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2-Naphthalenemethanol, decahydro-«alpha»,«alpha»,4a-trimethyl-8-methylene-, [2R-(2«alpha»,4a«alpha»,8a«beta»)]-


Normal alkane RI, non-polar column, custom temperature program

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase TR-5 MSTR-5 MSRTX-5 MSDB-15 % Phenyl polydimethyl siloxane
Column length (m) 15.15.30.30. 
Carrier gas HeliumHeliumHeliumHydrogen 
Substrate      
Column diameter (mm) 0.250.250.250.25 
Phase thickness (mum) 0.250.25 0.25 
Program 35 0C (3 min) 2 0C/min -> 60 0C (3 min) 2 0C/min -> 80 0C (3 min) 4 0C/min -> 120 0C (3 min) 5 0C/min -> 150 0C (3 min) 15 0C/min -> 240 0C (10 min)35 0C (3 min) 2 0C/min -> 60 0C (3 min) 2 0C/min -> 80 0C (3 min) 4 0C/min -> 120 0C (3 min) 5 0C/min -> 150 0C (3 mion) 15 0C/min -> 240 0C (10 min)not specified45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min)not specified
I 1639.1646.1649.1620.1655.
ReferenceKurashov, Mitrukova, et al., 2014Kurashov, Krylova, et al., 2013Pinheiro, de Queiros, et al., 2013Albano, Lima, et al., 2012Chaverri, Diaz, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CBP-5HP-5HP-5 MSHP-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHelium Helium
Substrate      
Column diameter (mm) 0.250.320.250.320.25
Phase thickness (mum) 0.250.250.25 0.25
Program 60 0C 3 0C/min -> 246 0C 10 0C/min -> 270 0C (5 min)not specified40 0C (5 min) 2 0C/min -> 270 0C -> 260 0C (20 min)not specified50 0C 95 min) 3 0C/min -> 100 0C 4 0C/min -> 160 0C 5 0C/min -> 220 0C (15 min)
I 1654.1651.1650.1649.1662.
ReferenceFortes, Naves, et al., 2011Kahriman, Tosun, et al., 2011Mancini, Arnold, et al., 2009Riahi, Pourbasheer, et al., 2009Yang, Yang, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5SLB-5 MSSLB-5 MSCP Sil 8 CBRTX-5
Column length (m) 25.30.30.30.30.
Carrier gas NitrogenHeliumHelium Helium
Substrate      
Column diameter (mm) 0.220.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Program not specified50 0C 3 0C/min -> 250 0C (1 min) 10 0C/min -> 300 0C (5 min)not specified60C => 2.5C/min => 170C => 10C/min => 250C (5min)60 0C (5 min) 5 0C/min -> 110 0C 3 0C/min -> 220 0C (5 min)
I 1648.1658.1649.1649.1656.
ReferenceChieng, Assim, et al., 2008Costa, De Fina, et al., 2008Costa, De Fina, et al., 2008Kristiawan, Sobolik, et al., 2008Zachariah, Leela, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5HP-5MSHP-5MSDB-1HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeHeH2He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Program not specified40C(10min) => 3C/min => 200C => 2C/min => 220C40C(5min) => 2C/min => 250C(15min) => 10C/min => 270C45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min)40C(3min) => 8C/min => 160C => 15C/min => 300C (10min)
I 1649.1648.1650.1620.1661.
ReferenceZachariah, Leela, et al., 2008Cole, Haber, et al., 2007Formisano, Mignola, et al., 2007Kamatou, Viljoen, et al., 2007Liu, Song, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1HP-5MSDB-5HP-5 MSHP-5MS
Column length (m) 30.30.50.30.30.
Carrier gas HeHeHeliumHeliumHe
Substrate      
Column diameter (mm) 0.20.250.320.250.25
Phase thickness (mum) 0.330.250.25  
Program 60C(5min) => 3C/min => 180C => 20C/min => 280C(10min)40C(3min) => 8C/min => 160C => 15C/min => 300C60 0C (1 min) 5 0C/min -> 160 0C 10 0C/min -> 250 0C40 0C (10 min) 3 oC/min -> 200 0C 2 0C/min -> 220 0C40C(10min) => 3C/min => 200C => 2C/min => 220C
I 1649.1647.1651.1648.1650.
ReferenceMerle, Verdeguer, et al., 2007Mu, Wang, et al., 2007Nivinsliene, Butkiene, et al., 2007Setzer, Stokes, et al., 2007Takaku, Haber, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5HP-5 MSHP-5MSDB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHydrogenHeliumHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (mum) 0.250.250.250.250.25
Program 40C(1min) => 8C/min => 160C => 12C/min => 300C(5min)not specified40 0C (10 min) 3 0C/min -> 200 0C 2 0C/min -> 220 0C40C(5min) => 2C/min => 250C (15min) => 10C/min => 270C60C => 2C/min => 100C => 3C/min => 160C => 5C/min => 280C
I 1645.1651.1649.1650.1638.
ReferenceLi, Deng, et al., 2006Pripdeevech, Wongpornchai, et al., 2006Schmidt, Noletto, et al., 2006Senatore, Apostolides Arnold, et al., 2006Srivastava, Mallavarapu, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-52DB-5BPX5DB-5Methyl Silicone
Column length (m) 30.30.25.30. 
Carrier gas HeHeHeliumHe 
Substrate      
Column diameter (mm) 0.320.250.220.25 
Phase thickness (mum) 0.150.250.250.25 
Program 45C => 1C/min => 100C => 5C/min => 250C (10min)35C => 4C/min => 180C => 10C/min => 250Cnot specified40C(1min) => 9C/min => 130C => 2C/min => 230Cnot specified
I 1651.1646.1641.1649.1649.
ReferenceTognolini, Barocelli, et al., 2006Cysne, Canuto, et al., 2005Dickschat, Bode, et al., 2005Hamm, Bleton, et al., 2005Couladis, Özcan, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase  OV-1BPX-5DB-1HP-5
Column length (m)  30.30.30.30.
Carrier gas  HeH2He 
Substrate      
Column diameter (mm)  0.250.250.250.25
Phase thickness (mum)  0.250.250.250.25
Program not specified45 0C (4 min) 3 0C/min -> 75 0C 4 0C/min -> 115 0C 6 0C/min -> 312 0C50 0C (1 min) 3 0C/min -> 150 0C 5 0C/min -> 250 0C (5 min)45C => 3C/min => 175C => 15C/min => 300C (10min)40C(5min) => 2C/min => 250C(15min) => 10C/min => 270C
I 1633.1634.1651.1620.1650.
ReferenceEl-Shazily, Hafez, et al., 2004Hafez and Abdel-Salam, 2004Koba, Sanda, et al., 2004Miguel, Simões, et al., 2004Senatore, Apostolides Arnold, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5SE-30SE-30DB-5DB-1
Column length (m) 30.  30.30.
Carrier gas He  HeHe
Substrate      
Column diameter (mm) 0.25  0.250.25
Phase thickness (mum) 0.25  0.250.1
Program 50C (3min) => 3C/min => 150C (10min) => 10C/min => 250Cnot specifiednot specified40C (1min) => 9C/min => 130C => 2C/min => 230C35C => 4C/min => 180C => 10C/min => 250C
I 1651.1633.1634.1649.1630.
ReferenceTepe, Donmez, et al., 2004Vinogradov, 2004Vinogradov, 2004Hamm, Lesellier, et al., 2003Silva, Matos, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30SE-30DB-1CP Sil 5 CBCP Sil 5 CB
Column length (m) 60.60.30.25.25.
Carrier gas HeHe N2 
Substrate      
Column diameter (mm) 0.250.250.25  
Phase thickness (mum)   0.250.39 
Program 50 0C (5 min) 5 0C/min -> 165 0C 4 0C/min -> 230 0Cnot specified45 0C 3 K/min -> 175 0C 15 K/min -> 300 0C (10 min)not specifiednot specified
I 1658.1657.1620.1640.1638.
ReferenceLi, Wu, et al., 2002Li, Wu, et al., 2002Figueiredo, Miguel, et al., 2001Weyerstahl, Marschall, et al., 2000Weyerstahl, Marschall, et al., 2000, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-1CP Sil 5 CBCP Sil 5 CBPolydimethyl siloxanes
Column length (m) 25.30.25.30. 
Carrier gas HeH2HeN2 
Substrate      
Column diameter (mm)  0.25 0.25 
Phase thickness (mum) 0.390.250.39  
Program not specified45C => 3C/min => 175C => 15C => 240C(10min)not specifiednot specifiednot specified
I 1644.1620.1635.1637.1634.
ReferenceWeyerstahl, Marschall, et al., 1999da Silva, Figueiredo, et al., 1998Weyerstahl, Marschall, et al., 1998Weyerstahl, Marschall, et al., 1997Zenkevich, 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase DB-1
Column length (m) 30.
Carrier gas H2
Substrate  
Column diameter (mm) 0.25
Phase thickness (mum) 0.25
Program 45 0C 3 0C/min -> 175 0C 15 0C/min -> 240 0C (10 min)
I 1620.
ReferenceBarroso, Figueiredo, et al., 1996
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Kurashov, Mitrukova, et al., 2014
Kurashov, E.A.; Mitrukova, G.G.; Krylova, Yu.V., Variations in the component composition of essential oil of Ceratophyllum demersum (Ceratophyllaceae) during vegetation (in press), Plant Resources (Rastitel'nye Resursy), 2014, 1, 000-000. [all data]

Kurashov, Krylova, et al., 2013
Kurashov, E.A.; Krylova, Yu.V.; Mitrukova, G.G., Variations in component composition of essential oil of Potamogeton pusillus (Potamogetonaceae) dirong vegetation, Plant Resources (Rastitel'nye Resursy), 2013, 000-000. [all data]

Pinheiro, de Queiros, et al., 2013
Pinheiro, P.F.; de Queiros, V.T.; Rondelli, V.M.; Costa, A.V.; MArcelino, T. deP.; Pratissoli, D., Insecticidal activity of citronells grass essential oil on Frankliniella schultzei and Myzus persicae, Cienc. Agrotec. Lavras, 2013, 37, 2, 138-144, https://doi.org/10.1590/S1413-70542013000200004 . [all data]

Albano, Lima, et al., 2012
Albano, S.M.; Lima, A.S.; Miguel, M.G.; Pedro, L.G.; Barroso, J.G.; Figueiredo, A.C., Antioxidant, anti-5-lipoxygenase and antiacetylcholinesterase activities of essential oils and decoction water of some aromatic plants, Rec. Nat. Prod., 2012, 6, 1, 35-48. [all data]

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Chaverri, C.; Diaz, C.; Cicco, J.F., Chemical analysis of essential oils from Ocotea gomezii W.C. Burger and Ocotea morae Gomez-Laur. (Lauraceae) collected at Reserva biologica Alberto M. Brenes in Costa Rica and their cytotoxic activity on Tumor cell lines, J. Braz. Chem. Soc., 2011, 22, 4, s1-s4, https://doi.org/10.1590/S0103-50532011000400018 . [all data]

Fortes, Naves, et al., 2011
Fortes, G.A.C.; Naves, S.S.; Godoi, F.F.F.; Duarte, A.R.; Ferri, P.H.; Santos, S.C., Assessment of a maturity index in Jabuticaba fruit by the evaluation of phenolic compounds, essential oil components, sugar content and total acidity, Amer. J. Food Technol., 2011, 6, 11, 974-984, https://doi.org/10.3923/ajft.2011.974.984 . [all data]

Kahriman, Tosun, et al., 2011
Kahriman, N.; Tosun, G.; Terzioglu, S.; Karaoglu, S.A.; Yayh, N., Chemical composition and antimicrobial activity of the essential oils from the flower, leaf, and stem of Senecio pandurifolis, Rec. Nat. Prod., 2011, 5, 2, 82-91. [all data]

Mancini, Arnold, et al., 2009
Mancini, E.; Arnold, N.A.; De Martino, L.; De Feo, V.; Formisano, C.; Rigano, D.; Senatore, F., Chemical composition and phytotoxic effects of essential oils of Salvia hierosolymitana Boiss. and Salvia multicaulis Vahl. var. simplicifolia Boiss. growing wild in Lebanon, Molecules, 2009, 14, 11, 4725-4736, https://doi.org/10.3390/molecules14114725 . [all data]

Riahi, Pourbasheer, et al., 2009
Riahi, S.; Pourbasheer, E.; Ganjali, M.R.; Norouzi, P., Investigation of different linear and non-linear chemometric methods for modeling of retention index of essential oil components: Concerns to support vector mashine, J. Hazard. Mat., 2009, 166, 2-3, 853-859, https://doi.org/10.1016/j.jhazmat.2008.11.097 . [all data]

Yang, Yang, et al., 2009
Yang, Z.; Yang, W.; Peng, Q.; He, Q.; Feng, Y.; Luo, S.; Yu, Z., Volatile phytochemical composition of rhisome of ginger after extraction by headspace solid-phase microextraction, petrol ether extraction and steam distillation extraction, Bangladesh J. Pharmacol., 2009, 4, 2, 136-143, https://doi.org/10.3329/bjp.v4i2.3232 . [all data]

Chieng, Assim, et al., 2008
Chieng, T.C.; Assim, Z.B.; Fasihuddin, B.A., Toxicity and antitermite activities of the essential oils from Piper sarmentosum, The Malaysian J. Anal. Sci., 2008, 12, 1, 234-239. [all data]

Costa, De Fina, et al., 2008
Costa, R.; De Fina, M.R.; Valentino, M.R.; Rustaiyan, A.; Dugo, P.; Dugo, G.; Mondello, L., An investigation on the volatile composition of some Artemisia species from Iran, Flavour Fragr. J., 2008, 24, 2, 75-82, https://doi.org/10.1002/ffj.1919 . [all data]

Kristiawan, Sobolik, et al., 2008
Kristiawan, M.; Sobolik, V.; Al-Haddad, M.; Allaf, K., Effect of pressure-drop rate on the isolation of cananga oil using instantaneous controlled pressure-drop process, Chem. Eng. Processing, 2008, 47, 1, 66-75, https://doi.org/10.1016/j.cep.2007.08.011 . [all data]

Zachariah, Leela, et al., 2008
Zachariah, T.J.; Leela, N.K.; Maya, K.M.; Rema, J.; Mathew, P.A.; Vipin, T.M.; Krishnamoorthy, B., Chemical composition of leaf oils of Myristica beddomeii (King), Myristica fragrans (Houtt.) and Myristica malabarica (Lamk.), J. Spices Arom. Crops, 2008, 17, 1, 10-15. [all data]

Cole, Haber, et al., 2007
Cole, R.A.; Haber, W.A.; Setzer, W.N., Chemical composition of essential oils of seven species of Eugenia from Monteverde, Costa Rica, Biochem. Syst. Ecol., 2007, 35, 12, 877-886, https://doi.org/10.1016/j.bse.2007.06.013 . [all data]

Formisano, Mignola, et al., 2007
Formisano, C.; Mignola, E.; Rigano, D.; Senatore, F.; Bellone, G.; Bruno, M.; Rosselli, S., Chemical composition and antimicrobial activity of the essential oil from aerial parts of Micromeria fruticulosa (Bertol.) Grande (Lamiaceae) growing wild in Southern Italy, Flavour Fragr. J., 2007, 22, 4, 289-292, https://doi.org/10.1002/ffj.1795 . [all data]

Kamatou, Viljoen, et al., 2007
Kamatou, G.P.P.; Viljoen, A.M.; Figueiredo, A.C.; Tilney, P.M.; Van Zyl, R.L.; Barroso, J.G.; Pedro, L.G.; Van Vuuren, S.F., Trichomes, essential oil composition and biological activities of Salvia albanicus Benth. and S. dolomitica Codd, two species from the Cape region of Soith Africa, South African J. Botany, 2007, 73, 1, 102-108, https://doi.org/10.1016/j.sajb.2006.08.001 . [all data]

Liu, Song, et al., 2007
Liu, L.; Song, G.; Hu, Y., GC?MS Analysis of the Essential Oils of Piper nigrum L. and Piper longum L., Chromatographia, 2007, 66, 9-10, 785-790, https://doi.org/10.1365/s10337-007-0408-2 . [all data]

Merle, Verdeguer, et al., 2007
Merle, H.; Verdeguer, M.; Blázquez, M.A.; Boira, H., Chemical composition of the essential oils from Eriocephalus africanus L. var. africanus populations growing in Spain, Flavour Fragr. J., 2007, 22, 6, 461-464, https://doi.org/10.1002/ffj.1821 . [all data]

Mu, Wang, et al., 2007
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Takaku, Haber, et al., 2007
Takaku, S.; Haber, W.A.; Setzer, W.N., Leaf essential oil composition of 10 species of Ocotea (Lauraceae) from Monteverde, Costa Rica, Biochem. Syst. Ecol., 2007, 35, 8, 525-532, https://doi.org/10.1016/j.bse.2007.02.003 . [all data]

Li, Deng, et al., 2006
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Pripdeevech, Wongpornchai, et al., 2006
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Schmidt, Noletto, et al., 2006
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Senatore, Apostolides Arnold, et al., 2006
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Srivastava, Mallavarapu, et al., 2006
Srivastava, S.; Mallavarapu, G.R.; Rai, S.K.; Singh, D.; Mishra, R.; Pandey-Rai, S.; Kumar, S., Composition of the essential oils of the leaves and flowers of Rhus mysurensis Heyne ex Wight Arn growing in the Aravalli mountain range at New Delhi, Flavour Fragr. J., 2006, 21, 2, 228-229, https://doi.org/10.1002/ffj.1561 . [all data]

Tognolini, Barocelli, et al., 2006
Tognolini, M.; Barocelli, E.; Ballabeni, V.; Bruni, R.; Bianchi, A.; Chiavarini, M.; Impicciatore, M., Comparative screening of plant essential oils: Phenylpropanoid moiety as basic core for antiplatelet activity, Life Sciences, 2006, 78, 13, 1419-1432, https://doi.org/10.1016/j.lfs.2005.07.020 . [all data]

Cysne, Canuto, et al., 2005
Cysne, J.B.; Canuto, K.M.; Pessoa, O.D.L.; Nunes, E.P.; Silveira, E.R., Leaf essential oils of four Piper species from the State of Ceará - Northeast of Brazil, J. Braz. Chem. Soc., 2005, 16, 6B, 1378-1381, https://doi.org/10.1590/S0103-50532005000800012 . [all data]

Dickschat, Bode, et al., 2005
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Hamm, Bleton, et al., 2005
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Couladis, Özcan, et al., 2004
Couladis, M.; Özcan, M.; Tzakou, O.; Akgül, A., Menengic (Pistacia terebinthus L.) agacinin degisik organlarinda ucucu yag bilesimi, Bitkisel Ilac Hammaddeleri Toplantisi, Bildiriler, 29-31 Mayis 2002, 2004, 6. [all data]

El-Shazily, Hafez, et al., 2004
El-Shazily, A.M.; Hafez, S.S.; Wink, M., Comparative study of the essential oils and extracts of Achillea fragrantissima (Forssk.) Sch. Bip. and Achillea santolina L. (Asteraceae) from Egypt, Pharmazie, 2004, 59, 226-230. [all data]

Hafez and Abdel-Salam, 2004
Hafez, S.S.; Abdel-Salam, H.A., chemical composition and antimicrobial activity of the volatile constituents of thuja occidentalis L. growing in Egipt, Alexandria J. Pharm. Sci., 2004, 18, 1, 41-47. [all data]

Koba, Sanda, et al., 2004
Koba, K.; Sanda, K.; Raynaud, C.; Nenonene, Y.A.; Millet, J.; Chaumont, J.P., Activités antimicrobiennes d'huiles essentielles de trois Cymbopogon sp. africains vis-àvis de germes pathogènes d'animaux de compagnie, Ann. Med. Vet., 2004, 148, 202-206. [all data]

Miguel, Simões, et al., 2004
Miguel, G.; Simões, M.; Figueiredo, A.C.; Barroso, J.G.; Pedro, L.G.; Carvalho, L., Composition and antioxidant activities of the essential oils of Thymus caespititius, Thymus camphoratus and Thymus mastichina, Food Chem., 2004, 86, 2, 183-188, https://doi.org/10.1016/j.foodchem.2003.08.031 . [all data]

Senatore, Apostolides Arnold, et al., 2004
Senatore, F.; Apostolides Arnold, N.; Piozzi, F., Chemical composition of the essential oil of Salvia multicaulis Vahl. var. simplicifolia Boiss. growing wild in Lebanon, J. Chromatogr. A, 2004, 1052, 1-2, 237-240, https://doi.org/10.1016/j.chroma.2004.08.095 . [all data]

Tepe, Donmez, et al., 2004
Tepe, B.; Donmez, E.; Unlu, M.; Candan, F.; Daferera, D.; Vardar-Unlu, G.; Polissiou, M.; Sokmen, A., Antimicrobial and antioxidative activities of the essential oils and methanol extracts of Salvia cryptantha (Montbret et Aucher ex Benth.) and Salvia multicaulis (Vahl), Food Chem., 2004, 84, 4, 519-525, https://doi.org/10.1016/S0308-8146(03)00267-X . [all data]

Vinogradov, 2004
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Hamm, Lesellier, et al., 2003
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Notes

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