2-Naphthalenemethanol, 1,2,3,4,4a,5,6,8a-octahydro-α,α,4a,8-tetramethyl-, [2R-(2α,4aα,8aβ)]-


Van Den Dool and Kratz RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5ZB-5BP-1BP-1HP-5
Column length (m) 30.30.50.50.30.
Carrier gas N2He HeN2
Substrate      
Column diameter (mm) 0.250.250.220.220.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.60.60.60.
Tend (C) 220.250.220.220.220.
Heat rate (K/min) 5.3.2.2.5.
Initial hold (min) 10.   10.
Final hold (min)   20.20. 
I 1652.1652.1643.1637.1658.
ReferenceFlamini, Tebano, et al., 2007Simoniatto, Bonani, et al., 2007Blanc, Bradesi, et al., 2006Duquesnoy, Dinh, et al., 2006Flamini, Tebano, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1HP-5DB-5RTX-1SPB-1
Column length (m) 50.30.50.60.30.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.220.250.20.220.25
Phase thickness (μm) 0.250.250.320.250.25
Tstart (C) 60.60.60.60.50.
Tend (C) 220.260.220.230.250.
Heat rate (K/min) 2.3.5.2.5.
Initial hold (min)   3. 3.
Final hold (min) 20. 5.35.15.
I 1645.1653.1652.1639.1668.
ReferenceGonny, Cavaleiro, et al., 2006Javidnia K., Miri R., et al., 2006Masoudi, Esmaeili, et al., 2006Paolini J., Desjobert J.M., et al., 2006Radulovic, Mananjarasoa, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5HP-5DB-1DB-1
Column length (m) 30.30.30.30.30.
Carrier gas HeHeN2N2He
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.60.50.40.
Tend (C) 280.250.220.260.250.
Heat rate (K/min) 4.5.5.2.3.
Initial hold (min) 5.2.10.3. 
Final hold (min)    5.20.
I 1669.1654.1653.1650.1620.
ReferenceSaroglou, Dorizas, et al., 2006Su, Ho, et al., 2006Celik, Gokturk, et al., 2005Dob, Berramdane, et al., 2005Fanciullino, Gancel, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1DB-1SPB-1BP-1HP-5MS
Column length (m) 50.25.30.50.30.
Carrier gas He He He
Substrate      
Column diameter (mm) 0.220.250.20.220.25
Phase thickness (μm) 0.250.250.20.250.25
Tstart (C) 60.60.70.60.60.
Tend (C) 220.180.220.220.280.
Heat rate (K/min) 2.3.3.2.4.
Initial hold (min)  10.  5.
Final hold (min) 20.10.15.20. 
I 1630.1655.1622.1646.1650.
ReferenceFerrari, Tomi, et al., 2005bin Jantan, Yalvema, et al., 2005Cavaleiro, Salgueiro, et al., 2004Gonny, Bradesi, et al., 2004Karioti, Hadjipavlou-Litina, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1SPB-1HP-5BP-1DB-5
Column length (m) 30.30.25.50.25.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.20.20.20.220.25
Phase thickness (μm) 0.20.20.330.250.25
Tstart (C) 70.70.60.60.75.
Tend (C) 220.220.240.220.210.
Heat rate (K/min) 3.3.3.2.3.
Initial hold (min)     10.
Final hold (min) 15.15.7.20.1.
I 1627.1627.1655.1645.1653.
ReferenceMoldão-Martins, Beirão-da-Costa, et al., 2004Moldão-Martins, Beirão-da-Costa, et al., 2004Sartoratto, Machado, et al., 2004Tam, Thuam, et al., 2004bin Ahmad and bin Jantan, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1BP-1RTX-1HP-5HP-5
Column length (m) 50.50.60.30.30.
Carrier gas HeHeHeN2N2
Substrate      
Column diameter (mm) 0.220.220.220.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 230.230.230.220.220.
Heat rate (K/min) 2.2.2.5.5.
Initial hold (min)    10.10.
Final hold (min) 35.35.45.  
I 1644.1644.1630.1654.1653.
ReferenceBianchini, Tomi, et al., 2003Bianchini, Tomi, et al., 2003Cavalli, Tomi, et al., 2003Dural, Bagci, et al., 2003Ertugrul, Dural, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1PE-5HP-5HP-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.25 0.250.250.25
Tstart (C) 40.40.60.60.60.
Tend (C) 250.280.240.280.280.
Heat rate (K/min) 3.3.3.3.3.
Initial hold (min)      
Final hold (min) 20.    
I 1619.1640.1654.1654.1653.
ReferenceGancel, Ollitrault, et al., 2003Isidorov and Vinogorova, 2003Macchioni, Cioni, et al., 2003Tsiri, Kretsi, et al., 2003Tzakou, Couladis, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-1SE-30RTX-5HP-1
Column length (m) 30.25.25.30.24.
Carrier gas  N2N2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.25 0.250.250.17
Tstart (C) 50.60.60.45.60.
Tend (C) 280.180.180.300.250.
Heat rate (K/min) 3.3.3.3.4.
Initial hold (min) 5.10.10.6.2.
Final hold (min)  10.10.10.20.
I 1652.1642.1642.1659.1635.
ReferenceDemetzos, Angelopoulou, et al., 2002bin Jantan and bin Ahmad, 2002bin Jantan, Ayop, et al., 2002Mondello, Zappia, et al., 2002Nath, Sarma, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBCP Sil 5 CBCP Sil 5 CBHP-5BP-1
Column length (m) 25.30.50.30.50.
Carrier gas N2H2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.22
Phase thickness (μm) 0.250.250.40.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 280.280.280.280.230.
Heat rate (K/min) 4.2.3.3.2.
Initial hold (min) 6.10.10.  
Final hold (min)  40.60. 35.
I 1625.1644.1640.1638.1644.
ReferencePino, Marbot, et al., 2002Pino, Marbot, et al., 2002, 2Pino, Marbot, et al., 2002, 3Pitarokili, Couladis, et al., 2002Bianchini, Tomi, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5 MSCP Sil 5 CBHP-5MSDB-1OV-1
Column length (m) 30.50.30.30.25.
Carrier gas HeHeHe  
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.40.250.250.3
Tstart (C) 70.60.60.50.50.
Tend (C) 210.280.280.220.200.
Heat rate (K/min) 4.3.4.3.3.
Initial hold (min) 10.10.5.3.1.
Final hold (min) 10.60.  20.
I 1657.1613.1652.1615.1620.
ReferenceHudaib, Grazia Bellardi, et al., 2001Pino, Marbot, et al., 2001Skaltsa, Mavrommati, et al., 2001Muselli, Hoi, et al., 1999Bicchi, Rubiolo, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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bin Jantan, I.; bin Ahmad, F., Chemical constituents of the essential oils of Goniothalamus malayanus Hook. f. and Thoms., Flavour Fragr. J., 2002, 17, 5, 372-374, https://doi.org/10.1002/ffj.1107 . [all data]

bin Jantan, Ayop, et al., 2002
bin Jantan, I.; Ayop, N.; Hiong, A.B.; Ahmad, A.S., Chemical composition of the essential oils of Cinnamomum cordatum Kosterm, Flavour Fragr. J., 2002, 17, 3, 212-214, https://doi.org/10.1002/ffj.1075 . [all data]

Mondello, Zappia, et al., 2002
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Nath, Sarma, et al., 2002
Nath, S.C.; Sarma, K.K.; Vajezikova, I.; Leclercq, P.A., Comparison of volatile inflorescence oils and taxonomy of certain Cymbopogon taxa described as Cymbopogon flexuosus (Nees ex Steud.) Wats., Biochem. Syst. Ecol., 2002, 30, 2, 151-162, https://doi.org/10.1016/S0305-1978(01)00066-7 . [all data]

Pino, Marbot, et al., 2002
Pino, J.A.; Marbot, R.; Quert, R.; García, H., Study of essential oils of Eucalyptus resinifera Smith, E. tereticornis Smith and Corymbia maculata (Hook.) K.D. Hill L.A.S. Johnson, grown in Cuba, Flavour Fragr. J., 2002, 17, 1, 1-4, https://doi.org/10.1002/ffj.1026 . [all data]

Pino, Marbot, et al., 2002, 2
Pino, J.A.; Marbot, R.; Bello, A., Volatile compounds of Psidium salutare (H.B.K.) Berg. fruit, J. Agric. Food Chem., 2002, 50, 18, 5146-5148, https://doi.org/10.1021/jf0116303 . [all data]

Pino, Marbot, et al., 2002, 3
Pino, J.A.; Marbot, R.; Vázquez, C., Characterization of volatile in Cosa Rican Guava [Psidium friedrichsthalianum (Berg) Niedenzu] fruit, J. Agric. Food Chem., 2002, 50, 21, 6023-6026, https://doi.org/10.1021/jf011456i . [all data]

Pitarokili, Couladis, et al., 2002
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Bianchini, Tomi, et al., 2001
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Notes

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