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2-Naphthalenemethanol, decahydro-«alpha»,«alpha»,4a-trimethyl-8-methylene-, [2R-(2«alpha»,4a«alpha»,8a«beta»)]-


Normal alkane RI, polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-20DB-WaxSupelcowax-10RTX-WaxCarbowax
Column length (m) 50.30.30.60.60.
Carrier gas HeliumHeliumNitrogenHeliumHe
Substrate      
Column diameter (mm) 0.220.250.250.220.2
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.80.50.60.60.
Tend (C) 220.240.200.230.250.
Heat rate (K/min) 2.3.5.2.2.
Initial hold (min)     8.
Final hold (min) 20.2. 30.15.
I 2219.2220.2200.2229.2227.
ReferenceYapi, Boti, et al., 2012Vahirua-Lechat, Mitermite, et al., 2010Hnawia, Menut, et al., 2009Museli, Pau, et al., 2009Ferhat, Tigrine-Kordjani, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-InnowaxDB-WaxSupelcowax-10Supelcowax-10Innowax
Column length (m) 30.60.30.30.30.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.70.50.40.50.
Tend (C) 240.220.250.250.280.
Heat rate (K/min) 2.4.2.3.9.
Initial hold (min)    5.3.
Final hold (min) 20.  10.3.
I 2211.2239.2272.2203.2215.
ReferenceHachicha, Skanji, et al., 2007Pala-Paul, Brophy, et al., 2007Raal, Orav, et al., 2007Vichi, Riu-Aumatell, et al., 2007Abdelwahed, Hayder, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase InnowaxAT-WaxBP-20DB-WaxSupelcowax 10
Column length (m) 30.60.50.60.30.
Carrier gas N2He HeHelium
Substrate      
Column diameter (mm) 0.250.250.220.250.20
Phase thickness (mum) 0.250.250.250.50.20
Tstart (C) 50.60.60.50.70.
Tend (C) 280.200.220.230.220.
Heat rate (K/min) 9.4.2.3.3.
Initial hold (min) 3.  2. 
Final hold (min) 3.20.20.20.15.
I 2220.2261.2230.2213.2215.
ReferenceAbdelwahed, Hayder, et al., 2006Borges, Rojas, et al., 2006Boti, Yao, et al., 2006Cai, Lin, et al., 2006Cavaleiro, Pinto, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxCP-Wax 52CBDB-WaxBP-20Carbowax-PEG
Column length (m) 60.30.60.50.60.
Carrier gas N2He HeHelium
Substrate      
Column diameter (mm) 0.250.320.250.220.20
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 70.60.70.60.60.
Tend (C) 230.220.230.220.250.
Heat rate (K/min) 2.3.32.2.2.
Initial hold (min) 2.7.2. 8.
Final hold (min) 20.3.20.20.15.
I 2218.2255.2233.2232.2227.
ReferenceChoi, 2006Hymete, Rohloff, et al., 2006Lan Phi N.T., Nishiyama C., et al., 2006Lesueur, Ban, et al., 2006Tigrine-Kordiani, Meklati, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax-10InnowaxSupelcowaxStabilwaxInnowax
Column length (m) 30.50.60.30.60.
Carrier gas HeHeHeH2He
Substrate      
Column diameter (mm) 0.250.20.20.320.25
Phase thickness (mum) 0.250.50.20.50.25
Tstart (C) 50.60.60.40.60.
Tend (C) 250.250.230.280.240.
Heat rate (K/min) 4.2.4.6.5.
Initial hold (min) 1. 30.5. 
Final hold (min) 10.60. 5.30.
I 2214.2222.2196.2193.2256.
ReferenceWong, Sivasothy, et al., 2006Bendimerad and Bendiab, 2005Gauvin and Smadja, 2005Jirovetz, Buchbauer, et al., 2005Joichi, Yomogida, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxZB-WaxBP-20DB-WaxSupelcowax-10
Column length (m) 30.30.50.60.30.
Carrier gas HeHelium N2N2
Substrate      
Column diameter (mm) 0.250.320.220.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.40.60.70.40.
Tend (C) 180.250.220.230.230.
Heat rate (K/min) 3.5.2.2.2.
Initial hold (min)  2. 2. 
Final hold (min) 40.5.20.20. 
I 2225.2192.2227.2245.2283.
ReferenceLee, Umano, et al., 2005N/ABlanc, Muselli, et al., 2004Choi, 2004González, Guerra, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxSupelcowax-10Innowax FSCBP-20TC-Wax
Column length (m) 60.30.60.25.60.
Carrier gas He HeliumH2 
Substrate      
Column diameter (mm) 0.250.250.250.330.25
Phase thickness (mum)  0.25 0.5 
Tstart (C) 60.40.60.80.80.
Tend (C) 220.210.220.220.240.
Heat rate (K/min) 2.2.4.5.3.
Initial hold (min) 4.2.10.  
Final hold (min)  33.   
I 2242.2222.2257.2244.2215.
ReferenceJiang and Kubota, 2004Lopez Arze, Collin, et al., 2004Lourens, Reddy, et al., 2004Dunlop, Bignell, et al., 2003Miyazawa, Yamafuji, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxSupelcowax-10InnowaxSupelcowax-10DB-Wax
Column length (m) 60.30.60.30.60.
Carrier gas HeliumN2He He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum)  0.25 0.250.25
Tstart (C) 70.40.60.40.45.
Tend (C) 210.230.220.210.240.
Heat rate (K/min) 2.2.4.2.3.
Initial hold (min)   10.2. 
Final hold (min) 60. 10.33. 
I 2234.2283.2257.2188.2230.
ReferenceMookdasanit, Tamura, et al., 2003Rotman, Ahumada, et al., 2003Suleimenov, Atazharova, et al., 2003Kabouss, Charrouf, et al., 2002Christoph, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase StabilwaxBP-20DB-WaxBP-20NB-351
Column length (m) 30.25.60.25.25.
Carrier gas H2NitrogenHelium H2
Substrate      
Column diameter (mm) 0.320.500.320.330.3
Phase thickness (mum) 0.250.250.250.50.5
Tstart (C) 60.60.50.80.70.
Tend (C) 280.200.230.220.250.
Heat rate (K/min) 10.5.5.5.5.
Initial hold (min) 5. 2. 2.
Final hold (min) 5.    
I 2222.2252.2229.2244.2212.
ReferenceJirovetz L., Buchbauer G., et al., 2001Mallavarapu, Rao, et al., 2000Paniandy, Chane-Ming, et al., 2000Dunlop, Bignell, et al., 1999Onocha, Ekundayo, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxBP-20HP-InnowaxDB-WaxBP-20
Column length (m) 60.25.60.30.25.
Carrier gas N2H2HeHeH2
Substrate      
Column diameter (mm)  0.330.250.320.33
Phase thickness (mum) 0.250.50.25 0.5
Tstart (C) 60.80.50.60.80.
Tend (C) 220.220.220.250.220.
Heat rate (K/min) 5.5.5.3.5.
Initial hold (min)   5.  
Final hold (min)      
I 2256.2244.2248.2246.2244.
ReferenceWeyerstahl, Marschall, et al., 1999Bignell, Dunlop, et al., 1998Stashenko, Cervantes, et al., 1998Abreu and Noronha, 1997Bignell, Dunlop, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-20BP-20BP-20BP-20BP-20
Column length (m) 25.25.25.25.25.
Carrier gas H2H2H2 H2
Substrate      
Column diameter (mm) 0.330.330.330.330.33
Phase thickness (mum) 0.50.50.50.50.5
Tstart (C) 80.80.80.80.80.
Tend (C) 220.220.220.220.220.
Heat rate (K/min) 5.5.5.5.5.
Initial hold (min)      
Final hold (min)      
I 2244.2244.2244.2244.2244.
ReferenceBignell, Dunlop, et al., 1997, 2Bignell, Dunlop, et al., 1997, 3Bignell, Dunlop, et al., 1997, 4Bignell, Dunlop, et al., 1997, 5Bignell, Dunlop, et al., 1997, 6
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax-10TC-WaxSupelcowax-10DB-WaxDB-Wax
Column length (m) 0.60.60.60.60.
Carrier gas He HeHydrogenH2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum)   0.250.250.25
Tstart (C) 40.80.40.50.50.
Tend (C) 240.240.200.238.238.
Heat rate (K/min) 3.3.3.4.4.
Initial hold (min)  5.3.  
Final hold (min)   30.8.13.
I 2283.2250.2283.2242.2248.
ReferenceZygadlo, Ariza-Espinar, et al., 1997Shuichi, Masazumi, et al., 1996Wong and Lai, 1996Kesselmans and Wijnberg, 1992van Beek, Kleis, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Yapi, Boti, et al., 2012
Yapi, T.A.; Boti, J.B.; Attioua, B.K.; Ahibo, A.C.; Bighelli, A.; Casanova, J.; Tomi, F., Three new natural compounds from the root bark essential oil from Xylopia aethiopica, Phytochem. Anal., 2012, 1-6. [all data]

Vahirua-Lechat, Mitermite, et al., 2010
Vahirua-Lechat, I.; Mitermite, Y.; Menut, C., Aromatic plants of French Polynesia. IV. Composition and chemical variations of the essential oils of leaves of Etlingera cevuga (seeman) R.E. Smith, J. Essen. Oil Res., 2010, 22, 5, 407-409, https://doi.org/10.1080/10412905.2010.9700357 . [all data]

Hnawia, Menut, et al., 2009
Hnawia, E.; Menut, C.; Agrebi, A.; Cabalion, P., Wood essential oil of two endemic trees from New Caledonia: Callitris sulcata (Parl.) Schltr. and Callitris neocaledonica Dummer, Biochem. Systematics Ecol., 2009, 36, 11, 859-866, https://doi.org/10.1016/j.bse.2008.08.007 . [all data]

Museli, Pau, et al., 2009
Museli, A.; Pau, M.; Desjobert, J.-M.; Foddai, M.; Usai, M.; Costa, J., Volatile constituents of Achllea ligustica All. by HS-SPME/GC/GC-MS. Comparison with essential oils obtained by hydrodistillation from Corsica and Sardinia, Chromatographia, 2009, 69, 5/6, 575-585, https://doi.org/10.1365/s10337-008-0939-1 . [all data]

Ferhat, Tigrine-Kordjani, et al., 2007
Ferhat, M.A.; Tigrine-Kordjani, N.; Chemat, S.; Meklati, B.Y.; Chemat, F., Rapid Extraction of Volatile Compounds Using a New Simultaneous Microwave Distillation: Solvent Extraction Device, Chromatographia, 2007, 65, 3-4, 217-222, https://doi.org/10.1365/s10337-006-0130-5 . [all data]

Hachicha, Skanji, et al., 2007
Hachicha, S.F.; Skanji, T.; Barrek, S.; Ghrabi, Z.G.; Zarrouk, H., Composition of the essential oil of Teucrium ramosissimum Desf. (Lamiaceae) from Tunisia, Flavour Fragr. J., 2007, 22, 2, 101-104, https://doi.org/10.1002/ffj.1764 . [all data]

Pala-Paul, Brophy, et al., 2007
Pala-Paul, J.; Brophy, J.J.; Perez-Alonso, M.J.; Usano, J.; Soria, S.C., Essential oil composition of the different parts of Eryngium corniculatum Lam. (Apiaceae) from Spain, J. Chromatogr. A, 2007, 1175, 2, 289-293, https://doi.org/10.1016/j.chroma.2007.10.061 . [all data]

Raal, Orav, et al., 2007
Raal, A.; Orav, A.; Arak, E.; Kailas, T.; Müürisepp, M., Variation in the composition of the essential oil of Valeriana officinalis L. roots from Estonia, Proc. Est. Acad. Sci. Chem., 2007, 56, 2, 67-74. [all data]

Vichi, Riu-Aumatell, et al., 2007
Vichi, S.; Riu-Aumatell, M.; Mora-Pons, M.; Guadayol, J.M.; Buxaderas, S.; López-Tamames, E., Analytical, Nutritional and Clinical Methods. HS-SPME coupled to GC/MS for quality control of Juniperus communis L. berries used for gin aromatization, Food Chem., 2007, 105, 4, 1748-1754, https://doi.org/10.1016/j.foodchem.2007.03.026 . [all data]

Abdelwahed, Hayder, et al., 2006
Abdelwahed, A.; Hayder, N.; Kilani, S.; Mahmoud, A.; Chibani, J.; Hammami, M.; Chekir-Ghedira, L.; Ghedira, K., Chemical composition and antimicrobial activity of essential oils from Tunisian Pituranthos tortuosus (Coss.) Maire, Flavour Fragr. J., 2006, 21, 1, 129-133, https://doi.org/10.1002/ffj.1542 . [all data]

Borges, Rojas, et al., 2006
Borges, R.; Rojas, L.B.; Cegarra, J.A.; Usubillaga, A., Study of the essential oils from the leaves and flowers of Lepechinia conferta (Benth) Epl., Flavour Fragr. J., 2006, 21, 1, 155-157, https://doi.org/10.1002/ffj.1550 . [all data]

Boti, Yao, et al., 2006
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Cai, Lin, et al., 2006
Cai, J.; Lin, P.; Zhu, X.; Su, Q., Comparative analysis of clary sage (S. sclarea L.) oil volatiles by GC-FTIR and GC-MS, Food Chem., 2006, 99, 2, 401-407, https://doi.org/10.1016/j.foodchem.2005.07.041 . [all data]

Cavaleiro, Pinto, et al., 2006
Cavaleiro, C.; Pinto, E.; Gonsales, M.J.; Salguero, L., Antifungal activity of Juniperus essential oils agains dermatophyte, Asrgillus and Candida strains, J. Appl. Microbiol., 2006, 100, 6, 1333-1338, https://doi.org/10.1111/j.1365-2672.2006.02862.x . [all data]

Choi, 2006
Choi, H.-S., Headspace analyses of fresh leaves and stems of Angelica gigas Nakai, a Korean medicinal herb, Flavour Fragr. J., 2006, 21, 4, 604-608, https://doi.org/10.1002/ffj.1602 . [all data]

Hymete, Rohloff, et al., 2006
Hymete, A.; Rohloff, J.; Iversen, T.-H., Essential oil from seeds and husks of Aframomum corrorima from Ethiopia, Flavour Fragr. J., 2006, 21, 4, 642-644, https://doi.org/10.1002/ffj.1634 . [all data]

Lan Phi N.T., Nishiyama C., et al., 2006
Lan Phi N.T.; Nishiyama C.; Choi H.-S.; Sawamura M., Evaluation of aroma characteristic compounds of Citrus natsudaidai Hayata (Natsudaidai) cold-pressed peel oil, Biosci. Biotechnol. Biochem., 2006, 70, 8, 1832-1838, https://doi.org/10.1271/bbb.50705 . [all data]

Lesueur, Ban, et al., 2006
Lesueur, D.; Ban, N.K.; Bighelli, A.; Muselli, A.; Casanova, J., Analysis of the root oil of Fokienia hodginsii (Dunn) Henry et Thomas (Cupressaceae) by GC, GC-MS and 13C-NMR, Flavour Fragr. J., 2006, 21, 1, 171-174, https://doi.org/10.1002/ffj.1557 . [all data]

Tigrine-Kordiani, Meklati, et al., 2006
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Wong, Sivasothy, et al., 2006
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Bendimerad and Bendiab, 2005
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Gauvin and Smadja, 2005
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Jirovetz, Buchbauer, et al., 2005
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Joichi, Yomogida, et al., 2005
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Lee, Umano, et al., 2005
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Blanc, Muselli, et al., 2004
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Choi, 2004
Choi, H.-S., Aroma evaluation of an aquatic herb, changpo (Acorus calamus Var. angustatus Bess), by AEDA and SPME, J. Agric. Food Chem., 2004, 52, 26, 8099-8104, https://doi.org/10.1021/jf040239p . [all data]

González, Guerra, et al., 2004
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Jiang and Kubota, 2004
Jiang, L.; Kubota, K., Differences in the volatile components and their odor characteristics of green and ripe fruits and dried pericarp of Japanese pepper (Xanthoxylum piperitum DC.), J. Agric. Food Chem., 2004, 52, 13, 4197-4203, https://doi.org/10.1021/jf030663a . [all data]

Lopez Arze, Collin, et al., 2004
Lopez Arze, J.B.; Collin, G.; Garneau, F.-X.; Jean, F.-I.; Gagnon, H., Essential oils from Bolivia. II. Asteraceae: Ophryosporus heptanthus (Wedd.) H. Rob. et King, J. Essent. Oil Res., 2004, 16, 4, 374-376, https://doi.org/10.1080/10412905.2004.9698747 . [all data]

Lourens, Reddy, et al., 2004
Lourens, A.C.U.; Reddy, D.; Baser, K.H.C.; Viljoen, A.M.; Van Vuuren, S.F., In vitro Biological Activity and Essential Oil Composition of Four Indigenous South Africal Helichrysum Species, J. Ethnopharmacol., 2004, 95, 2-3, 253-258, https://doi.org/10.1016/j.jep.2004.07.027 . [all data]

Dunlop, Bignell, et al., 2003
Dunlop, P.J.; Bignell, C.M.; Hibbert, D.B.; Brooker, M.I.H., Use of gas chromatograms of the essential leaf oils of the genus Eucalyptus for taxonomic purposes: E. subser. Euglobulares (Blakely), Flavour Fragr. J., 2003, 18, 2, 162-169, https://doi.org/10.1002/ffj.1190 . [all data]

Miyazawa, Yamafuji, et al., 2003
Miyazawa, M.; Yamafuji, C.; Kurose, K.; Ishikawa, Y., Volatile components of the rhizomes of Cirsium japonicum DC, Flavour Fragr. J., 2003, 18, 1, 15-17, https://doi.org/10.1002/ffj.1135 . [all data]

Mookdasanit, Tamura, et al., 2003
Mookdasanit, J.; Tamura, H.; Yoshizawa T.; Tokunaga T.; Nakanishi, K., Trace Volatile Compounds in Essential Oil of Citrus Sudachi by Means of Modified Solvent Extraction Method, Food Sci Technol. Res., 2003, 9, 1, 54-61, https://doi.org/10.3136/fstr.9.54 . [all data]

Rotman, Ahumada, et al., 2003
Rotman, A.; Ahumada, O.; Demo, M.S.; Oliva, M.M.; Turina, A.V.; López, M.L.; Zygadlo, J.A., Aromatic plants from Yungas. Part III. Composition and antimicrobial activity of Myrrhinium atropurpureum Schott var. octandrum Bentham essential oil, Flavour Fragr. J., 2003, 18, 3, 211-214, https://doi.org/10.1002/ffj.1189 . [all data]

Suleimenov, Atazharova, et al., 2003
Suleimenov, E.M.; Atazharova, G.A.; Demirchi, B.; Baser, K.H.C.; Adekenov, S.M., Essential oil composition of Artemisia Lercheana and A. Sieversiana of Kazakhstan flora in Recent problems of development of new medicines of natural origin, Proceedings of symposium, St.Petersburg - Pushkin, 2003, 382-385. [all data]

Kabouss, Charrouf, et al., 2002
Kabouss, A.E.; Charrouf, Z.; Faid, M.; Garneau, F.-X.; Collin, G., Chemical composition and antimicrobial activity of the leaf essential oil of Argania spinosa L. Skeels, J. Essent. Oil Res., 2002, 14, 2, 147-149, https://doi.org/10.1080/10412905.2002.9699801 . [all data]

Christoph, 2001
Christoph, F., Chemische Zuzammensetzung und antimikrobielle Eigenschaften der ätherischen Öle von Leptospermum scoparium J. R. et G. Forst. und anderer Teebaumöle der Gattungen Kunzea, Leptospermum und Melaleuca unter besonderer Berücksichtigung von Handelsölen, Dissertation, University of Hamburg, Germany, 2001, 196. [all data]

Jirovetz L., Buchbauer G., et al., 2001
Jirovetz L.; Buchbauer G.; Shafi P.M.; Rosamma M.K.; Geissler M., Analysis of the composition and aroma of the essential leaf oil of Syzygium travancoricum from South India by GC-FID, GC-MS, and olfactometry. Seasonal changes of composition, Chromatographia Sup., 2001, 53, S1, s372-s374, https://doi.org/10.1007/BF02490359 . [all data]

Mallavarapu, Rao, et al., 2000
Mallavarapu, G.R.; Rao, L.; Ramesh, S., Volatile constituents of the leaf and fruit oils of Murraya koenigii Spreng., L. Ess. Oil Res., 2000, 12, 6, 766-768, https://doi.org/10.1080/10412905.2000.9712211 . [all data]

Paniandy, Chane-Ming, et al., 2000
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Notes

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