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2-Naphthalenemethanol, decahydro-«alpha»,«alpha»,4a-trimethyl-8-methylene-, [2R-(2«alpha»,4a«alpha»,8a«beta»)]-


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5 MSHP-5 MSRTX-1HP-5 MSDB-5 MS
Column length (m) 30.60.60.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.220.250.25
Phase thickness (mum)  0.250.250.250.25
Tstart (C) 60.40.60.50.60.
Tend (C) 240.250.230.250.270.
Heat rate (K/min) 3.3.2.7.3.
Initial hold (min)  1. 1. 
Final hold (min)  20.45.5. 
I 1641.1652.1632.1652.1654.
ReferencePinheiro, de Queiros, et al., 2013Sardashti, Valizadeh, et al., 2013Yapi, Boti, et al., 2012Zouari, Ayadi, et al., 2012Cui, Yang, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSHP-5CP-Sil 5 CBRTX-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumNitrogenNitrogenHydrogen
Substrate      
Column diameter (mm) 0.250.320.250.320.25
Phase thickness (mum) 0.250.250.260.250.25
Tstart (C) 60.60.45.60.50.
Tend (C) 270.240.280.210.250.
Heat rate (K/min) 3.3.3.3.5.
Initial hold (min)  2.  5.
Final hold (min)   22. 5.
I 1657.1651.1647.1641.1651.
ReferenceCui, Yang, et al., 2011Kahriman, Tosun, et al., 2011Mothana, Hasson, et al., 2011Prasad, Moulekhi, et al., 2011Abderrahim, Belhamel, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5HP-5HP-5 MSDB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.2520.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.50.100.80.
Tend (C) 240.240.240.220.240.
Heat rate (K/min) 3.3.3.2.3.
Initial hold (min)   5.  
Final hold (min)     2.
I 1647.1646.1661.1650.1644.
ReferenceCavar, Maksimovic, et al., 2010Magalhaes, Lima, et al., 2010Monsef-Esfahani, Miri, et al., 2010Pripdeevech, Chumpolsri, et al., 2010Vahirua-Lechat, Mitermite, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Sil 5 CBDB-5DB-5 MSRTX-1RTX-1
Column length (m) 30.30.30.60.60.
Carrier gas NitrogenHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.220.22
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.50.50.60.60.
Tend (C) 200.250.250.230.230.
Heat rate (K/min) 5.5.2.2.2.
Initial hold (min)  2.5.  
Final hold (min)    30.30.
I 1668.1651.1651.1638.1641.
ReferenceHnawia, Menut, et al., 2009Ho, Wang, et al., 2009Koba, Sanda, et al., 2009Museli, Pau, et al., 2009Museli, Pau, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1DB-5DB-5HP-5 MSHP-5
Column length (m) 30.30.50.30.30.
Carrier gas HeliumNitrogenNitrogenHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.200.250.25
Phase thickness (mum) 0.250.250.320.250.25
Tstart (C) 40.40.60.50.50.
Tend (C) 300.230.220.280.280.
Heat rate (K/min) 4.2.5.4.9.
Initial hold (min) 2. 3. 3.
Final hold (min) 10. 5. 3.
I 1626.1651.1649.1659.1650.
ReferenceNibret and Wink, 2009Scrivanti, Anton, et al., 2009Shafaghat and Sadeghi, 2009Zhao, Zeng, et al., 2009Aicha, Ines, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5HP-5 MSDB-5
Column length (m) 25.60.25.30.50.
Carrier gas NitrogenNitrogenHeliumHeliumNitrogen
Substrate      
Column diameter (mm) 0.220.250.250.250.20
Phase thickness (mum) 0.250.250.250.250.32
Tstart (C) 50.60.60.50.60.
Tend (C) 300.250.240.230.220.
Heat rate (K/min) 6.55.4.3.5.
Initial hold (min) 2. 2.10.3.
Final hold (min) 7.10. 10.5.
I 1648.1669.1647.1649.1686.
ReferenceChieng, Assim, et al., 2008Mosayebi, Amin, et al., 2008Verdian-rizi, 2008Adams, Beauchamp, et al., 2007Amiri, 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5HP-5MSHP-1
Column length (m) 30.30.30.30.30.
Carrier gas HeHeliumHeliumHeHe
Substrate      
Column diameter (mm) 0.260.260.250.250.25
Phase thickness (mum) 0.250.250.260.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 240.290.240.250.240.
Heat rate (K/min) 3.3.4.2.2.
Initial hold (min)   2.8. 
Final hold (min)   20.15.20.
I 1649.1649.1654.1649.1621.
ReferenceBos, Woerdenbag, et al., 2007Elfami, Bos, et al., 2007Farsam, Amanlou, et al., 2007Ferhat, Tigrine-Kordjani, et al., 2007Hachicha, Skanji, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-101DB-5DB-1SPB-5HP-5MS
Column length (m) 25.30.50.30.30.
Carrier gas HeHeliumHeHeHe
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (mum) 0.20.250.250.250.25
Tstart (C) 70.60.95.50.40.
Tend (C) 200.220.240.250.250.
Heat rate (K/min) 3.4.4.2.3.
Initial hold (min) 2.   5.
Final hold (min)     10.
I 1604.1652.1638.1645.1655.
ReferenceJerkovic, Mastelic, et al., 2007Morteza-Semnani, Saeedi, et al., 2007Pala-Paul, Brophy, et al., 2007Raal, Orav, et al., 2007Vichi, Riu-Aumatell, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5MSHP-5HP-5AT-5
Column length (m) 30.30.30.30.60.
Carrier gas HeHeN2N2He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.320.250.250.250.25
Tstart (C) 60.40.50.50.60.
Tend (C) 250.260.280.280.200.
Heat rate (K/min) 5.4.9.9.4.
Initial hold (min) 30. 3.3. 
Final hold (min)   3.3.20.
I 1650.1645.01635.1646.1650.
ReferenceYassa and Akhani, 2007Zizovic, Stamenic, et al., 2007Abdelwahed, Hayder, et al., 2006Abdelwahed, Hayder, et al., 2006Borges, Rojas, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1HP-5MSSPB-1HP-5DB-5
Column length (m) 50.30.30.25.30.
Carrier gas  HeHeliumHeN2
Substrate      
Column diameter (mm) 0.220.250.200.250.25
Phase thickness (mum) 0.250.250.200.250.25
Tstart (C) 60.60.70.50.70.
Tend (C) 220.280.220.300.230.
Heat rate (K/min) 2.3.3.5.2.
Initial hold (min)    5.2.
Final hold (min) 20. 15. 20.
I 1638.1649.1622.1651.1654.
ReferenceBoti, Yao, et al., 2006Bozin, Mimicá-Dukic, et al., 2006Cavaleiro, Pinto, et al., 2006Champagnat, Figueredo, et al., 2006Choi, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5MSDB-5HP-1CP Sil 5 CB
Column length (m) 30.30.30.50.30.
Carrier gas He HeliumHe 
Substrate      
Column diameter (mm) 0.320.250.260.20.25
Phase thickness (mum) 0.250.250.250.330.25
Tstart (C) 60.60.60.60.40.
Tend (C) 246.280.290.250.220.
Heat rate (K/min) 3.4.3.2.3.
Initial hold (min)      
Final hold (min)    40.3.
I 1650.1649.1649.1627.1651.
ReferenceCoronel, Cerda-Garcia-Rojas, et al., 2006Ebrahim Sajjadi and Mehregan, 2006Elfami, Komar, et al., 2006Filippi, Lanfranchi, et al., 2006Hymete, Rohloff, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSHP-5MSMethyl SiliconeDB-1
Column length (m) 30.30.30.25.60.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.50.50.90.70.
Tend (C) 280.280.280.220.230.
Heat rate (K/min) 5.5.5.7.2.
Initial hold (min) 4.4.4.2.2.
Final hold (min) 10.10.10. 20.
I 1656.1664.1656.1628.1633.
ReferenceKim, Abd El-Aty, et al., 2006Kim, Abd El-Aty, et al., 2006Kim, El-Aty, et al., 2006Kitchlu, Bakshi, et al., 2006Lan Phi N.T., Nishiyama C., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1HP-5DB-5DB-5HP-5
Column length (m) 50.30.30.30.25.
Carrier gas HeHeliumHeHeH2
Substrate      
Column diameter (mm) 0.220.320.250.250.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.40.60.60.60.
Tend (C) 220.240.220.260.240.
Heat rate (K/min) 2.4.4.4.3.
Initial hold (min)    4. 
Final hold (min) 20.5.   
I 1639.1645.1653.1653.1655.
ReferenceLesueur, Ban, et al., 2006Miyazawa and Kawata, 2006Morteza-Semnani, Akbarzadeh, et al., 2006Morteza-Semnani, Saeedi, et al., 2006Potzernheim, Bizzo, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSHP-5MSHP-5MSDB-5
Column length (m) 30.30.30.30.30.
Carrier gas Hydrogen HeHeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 120.50.60.60.40.
Tend (C) 180.250.243.280.260.
Heat rate (K/min) 2.10.3.4.2.
Initial hold (min)  5.  5.
Final hold (min)     20.
I 1644.1667.1642.1652.1648.
ReferencePripdeevech, Wongpornchai, et al., 2006Robinson, 2006Sabulal, Dan, et al., 2006Sajjadi, 2006Senatore, Landolfi, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5 MSDB-5HP-5SPB-1
Column length (m) 60.30.30.30.30.
Carrier gas HeliumHeliumN2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.50.
Tend (C) 250.250.240.250.250.
Heat rate (K/min) 5.2.4.10.4.
Initial hold (min)  8. 2.1.
Final hold (min) 10.15. 10.10.
I 1642.1649.1649.1654.1602.
ReferenceSonboli, Mirjalili, et al., 2006Tigrine-Kordiani, Meklati, et al., 2006Trilles, Bombarda, et al., 2006Wang, Yang, et al., 2006Wong, Sivasothy, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1BPX5HP-5DB-5HP-5MS
Column length (m) 50.25.25.30.25.
Carrier gas HeHeliumHeHeHe
Substrate      
Column diameter (mm) 0.20.220.20.250.25
Phase thickness (mum) 0.50.250.330.25 
Tstart (C) 60.50.60.60.50.
Tend (C) 250.320.240.300.250.
Heat rate (K/min) 2.5.3.3.3.
Initial hold (min)  5. 3.3.
Final hold (min) 60. 7. 10.
I 1632.1637.1644.1650.1651.
ReferenceBendimerad and Bendiab, 2005Dickschat, Bode, et al., 2005Duarte, Figueira, et al., 2005Ferraz, Limberger, et al., 2005Ghasemi Y., Faridi P., et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBHP-5MSHP-5MSHP-5MSDB-5
Column length (m) 25.30.30.30.30.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.150.250.250.25 
Tstart (C) 50.60.60.60.40.
Tend (C) 230.280.275.280.240.
Heat rate (K/min) 3.4.4.4.4.
Initial hold (min)      
Final hold (min)      
I 1644.1648.1649.1648.1647.
ReferenceOgunwande, Olawore, et al., 2005Sajjadi S.E. and Eskandari B., 2005Sajjadi and Ghannadi, 2005Sajjadi, 2005Sefidkon and Jamzad, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSDB-5DB-5PE-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeH2
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.60.60.60.60.
Tend (C) 260.280.300.300.230.
Heat rate (K/min) 2.3.3.3.5.
Initial hold (min) 5.5.  2.
Final hold (min) 20.   4.
I 1648.1648.1645.1644.1635.
ReferenceSenatore, Apostolides Arnold, et al., 2005Setzer, Noletto, et al., 2005Simoes-Pires C.A., Debenedetti S., et al., 2005Simoes-Pires C.A., Debenedetti S., et al., 2005Singh, Raina, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1DB-5MSHP-5HP-5DB-5
Column length (m) 60.30.30.30.30.
Carrier gas HeHeHeliumHeHe
Substrate      
Column diameter (mm) 0.250.250.320.320.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.80.40.60.90.
Tend (C) 250.250.250.260.220.
Heat rate (K/min) 5.5.5.5.7.
Initial hold (min)  2.2.2.2.
Final hold (min) 10.9.5.13.5.
I 1650.1655.1633.1653.1635.
ReferenceSonboli A., Fakhari A.R., et al., 2005Watanabe Y., Mihara R., et al., 2005N/AYayli, Yasar, et al., 2005Agnihotri, Thappa, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1SPB-5DB-5DB-5RTX-1
Column length (m) 50.60.30.30.30.
Carrier gas  HeN2HeN2
Substrate      
Column diameter (mm) 0.220.320.250.250.32
Phase thickness (mum) 0.251.0.250.250.25
Tstart (C) 60.60.40.60.60.
Tend (C) 220.200.230.300.300.
Heat rate (K/min) 2.4.2.3.4.
Initial hold (min)      
Final hold (min) 20.30.   
I 1640.1666.1649.1642.1642.
ReferenceBlanc, Muselli, et al., 2004Gauvin, Ravaomanarivo, et al., 2004González, Guerra, et al., 2004Limberger, Sobral, et al., 2004Lis, Boczek, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSDB-5DB-5NB-30
Column length (m) 30.30.30.50.50.
Carrier gas  HeHeliumHeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (mum) 0.250.25  0.25
Tstart (C) 40.60.60.60.50.
Tend (C) 210.275.240.240.250.
Heat rate (K/min) 2.4.2.2.2.
Initial hold (min) 2.    
Final hold (min) 33. 999.999. 
I 1646.1657.1645.1645.1620.
ReferenceLopez Arze, Collin, et al., 2004Mehrabani, Asadipour, et al., 2004Miyazawa, Fuhita, et al., 2004Miyazawa, Fujita, et al., 2004Orav, Stulova, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase NB-30HP-5DB-5CP Sil 5 CBHP-5MS
Column length (m) 50.25.30.20.30.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.20.20.250.250.25
Phase thickness (mum) 0.250.50.250.250.25
Tstart (C) 50.30.60.100.60.
Tend (C) 250.280.240.270.280.
Heat rate (K/min) 2.3.3.8.3.
Initial hold (min)    2. 
Final hold (min)      
I 1619.1670.1647.1630.1649.
ReferenceOrav, Stulova, et al., 2004Shafi, Nambiar, et al., 2004Tellez, Khan, et al., 2004Thappa, Bakshi, et al., 2004Couladis, Özcan, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5MSRSL-200DB-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas N2HeH2HeHelium
Substrate      
Column diameter (mm) 0.250.250.320.250.32
Phase thickness (mum) 0.250.250.250.25 
Tstart (C) 50.60.40.60.70.
Tend (C) 200.280.280.250.210.
Heat rate (K/min) 5.4.6.3.2.
Initial hold (min)   5.  
Final hold (min)   5. 60.
I 1619.1649.1644.1644.1649.
ReferenceFekam Boyom, Ngouana, et al., 2003Ghasemi, Asghari, et al., 2003Jirovetz, Buchbauer, et al., 2003Limberger, Simões-Pires, et al., 2003Mookdasanit, Tamura, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-55 % Phenyl methyl siloxaneBP-1
Column length (m) 30.30.30.30.25.
Carrier gas N2HeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.50
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.60.60.75.60.
Tend (C) 230.240.280.200.220.
Heat rate (K/min) 2.3.3.3.5.
Initial hold (min)    4. 
Final hold (min)   30.8.10.
I 1649.1650.1640.1651.1631.
ReferenceRotman, Ahumada, et al., 2003da Silva, Luz, et al., 2003Caredda, Marongiu, et al., 2002Cicció and Gómez-Laurito, 2002Das, Ram, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5RSL-200DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas N2N2H2 He
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.50.40.40.35.
Tend (C) 250.250.280.210.280.
Heat rate (K/min) 4.4.6.2.4.
Initial hold (min)  5.5.2.2.
Final hold (min)   5.33.15.
I 1649.1649.1630.1653.1664.
ReferenceFarah, Fechtal, et al., 2002Farah, Fechtal. M., et al., 2002Jirovetz, Buchbauer, et al., 2002Kabouss, Charrouf, et al., 2002Krauze-Baranowska, Mardarowicz, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-5HP-5DB-1DB-1
Column length (m) 25.30.30.30.60.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (mum)  0.250.250.25 
Tstart (C) 50.60.60.60.40.
Tend (C) 200.250.275.250.250.
Heat rate (K/min) 5.3.4.4.4.
Initial hold (min)   4.10. 
Final hold (min)      
I 1650.1643.1646.1668.1612.
ReferenceKuiate, Bessière, et al., 2002Limberger, Simões-Pires, et al., 2002Lockwood, Asghari, et al., 2002Norouzi-Arasi, Yavari, et al., 2002Sefidkon, Dabiri, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSHP-5BP-1RSL-200RTX-1
Column length (m) 30.30.30.30.30.
Carrier gas HeN2N2H2N2
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.40.60.
Tend (C) 270.220.220.280.300.
Heat rate (K/min) 3.5.5.6.4.
Initial hold (min)  10. 5. 
Final hold (min)    5. 
I 1650.1651.1631.1677.1648.
ReferenceZoghbi, Andrade, et al., 2002Flamini, Cioni, et al., 2001Gupta, Mallavarapu, et al., 2001Jirovetz L., Buchbauer G., et al., 2001Kalemba, Marschall, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-1DB-1DB-5DB-1
Column length (m) 30.30.30.30.25.
Carrier gas HeN2HeHeNitrogen
Substrate      
Column diameter (mm) 0.250.250.20.250.50
Phase thickness (mum) 0.250.25 0.250.25
Tstart (C) 60.80.60.60.60.
Tend (C) 240.225.240.240.220.
Heat rate (K/min) 3.4.3.3.5.
Initial hold (min)      
Final hold (min) 30.    
I 1628.1616.1646.51649.1630.
ReferenceMarongiu, Porcedda, et al., 2001Palá-Paúl, Pérez-Alonso, et al., 2001Santos, Moreira, et al., 2001Tellez M., Estell R., et al., 2001Mallavarapu, Rao, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101BP-1DB-1CP Sil 5 CBDB-5MS
Column length (m) 25.25.50.25.30.
Carrier gas N2N2HeN2He
Substrate      
Column diameter (mm) 0.250.500.25 0.25
Phase thickness (mum)  0.250.250.390.25
Tstart (C) 50.60.70.60.60.
Tend (C) 200.220.240.220.240.
Heat rate (K/min) 5.5.4.5.3.
Initial hold (min)      
Final hold (min)  10.   
I 1643.1631.1617.1643.1655.
ReferenceAyedoun, Adéoti, et al., 1999Mallavarapu, Kulkarni, et al., 1999Palá-Paúl, Pérez-Alonso, et al., 1999Weyerstahl, Marschall, et al., 1999Zoghbi, Andrade, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5OV-1DB-5HP-1DB-5
Column length (m) 50.50.30.60.30.
Carrier gas HeHeHeliumHeHe
Substrate      
Column diameter (mm) 0.320.320.250.250.32
Phase thickness (mum) 0.250.250.250.25 
Tstart (C) 60.50.60.50.60.
Tend (C) 240.250.240.280.250.
Heat rate (K/min) 3.10.3.4.3.
Initial hold (min)  5. 5. 
Final hold (min) 20.20.   
I 1661.1643.1651.1665.1645.
ReferenceDoneanu and Anitescu, 1998Kökdil, Kurucu, et al., 1998Santos, Andrade, et al., 1998Stashenko, Cervantes, et al., 1998Abreu and Noronha, 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-1DB-5CBP-1HP-1
Column length (m) 25. 30.25.23.
Carrier gas He HeliumHeHe
Substrate      
Column diameter (mm) 0.25 0.250.220.32
Phase thickness (mum) 0.25 0.25 0.17
Tstart (C) 60.80.60.60.60.
Tend (C) 300.220.240.240.250.
Heat rate (K/min) 6.6.3.5.5.
Initial hold (min)     3.
Final hold (min)     30.
I 1613.1620.1650.1634.1628.
ReferenceBos, Woerdenbag, et al., 1997Salgueiro, Vila, et al., 1997Tellez, Estell, et al., 1997Zygadlo, Ariza-Espinar, et al., 1997Ayedoun, Adeoti, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillary
Active phase OV-101SPB-1CP Sil 5 CBDB-1
Column length (m) 50.50.25.60.
Carrier gas N2He Hydrogen
Substrate     
Column diameter (mm) 0.250.20.250.25
Phase thickness (mum) 0.170.33 0.25
Tstart (C) 50.40.60.50.
Tend (C) 220.200.280.238.
Heat rate (K/min) 5.3.5.4.
Initial hold (min)  3.  
Final hold (min)  30. 8.
I 1650.1634.1642.1638.
ReferenceChacko, Jayalekshmy, et al., 1996Wong and Lai, 1996Kaul, Singh, et al., 1993Kesselmans and Wijnberg, 1992
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Pinheiro, de Queiros, et al., 2013
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Hnawia, Menut, et al., 2009
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Koba, Sanda, et al., 2009
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Museli, Pau, et al., 2009
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Nibret and Wink, 2009
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Scrivanti, Anton, et al., 2009
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Shafaghat and Sadeghi, 2009
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Zhao, Zeng, et al., 2009
Zhao, C.; Zeng, Y.; Wan, M.; Li, R.; Liang, Y.; Li, C.; Zeng, Z.; Chau, F.-T., Comparative analysis of essential oils from eight herbal medicines with pungent flavor and cool nature by GC-MS and chemometric resolution methods, J. Sep. Sci., 2009, 32, 4, 660-670, https://doi.org/10.1002/jssc.200800484 . [all data]

Aicha, Ines, et al., 2008
Aicha, N.; Ines, S.; Mohamed, B.S.; Ines, B.; Soumaya, K.; Kamel, G.; Mohamed, N.; Imed, C.; Mohamed, H.; Leila, C.-G., Chemical composition, mutagenic and antimutagenic activities of essential oils from (Tunisian) Artemisia campestris and Artemisia herba-alba, J. Ess. Oil Res., 2008, 20, 5, 471-477. [all data]

Chieng, Assim, et al., 2008
Chieng, T.C.; Assim, Z.B.; Fasihuddin, B.A., Toxicity and antitermite activities of the essential oils from Piper sarmentosum, The Malaysian J. Anal. Sci., 2008, 12, 1, 234-239. [all data]

Mosayebi, Amin, et al., 2008
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Verdian-rizi, 2008
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Adams, Beauchamp, et al., 2007
Adams, R.P.; Beauchamp, P.S.; Dev, V.; Dutz, S.M., New Natural Products Isolated from One-Seeded Juniperus of the Southwestern United States: Isolation and Occurence of 2-Ethenyl-3-methyl Phanol and Its Derivatives, J. Essent. Oil Res., 2007, 19, 2, 146-152, https://doi.org/10.1080/10412905.2007.9699247 . [all data]

Amiri, 2007
Amiri, H., Quantative and qualative changes of essential oil of Salvia bracteata BAnk et Sol. in different growth stages, DARU, 2007, 15, 2, 79-82. [all data]

Bos, Woerdenbag, et al., 2007
Bos, R.; Woerdenbag, H.J.; Kayser, O.; Quax, W.J.; Ruslan, K.; Elfami, Essential oil constituents of Piper cubeba L. fils. from Indonesia, J. Essent. Oil Res., 2007, 19, 1, 14-17, https://doi.org/10.1080/10412905.2007.9699217 . [all data]

Elfami, Bos, et al., 2007
Elfami; Bos, R.; Ruslan, K.; Woerdenbag, H.J.; Kayser, P.; Quax, W.J., Essential Oil Constituents of Piper cubeba from Indonesia, 2007, 53-60. [all data]

Farsam, Amanlou, et al., 2007
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Hachicha, Skanji, et al., 2007
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Jerkovic, Mastelic, et al., 2007
Jerkovic, I.; Mastelic, J.; Marijanovic, Z., Bound volatile compounds and essential oil from the fruit of Maclura pomifera (Raf.) Schneid. (osage orange), Flavour Fragr. J., 2007, 22, 1, 84-88, https://doi.org/10.1002/ffj.1763 . [all data]

Morteza-Semnani, Saeedi, et al., 2007
Morteza-Semnani, K.; Saeedi, M.; Akbarzadeh, M., Essential oil composition of Teucrium scordium L., Acta Pharm., 2007, 57, 4, 499-504, https://doi.org/10.2478/v10007-007-0040-6 . [all data]

Pala-Paul, Brophy, et al., 2007
Pala-Paul, J.; Brophy, J.J.; Perez-Alonso, M.J.; Usano, J.; Soria, S.C., Essential oil composition of the different parts of Eryngium corniculatum Lam. (Apiaceae) from Spain, J. Chromatogr. A, 2007, 1175, 2, 289-293, https://doi.org/10.1016/j.chroma.2007.10.061 . [all data]

Raal, Orav, et al., 2007
Raal, A.; Orav, A.; Arak, E.; Kailas, T.; Müürisepp, M., Variation in the composition of the essential oil of Valeriana officinalis L. roots from Estonia, Proc. Est. Acad. Sci. Chem., 2007, 56, 2, 67-74. [all data]

Vichi, Riu-Aumatell, et al., 2007
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Yassa and Akhani, 2007
Yassa, N.; Akhani, H., The essential oils composition in two species of the genus Eriocycla Lindl. (Apiaceae) from Iran, 2007, retrieved from http://biology.ut.ac.ir/members/akhani/PdfReprintNumber/27.pdf. [all data]

Zizovic, Stamenic, et al., 2007
Zizovic, I.; Stamenic, M.; Ivanovic, J.; Orlovic, A.; Ristic, M.; Djordjevic, S.; Petrovic, S.D.; Skala, D., Supercritical carbon dioxide extraction of sesquiterpenes from valerian root, J. Supercrit. Fluids, 2007, 43, 2, 249-258, https://doi.org/10.1016/j.supflu.2007.05.007 . [all data]

Abdelwahed, Hayder, et al., 2006
Abdelwahed, A.; Hayder, N.; Kilani, S.; Mahmoud, A.; Chibani, J.; Hammami, M.; Chekir-Ghedira, L.; Ghedira, K., Chemical composition and antimicrobial activity of essential oils from Tunisian Pituranthos tortuosus (Coss.) Maire, Flavour Fragr. J., 2006, 21, 1, 129-133, https://doi.org/10.1002/ffj.1542 . [all data]

Borges, Rojas, et al., 2006
Borges, R.; Rojas, L.B.; Cegarra, J.A.; Usubillaga, A., Study of the essential oils from the leaves and flowers of Lepechinia conferta (Benth) Epl., Flavour Fragr. J., 2006, 21, 1, 155-157, https://doi.org/10.1002/ffj.1550 . [all data]

Boti, Yao, et al., 2006
Boti, J.B.; Yao, P.A.; Koukoua, G.; N'Guessan, T.Y.; Casanova, J., Components and chemical variability of Isolona campanulata Engler Diels leaf oil, Flavour Fragr. J., 2006, 21, 1, 166-170, https://doi.org/10.1002/ffj.1555 . [all data]

Bozin, Mimicá-Dukic, et al., 2006
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Cavaleiro, Pinto, et al., 2006
Cavaleiro, C.; Pinto, E.; Gonsales, M.J.; Salguero, L., Antifungal activity of Juniperus essential oils agains dermatophyte, Asrgillus and Candida strains, J. Appl. Microbiol., 2006, 100, 6, 1333-1338, https://doi.org/10.1111/j.1365-2672.2006.02862.x . [all data]

Champagnat, Figueredo, et al., 2006
Champagnat, P.; Figueredo, G.; Chalchat, J.-C.; Bessiere, J.-M., Essential oil composition of Vetiveria nigritana from Mali, J. Essent. Oil Res., 2006, 18, 6, 647-649, https://doi.org/10.1080/10412905.2006.9699193 . [all data]

Choi, 2006
Choi, H.-S., Headspace analyses of fresh leaves and stems of Angelica gigas Nakai, a Korean medicinal herb, Flavour Fragr. J., 2006, 21, 4, 604-608, https://doi.org/10.1002/ffj.1602 . [all data]

Coronel, Cerda-Garcia-Rojas, et al., 2006
Coronel, A. del.C.; Cerda-Garcia-Rojas, C.M.; Joseph-Nathan, P.; Catalán, C.A.N., Chemical composition, seasonal variation and a new sesquiterpene alcohol from the essential oil of Lippia integrifolia, Flavour Fragr. J., 2006, 21, 5, 839-847, https://doi.org/10.1002/ffj.1736 . [all data]

Ebrahim Sajjadi and Mehregan, 2006
Ebrahim Sajjadi, S.; Mehregan, I., Volatile constituents of flowers and leaves of Anthemis hyalina, Chem. Nat. Compd. (Engl. Transl.), 2006, 42, 5, 531-533, https://doi.org/10.1007/s10600-006-0207-2 . [all data]

Elfami, Komar, et al., 2006
Elfami, R.B.; Komar, R.; Woerdenbag, H.J.; Kayser, P.; Quax, W.J., Essential oil constituents of Piper cubeba from Indonesia, 2006, retrieved from http://dissertations.ub.rug.nl/FILES/facultiew/science/2006/elfahmi/05c5.pdf. [all data]

Filippi, Lanfranchi, et al., 2006
Filippi, J.-J.; Lanfranchi, D.-A.; Prado, S.; Baldovini, N.; Meierhenrich, U.J., Composition, Enantiomeric Distribution, and Antibacterial Activity of the Essential Oil of Achillea ligustica All. from Corsica, J. Agric. Food Chem., 2006, 54, 17, 6308-6313, https://doi.org/10.1021/jf060752y . [all data]

Hymete, Rohloff, et al., 2006
Hymete, A.; Rohloff, J.; Iversen, T.-H., Essential oil from seeds and husks of Aframomum corrorima from Ethiopia, Flavour Fragr. J., 2006, 21, 4, 642-644, https://doi.org/10.1002/ffj.1634 . [all data]

Kim, Abd El-Aty, et al., 2006
Kim, M.R.; Abd El-Aty, A.M.; Kim, I.S.; Shim, J.H., Determination of volatile flavor components in danggui cultivars by solvent free injection and hydrodistillation followed by gas chromatographic-mass spectrometric analysis, J. Chromatogr. A, 2006, 1116, 1-2, 259-264, https://doi.org/10.1016/j.chroma.2006.03.060 . [all data]

Kim, El-Aty, et al., 2006
Kim, M.R.; El-Aty, A.M.A.; Choi, J.-H.; Lee, K.B.; Shim, J.H., Identification of volatile components in Angelica species using supercritical-CO2 fluid extraction and solid phase microextraction coupled to gas chromatography-mass spectrometry, Biomedical Chromatography, 2006, 20, 11, 1267-1273, https://doi.org/10.1002/bmc.696 . [all data]

Kitchlu, Bakshi, et al., 2006
Kitchlu, S.; Bakshi, S.K.; Kaul, M.K.; Bhan, M.K.; Thapa, R.K.; Agarwal, S.G., Tanacetum gracile Hook. f T. A new source of lavandulol from Ladakh Himalaya (India), Flavour Fragr. J., 2006, 21, 4, 690-692, https://doi.org/10.1002/ffj.1674 . [all data]

Lan Phi N.T., Nishiyama C., et al., 2006
Lan Phi N.T.; Nishiyama C.; Choi H.-S.; Sawamura M., Evaluation of aroma characteristic compounds of Citrus natsudaidai Hayata (Natsudaidai) cold-pressed peel oil, Biosci. Biotechnol. Biochem., 2006, 70, 8, 1832-1838, https://doi.org/10.1271/bbb.50705 . [all data]

Lesueur, Ban, et al., 2006
Lesueur, D.; Ban, N.K.; Bighelli, A.; Muselli, A.; Casanova, J., Analysis of the root oil of Fokienia hodginsii (Dunn) Henry et Thomas (Cupressaceae) by GC, GC-MS and 13C-NMR, Flavour Fragr. J., 2006, 21, 1, 171-174, https://doi.org/10.1002/ffj.1557 . [all data]

Miyazawa and Kawata, 2006
Miyazawa, M.; Kawata, J., Identification of the Key Aroma Compounds in Dried Roots of Rubia cordifolia, L. Oleo Sci., 2006, 55, 1, 37-39, https://doi.org/10.5650/jos.55.37 . [all data]

Morteza-Semnani, Akbarzadeh, et al., 2006
Morteza-Semnani, K.; Akbarzadeh, M.; Changizi, S., Essential oils composition of Stachys byzantina, S. inflata, S. lavandulifolia and S. laxa from Iran, Flavour Fragr. J., 2006, 21, 2, 300-303, https://doi.org/10.1002/ffj.1594 . [all data]

Morteza-Semnani, Saeedi, et al., 2006
Morteza-Semnani, K.; Saeedi, M.; Akbarsadeh, M.; Moshiri, K., The essential oil composition of Onosma microcarpum DC., Flavour Fragr. J., 2006, 21, 2, 314-316, https://doi.org/10.1002/ffj.1597 . [all data]

Potzernheim, Bizzo, et al., 2006
Potzernheim, M.C.L.; Bizzo, H.R.; Vieira, R.F., Analysis of the essential oil of three species of Piper collected in the region of the Distrito Federal (Cerrado - Brazilian Savannah) and comparison with oils of plants from region of Paraty, State of Rio de Janeiro (Atlantic Rain Forest), Brazilian Journal of Pharmacognosy, 2006, 16, 2, 246-251. [all data]

Pripdeevech, Wongpornchai, et al., 2006
Pripdeevech, P.; Wongpornchai, S.; Promsiri, A., Highly Volatile Constituents of Vetiveria zizanioides Roots Grown under Different Cultivation Conditions, Molecules, 2006, 11, 10, 817-826, https://doi.org/10.3390/11100817 . [all data]

Robinson, 2006
Robinson, C.J., A new essential oil - Agonis fragrans, A report for the Rural Industries Research and Development Corporation, RIRDC Publication No. 06/090, Rural Industries Research and Development Corporation, Barton, ACT, 2006, 12. [all data]

Sabulal, Dan, et al., 2006
Sabulal, B.; Dan, M.; Pradeep, N.S.; Valsamma, R.K.; George, V., Composition and antimicrobial activity of essential oil from the fruits of Amomum cannicarpum, Acta Pharm. Sin., 2006, 56, 473-480. [all data]

Sajjadi, 2006
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Notes

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