., 2004Couladis, Özcan, et al., 2003Fekam Boyom, Ngouana, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RSL-200RSL-200DB-1HP-5DB-1
Column length (m) 30.30.60.30.60.
Carrier gas H2H2HeHeHe
Substrate      
Column diameter (mm) 0.320.320.250.250.32
Phase thickness (μm) 0.250.250.250.320.25
Tstart (C) 40.40.50.60.50.
Tend (C) 280.280.250.250.200.
Heat rate (K/min) 6.6.4.5.3.
Initial hold (min) 5.5. 30.6.
Final hold (min) 5.5.   
I 1649.1669.1636.1660.1644.
ReferenceJirovetz, Buchbauer, et al., 2003Jirovetz, Buchbauer, et al., 2003, 2Pourmortazavi, Sefidkon, et al., 2003Yassa, Akhani, et al., 2003Cimanga, Apers, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-5DB-5MSDB-1
Column length (m) 30.30.30.30.50.
Carrier gas N2N2HeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.50.60.60.60.
Tend (C) 250.250.240.240.240.
Heat rate (K/min) 4.4.3.3.3.
Initial hold (min)  5.   
Final hold (min)      
I 1652.1652.1653.1650.1623.
ReferenceFarah, Fechtal, et al., 2002Farah, Fechtal. M., et al., 2002Flamini, Ertugrul, et al., 2002Maia, Zoghbi, et al., 2002Velasco-Negueruela, Pérez-Alonso, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1BP-1DB-5MSDB-5DB-5
Column length (m) 60.30.30.30.60.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.25 
Tstart (C) 40.60.60.60.50.
Tend (C) 280.220.240.270.250.
Heat rate (K/min) 4.5.3.3.3.
Initial hold (min) 5.   5.
Final hold (min)   30.  
I 1639.1637.1630.1657.1652.
ReferenceDabiri and Sefidkon, 2001Gupta, Mallavarapu, et al., 2001Marongiu, Porcedda, et al., 2001Palmeira, Conserva, et al., 2001Rousis, Papadogianni, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1OV-101DB-5MSDB-5OV-101
Column length (m) 30.50.30.30.25.
Carrier gas HeN2HeHelium 
Substrate      
Column diameter (mm) 0.20.20.250.250.32
Phase thickness (μm)   0.250.25 
Tstart (C) 60.80.60.60.50.
Tend (C) 240.200.240.240.200.
Heat rate (K/min) 3.1.3.3.5.
Initial hold (min)      
Final hold (min)  20.   
I 1649.51677.1650.1653.1648.
ReferenceSantos, Moreira, et al., 2001Menon, Chacko, et al., 1999Zoghbi, Andrade, et al., 1999Santos, Andrade, et al., 1998Zollo, Biyiti, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1DB-5HP-1OV-101
Column length (m) 30. 30.23.50.
Carrier gas He HeliumHeN2
Substrate      
Column diameter (mm) 0.32 0.250.320.25
Phase thickness (μm)   0.250.170.17
Tstart (C) 60.80.60.60.50.
Tend (C) 250.220.240.250.220.
Heat rate (K/min) 3.6.3.5.5.
Initial hold (min)    3. 
Final hold (min)    30. 
I 1645.1634.1653.1625.1660.
ReferenceAbreu and Noronha, 1997Salgueiro, Vila, et al., 1997Tellez, Estell, et al., 1997Ayedoun, Adeoti, et al., 1996Chacko, Jayalekshmy, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Sardashti, Valizadeh, et al., 2013
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Notes

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