Naphthalene, 1,2,3,4,4a,5,6,8a-octahydro-4a,8-dimethyl-2-(1-methylethenyl)-, [2R-(2α,4aα,8aβ)]-

Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSDB-5 MSHP-5 MSDB-5Elite-5 MS
Column length (m) 60.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.60.60.60.40.
Tend (C) 250.270.220.240.220.
Heat rate (K/min) 3.3.4.3.4.
Initial hold (min) 1. 20.  
Final hold (min) 20. 20.  
I 1491.1497.1492.1494.1484.
ReferenceSardashti, Valizadeh, et al., 2013Cui, Yang, et al., 2011Feizbakhsh and Naeemy, 2011Karimi, Farmani, et al., 2011Baharum, Bunawan, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5HP-5 MSHP-5 MSHP-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.60.60.70.70.
Tend (C) 300.240.220.290.290.
Heat rate (K/min) 50.3.5.5.5.
Initial hold (min) 5. 10.  
Final hold (min) 5.  10.10.
I 1493.1492.1498.1503.1494.
ReferenceBi Kouame, Bedi, et al., 2010Magalhaes, Lima, et al., 2010Ogunwande, Flamini, et al., 2010Radulovic, Blagojevic, et al., 2010Radulovic, Dordevic, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SLB-5 MSSLB-5 MSDB-5DB-5SE-54
Column length (m) 10.10.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.100.100.250.250.25
Phase thickness (μm) 0.100.100.250.250.25
Tstart (C) 50.50.40.40.60.
Tend (C) 250.250.240.250.260.
Heat rate (K/min) 10.10.3.10.2.
Initial hold (min)   1.1.5.
Final hold (min)    3.999.
I 1491.1500.1501.1490.1487.
ReferenceScandinaro, Tranchida, et al., 2010Scandinaro, Tranchida, et al., 2010de Souza, Lopes, et al., 2010Yang, Zhang, et al., 2010Dayisoylu and Alma, 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5CP-Sil 5 CBDB-5HP-5 MSHP-5
Column length (m) 60.30.30.30.30.
Carrier gas NitrogenNitrogenHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.350.250.250.250.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.50.35.50.
Tend (C) 230.200.250.195.280.
Heat rate (K/min) 4.5.5.2.5.
Initial hold (min)   2.5.2.
Final hold (min) 40.  30.5.
I 1514.1506.1498.1489.1494.
ReferenceGauvin-Bialecki and Marodon, 2009Hnawia, Menut, et al., 2009Ho, Wang, et al., 2009Kim and Chung, 2009Lago, Favero, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-55 % Phenyl methyl siloxaneDB-5DB-5 MSDB-5
Column length (m) 30.60.30.30.30.
Carrier gas HeliumHeliumNitrogenHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 70.90.40.50.40.
Tend (C) 240.225.230.220.240.
Heat rate (K/min) 5.3.2.3.3.
Initial hold (min)    2.1.
Final hold (min)  3. 70. 
I 1491.1499.1498.1485.1501.
ReferenceLawal and Oyedelji, 2009Retta, Gattuso, et al., 2009Scrivanti, Anton, et al., 2009Shimizu, Imayoshi, et al., 2009de Souza, Lopes, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1HP-5 MSDB-5ZB-1DB-5 MS
Column length (m) 25.30.30.30.30.
Carrier gas  HeliumHeliumNitrogenHelium
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.170.250.250.250.25
Tstart (C) 50.50.100.45.50.
Tend (C) 260.280.300.230.300.
Heat rate (K/min) 1.4.20.3.5.
Initial hold (min) 5. 2. 5.
Final hold (min) 5. 10. 5.
I 1489.1496.1470.1478.1498.
ReferenceWetwiayaklung, Thavanapong, et al., 2009Zhao, Zeng, et al., 2009Khokra, Prakash, et al., 2008Mierendorff, Stahl-Biskup, et al., 2008Noudogbessi, Yedomonhan, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5CP Sil 5 CBHP-5 MSDB-5MSZB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumN2HeliumHe 
Substrate      
Column diameter (mm) 0.250.320.320.250.25
Phase thickness (μm) 0.320.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 250.300.280.240.220.
Heat rate (K/min) 5.4.4.3.4.
Initial hold (min) 30. 5. 5.
Final hold (min)     20.
I 1494.1494.1497.1497.1497.
ReferenceYassa and Akhani, 2008Baran, von Reuss, et al., 2007Capetanos, Saroglou, et al., 2007Da Silva J.K.R., Sousa P.J.C., et al., 2007Mohottalage, Tabacchi, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1Methyl SiliconeDB-1SPB-1HP-5 MS
Column length (m) 30.50.50.30.30.
Carrier gas  HeliumHeHeHelium
Substrate      
Column diameter (mm) 0.250.250.250.20.25
Phase thickness (μm) 0.15 0.250.20.25
Tstart (C) 60.50.95.70.60.
Tend (C) 220.240.240.220.280.
Heat rate (K/min) 3.3.4.3.3.
Initial hold (min)      
Final hold (min)    15. 
I 1488.1498.1492.1479.1498.
ReferenceOuattara, Koudou, et al., 2007Ozcan and Chalchat, 2007Pala-Paul, Brophy, et al., 2007Pinto, Salgueiro, et al., 2007Vagionas, Graikou, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5AT-5BP-1HP-5MS
Column length (m) 30.30.60.50.30.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.250.250.250.220.25
Phase thickness (μm) 0.250.320.250.250.25
Tstart (C) 40.60.60.60.60.
Tend (C) 250.250.200.220.280.
Heat rate (K/min) 3.5.4.2.3.
Initial hold (min) 5.30.   
Final hold (min) 10. 20.20. 
I 1470.1494.1494.1494.1495.
ReferenceVichi, Riu-Aumatell, et al., 2007Yassa and Akhani, 2007Borges, Rojas, et al., 2006Boti, Yao, et al., 2006Bozin, Mimicá-Dukic, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1HP-1HP-1HP-1HP-1
Column length (m) 50.50.50.50.50.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.20.20.20.20.2
Phase thickness (μm) 0.330.330.50.330.33
Tstart (C) 60.60.60.60.60.
Tend (C) 250.250.250.250.250.
Heat rate (K/min) 2.2.2.2.2.
Initial hold (min) 4.4. 4. 
Final hold (min) 30.30.120.30.60.
I 1488.1499.1488.1488.1494.
ReferenceCastel, Fernandez, et al., 2006Castel, Fernandez, et al., 2006Castel, Fernandez, et al., 2006, 2Castel, Fernandez, et al., 2006, 2Fernandez, Pintaric, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5Ultra-2HP-5
Column length (m) 30.30.30.50.25.
Carrier gas HeHeHeliumHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (μm) 0.250.250.250.320.33
Tstart (C) 60.60.60.50.30.
Tend (C) 240.240.260.270.280.
Heat rate (K/min) 5.5.3.2.3.
Initial hold (min) 2.2.   
Final hold (min)      
I 1494.1494.1491.1505.1505.
ReferenceGohari, Hadjiakhoondi, et al., 2006Gohari A.R., Hadjiakhoondi A., et al., 2006Javidnia, Miri, et al., 2006Schlumpberger B.O., Clery R.A., et al., 2006Shafi, Jose, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1SPB-1ZB-5DB-1DB-1
Column length (m) 50.30.60.30.60.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (μm) 0.330.250.250.250.25
Tstart (C) 50.50.40.60.60.
Tend (C) 220.250.250.250.250.
Heat rate (K/min) 4.4.6.5.5.
Initial hold (min) 1.1.7.5. 
Final hold (min) 10.10.1.15.10.
I 1486.1475.1521.1500.1504.
ReferenceWong, Lim, et al., 2006Wong, Sivasothy, et al., 2006Dötterl, Wolfe, et al., 2005Facundo, Pinto, et al., 2005Fakhari A.R., Sonboli A., et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSHP-5MSDB-5MSDB-1
Column length (m) 30.30.25.30.50.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 60.60.50.60.95.
Tend (C) 300.200.250.280.240.
Heat rate (K/min) 3.4.3.3.4.
Initial hold (min) 3.30.3.30. 
Final hold (min)   10.  
I 1486.1487.1493.1470.1492.
ReferenceFerraz, Limberger, et al., 2005Gauvin and Smadja, 2005Ghasemi Y., Faridi P., et al., 2005Marongiu, Piras, et al., 2005Palá-Paúl, Pérez-Alonso, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSDB-5DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.60.60.60.60.
Tend (C) 260.280.300.300.300.
Heat rate (K/min) 2.3.3.3.3.
Initial hold (min) 5.5.   
Final hold (min) 20.    
I 1494.1495.1488.1488.1488.
ReferenceSenatore, Apostolides Arnold, et al., 2005Setzer, Noletto, et al., 2005Simoes-Pires C.A., Debenedetti S., et al., 2005Simoes-Pires C.A., Debenedetti S., et al., 2005Simoes-Pires C.A., Debenedetti S., et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1CP Sil 8 CBHP-5 MSHP-5MSDB-5MS
Column length (m) 30.30.30.30.30.
Carrier gas N2HeHe He
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.25 0.500.250.25
Tstart (C) 60.60.60.40.80.
Tend (C) 220.290.260.220.250.
Heat rate (K/min) 5.3.3.3.5.
Initial hold (min)  5. 5.2.
Final hold (min) 15. 20.10.9.
I 1492.1514.1487.1470.1495.
ReferenceSrivastava, Srivastava, et al., 2005Suárez, Vásquez, et al., 2005Topçu, Barla, et al., 2005Vichi, Riu-Aumatell, et al., 2005Watanabe Y., Mihara R., et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5CP Sil 5 CBDB-1DB-5MSDB-5
Column length (m) 30.30.30.30.30.
Carrier gas H2N2N2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.50.50.60.60.
Tend (C) 290.200.200.240.300.
Heat rate (K/min) 4.5.5.3.3.
Initial hold (min)      
Final hold (min)      
I 1493.1492.1495.1494.1481.
ReferenceAbreu, Reis, et al., 2004Agnaniet, Menut, et al., 2004Fekam Boyom, Fotio, et al., 2004paz Lima, Silva, et al., 2004Limberger, Sobral, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5NB-30NB-30
Column length (m) 30.30.50.50.50.
Carrier gas  HeliumHeliumHeHe
Substrate      
Column diameter (mm) 0.250.250.250.20.2
Phase thickness (μm) 0.15  0.250.25
Tstart (C) 60.60.60.50.50.
Tend (C) 220.240.240.250.250.
Heat rate (K/min) 3.2.2.2.2.
Initial hold (min) 3.    
Final hold (min)  999.999.  
I 1490.1488.1488.1493.1492.
ReferenceMevy, Bessiere, et al., 2004Miyazawa, Fuhita, et al., 2004Miyazawa, Fujita, et al., 2004Orav, Stulova, et al., 2004Orav, Stulova, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5HP-5HP-5MSDB-1
Column length (m) 50.25.30.30.30.
Carrier gas N2H2N2HeN2
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.520.250.250.25
Tstart (C) 95.40.60.60.50.
Tend (C) 240.240.220.280.200.
Heat rate (K/min) 4.4.5.3.5.
Initial hold (min)   10.  
Final hold (min)      
I 1469.1498.1484.1492.1501.
ReferencePalá-Paúl, Velasco-Negueruela, et al., 2004Simic, Sokovic, et al., 2004Bertoli, Menichini, et al., 2003Couladis, Özcan, et al., 2003Fekam Boyom, Ngouana, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RSL-200RSL-200DB-5DB-1DB-5MS
Column length (m) 30.30.30.30.30.
Carrier gas H2H2HeN2He
Substrate      
Column diameter (mm) 0.320.320.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.40.60.80.60.
Tend (C) 280.280.250.250.240.
Heat rate (K/min) 6.6.3.4.3.
Initial hold (min) 5.5.   
Final hold (min) 5.5.   
I 1492.1491.1490.1473.1493.
ReferenceJirovetz, Buchbauer, et al., 2003Jirovetz, Buchbauer, et al., 2003, 2Limberger, Simões-Pires, et al., 2003Mahalwal and Ali, 2003Maia, Taveira, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-1HP-5DB-1
Column length (m) 30.30.60.30.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.50.60.40.
Tend (C) 280.280.270.280.260.
Heat rate (K/min) 3.3.4.3.4.
Initial hold (min)     5.
Final hold (min) 30.30.   
I 1487.1485.1475.1476.1473.
ReferenceMarongiu, Porcedda, et al., 2003Marongiu, Porcedda, et al., 2003Mirza and Nik, 2003Pitarokili, Tzakou, et al., 2003Sefidkon, Naderi Nik, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5DB-5MSHP-5DB-5
Column length (m) 60.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.320.25
Tstart (C) 50.60.60.60.60.
Tend (C) 280.240.240.250.240.
Heat rate (K/min) 4.3.3.5.3.
Initial hold (min)    30. 
Final hold (min)      
I 1489.1494.1492.1494.1496.
ReferenceShahmir, Ahmadi, et al., 2003da Silva, Luz, et al., 2003Taveira, de Lima, et al., 2003Yassa, Akhani, et al., 2003Zoghbi, Andrade, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-5DB-1MDN-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeN2H2 He
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.40.40.60.
Tend (C) 280.250.245.280.240.
Heat rate (K/min) 3.4.3.8.3.
Initial hold (min)   20.3. 
Final hold (min)      
I 1496.1494.1468.1489.1494.
ReferenceCongiu, Falconieri, et al., 2002Farah, Fechtal, et al., 2002Gancel, Ollé, et al., 2002Jelén, 2002Kobaisy, Tellez, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5DB-5OV-101DB-5DB-5MS
Column length (m) 30.30.25.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 60.35.50.60.60.
Tend (C) 150.280.200.240.240.
Heat rate (K/min) 1.3.5.3.3.
Initial hold (min) 3.2.   
Final hold (min)  15.   
I 1483.1505.1481.1493.1496.
ReferenceKovacevic and Kac, 2002Krauze-Baranowska, Mardarowicz, et al., 2002Kuiate, Bessière, et al., 2002Maia, da Silva, et al., 2002Maia, Zoghbi, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5MSDB-5BP-1
Column length (m) 30.25.30.30.30.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (μm) 0.25 0.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 300.220.270.240.220.
Heat rate (K/min) 2.3.3.3.5.
Initial hold (min)      
Final hold (min)      
I 1484.1499.1493.1495.1486.
ReferenceRuberto, Biondi, et al., 2002Schwob, Bessière, et al., 2002Zoghbi, Andrade, et al., 2002Zoghbi, Andrade, et al., 2002, 2Gupta, Mallavarapu, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RSL-200HP-1RTX-5DB-5MSDB-5
Column length (m) 30.25.30.30.30.
Carrier gas H2N2HeHeHe
Substrate      
Column diameter (mm) 0.320.20.250.250.25
Phase thickness (μm) 0.250.110.250.250.25
Tstart (C) 40.60.60.60.60.
Tend (C) 280.190.150.240.270.
Heat rate (K/min) 6.2.51.3.3.
Initial hold (min) 5.3.3.  
Final hold (min) 5.1. 30. 
I 1509.1476.1483.1481.1496.
ReferenceJirovetz L., Buchbauer G., et al., 2001Kovacevic and Kac, 2001Kovacevic and Kac, 2001Marongiu, Porcedda, et al., 2001Palmeira, Conserva, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5CP Sil 5 CBCP Sil 5 CBDB-1
Column length (m) 30.30.25.25.33.
Carrier gas N2H2 HeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.150.40.50
Tstart (C) 80.60.50.60.50.
Tend (C) 225.285.230.260.135.
Heat rate (K/min) 4.3.3.5.20.
Initial hold (min)    40.2.
Final hold (min)      
I 1464.1491.1479.1491.1506.
ReferencePalá-Paúl, Pérez-Alonso, et al., 2001Santos-Gomes and Fernandes-Ferreira, 2001Asekun and Ekundayo, 2000Baser, Özek, et al., 2000Feger, Brandauer, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1OV-101DB-5DB-5MS
Column length (m) 30.25.50.30.30.
Carrier gas HeNitrogenNitrogenHeHe
Substrate      
Column diameter (mm) 0.250.500.250.250.25
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 60.60.40.60.60.
Tend (C) 240.220.200.240.240.
Heat rate (K/min) 3.5.2.3.3.
Initial hold (min)   10.  
Final hold (min)      
I 1492.1495.1490.1494.1485.
ReferenceMaia, Zoghbi, et al., 2000Mallavarapu, Rao, et al., 2000Tamura, Boonbumrung, et al., 2000Tellez, Dayan, et al., 2000Zoghbi, Andrade, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-1OV-101DB-5DB-5
Column length (m) 30.60.25.30.30.
Carrier gas HeliumHe HeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.25 0.25 
Tstart (C) 60.50.50.65.60.
Tend (C) 240.280.200.300.240.
Heat rate (K/min) 3.4.5.4.4.
Initial hold (min)  5. 2. 
Final hold (min)      
I 1496.1512.1492.1481.1497.
ReferenceSantos, Andrade, et al., 1998Stashenko, Cervantes, et al., 1998Zollo, Biyiti, et al., 1998Elias, Simoneit, et al., 1997Zunino, Novillo-Newton, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5SPB-1HP-5Methyl SiliconeMethyl Silicone
Column length (m) 30.50. 50.50.
Carrier gas  He N2N2
Substrate      
Column diameter (mm) 0.250.2 0.250.25
Phase thickness (μm) 0.250.33 0.170.17
Tstart (C) 60.40.35.80.80.
Tend (C) 300.200.200.200.200.
Heat rate (K/min) 4.3.6.2.3.
Initial hold (min) 2.3.2.  
Final hold (min) 5.30.   
I 1491.61495.1534.1484.1483.
ReferenceGawdzik, Mardarowicz, et al., 1996Wong and Lai, 1996Larsen and Frisvad, 1995Gopalakrishnan, Menon, et al., 1993Gopalakrishnan, Menon, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-54CP Sil 8 CBDB-1DB-1SE-30
Column length (m) 30.25.60.60.30.
Carrier gas Hydrogen HeHe 
Substrate      
Column diameter (mm) 0.250.200.320.32 
Phase thickness (μm) 0.25    
Tstart (C) 60.60.30.30.50.
Tend (C) 250.230.210.210.240.
Heat rate (K/min) 2.3.2.2.4.
Initial hold (min) 5.10.4.4.2.
Final hold (min) 2.   10.
I 1487.1529.1482.1489.1484.
ReferenceKollmannsberger, Nitz, et al., 1992Jantan and Goh, 1990Takeoka and Butter, 1989Takeoka and Butter, 1989Ramaswami, Briscese, et al., 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase SE-30
Column length (m) 30.
Carrier gas  
Substrate  
Column diameter (mm)  
Phase thickness (μm)  
Tstart (C) 50.
Tend (C) 240.
Heat rate (K/min) 4.
Initial hold (min) 2.
Final hold (min) 10.
I 1484.
ReferenceRamaswami, Briscese, et al., 1986
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Zhao, Zeng, et al., 2009
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Mohottalage, Tabacchi, et al., 2007
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Ouattara, Koudou, et al., 2007
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Ozcan and Chalchat, 2007
Ozcan, M.M.; Chalchat, J.C., Chemical Composition od Carrot Seeds (Daucus carota L.) Cultivated in Turkey: Characterization of the Seed Oil and Essential Oil, Grasas y Aceites, 2007, 58, 4, 359-365. [all data]

Pala-Paul, Brophy, et al., 2007
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Pinto, Salgueiro, et al., 2007
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Vagionas, Graikou, et al., 2007
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Yassa and Akhani, 2007
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Borges, Rojas, et al., 2006
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Castel, Fernandez, et al., 2006, 2
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Fernandez, Pintaric, et al., 2006
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Gohari, Hadjiakhoondi, et al., 2006
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Gohari A.R., Hadjiakhoondi A., et al., 2006
Gohari A.R.; Hadjiakhoondi A.; Sadat-Ebrahimi E.; Saeidnia S.; Shafiee A., Composition of the volatile oils of Satureja spicigera C. Koch Boiss. and S-macrantha C. A. Mey from Iran, Flavour Fragr. J., 2006, 21, 3, 510-512, https://doi.org/10.1002/ffj.1613 . [all data]

Javidnia, Miri, et al., 2006
Javidnia, K.; Miri, R.; Kamalinejad, M.; Mehdipour, A.R., Composition of the essential oil of Diplotaenia cachrydifolia Boiss. from Iran, J. Ess. Oil Res., 2006, 18, 1, 86-87, https://doi.org/10.1080/10412905.2006.9699393 . [all data]

Schlumpberger B.O., Clery R.A., et al., 2006
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Shafi, Jose, et al., 2006
Shafi, P.M.; Jose, B.; Radhamani, K.T.; Clery, R.A., Influence of pH on essential oil composition of Zanthoxylum rhetsa seeds obtained by steam distillation, Flavour Fragr. J., 2006, 21, 2, 317-318, https://doi.org/10.1002/ffj.1598 . [all data]

Wong, Lim, et al., 2006
Wong, K.C.; Lim, T.B.; Ali, D.M.H., Essential oil of Homalomena sagittifolia Jungh., Flavour Fragr. J., 2006, 21, 5, 786-788, https://doi.org/10.1002/ffj.1714 . [all data]

Wong, Sivasothy, et al., 2006
Wong, K.C.; Sivasothy, Y.; Boey, P.L., Essential oil of Elettariopsis elan C.K. Lim, Flavour Fragr. J., 2006, 21, 3, 562-564, https://doi.org/10.1002/ffj.1654 . [all data]

Dötterl, Wolfe, et al., 2005
Dötterl, S.; Wolfe, L.M.; Jürgens, A., Qualitative and quantitative analyses of flower scent in Silene latifolia, Phytochemistry, 2005, 66, 2, 203-213, https://doi.org/10.1016/j.phytochem.2004.12.002 . [all data]

Facundo, Pinto, et al., 2005
Facundo, V.A.; Pinto, A.C.; Rezende, C.M., Aroma compounds and volatile chemical composition of Ruellia menthoides (Nees) Hiern, Flavour Fragr. J., 2005, 20, 1, 93-95, https://doi.org/10.1002/ffj.1380 . [all data]

Fakhari A.R., Sonboli A., et al., 2005
Fakhari A.R.; Sonboli A.; Heydari R., Composition of the essential oil of Rhabdosciadium strausii from Iran, Chem. Nat. Compd. (Engl. Transl.), 2005, 41, 4, 413-414, https://doi.org/10.1007/s10600-005-0164-1 . [all data]

Ferraz, Limberger, et al., 2005
Ferraz, A.B.F.; Limberger, R.P.; Bordignon, S.A.L.; von Poser, G.L.; Henriques, A.T., Essential oil composition of six Hypericum species from southern Brazil, Flavour Fragr. J., 2005, 20, 3, 335-339, https://doi.org/10.1002/ffj.1435 . [all data]

Gauvin and Smadja, 2005
Gauvin, A.; Smadja, J., Essential oil composition of four Psiadia species from Reunion Island: A chemotaxonomic study, Biochem. Syst. Ecol., 2005, 33, 7, 705-714, https://doi.org/10.1016/j.bse.2004.12.013 . [all data]

Ghasemi Y., Faridi P., et al., 2005
Ghasemi Y.; Faridi P.; Mehregan I.; Mohagheghzadeh A., Ferula gummosa fruits: An aromatic antimicrobial agent, Chem. Nat. Compd. (Engl. Transl.), 2005, 41, 3, 311-314, https://doi.org/10.1007/s10600-005-0138-3 . [all data]

Marongiu, Piras, et al., 2005
Marongiu, B.; Piras, A.; Porcedda, S.; Scorciapino, A., Chemical composition of the essential oil and supercritical CO2 extract of Commiphora myrrha (Nees) Engl. and of Acorus calamus L., J. Agric. Food Chem., 2005, 53, 20, 7939-7943, https://doi.org/10.1021/jf051100x . [all data]

Palá-Paúl, Pérez-Alonso, et al., 2005
Palá-Paúl, J.; Pérez-Alonso, M.; Velasco-Negueruela, A.; Vadaré, J.; Villa, A.M.; Sanz, J.; Brophy, J.J., Analysis of the essential oil composition from the different parts of Eryngium glaciale Boiss. from Spain, J. Chromatogr. A, 2005, 1094, 1-2, 179-182, https://doi.org/10.1016/j.chroma.2005.09.029 . [all data]

Senatore, Apostolides Arnold, et al., 2005
Senatore, F.; Apostolides Arnold, N.; Bruno, M., Volatile components of Centaurea eryngioides Lam. and Centaurea liberica Trev. var. hermonis Boiss. Lam., two Asteraceae growing wild in Lebanon, Nat. Prod. Res., 2005, 19, 8, 749-754, https://doi.org/10.1080/14786410412331302136 . [all data]

Setzer, Noletto, et al., 2005
Setzer, W.N.; Noletto, J.A.; Lawton, R.O.; Haber, W.A., Leaf essential oil composition of five Zanthoxylum species from Monteverde, Costa Rica, Molecular Diversity, 2005, 9, 1-3, 3-13, https://doi.org/10.1007/s11030-005-1298-6 . [all data]

Simoes-Pires C.A., Debenedetti S., et al., 2005
Simoes-Pires C.A.; Debenedetti S.; Spegazzini E.; Mentz L.A.; Matzenbacher N.I.; Limberger R.P.; Henriques A.T., Investigation of the essential oil from eight species of Baccharis belonging to sect. Caulopterae (Asteraceae, Astereae): a taxonomic approach, Plant Systematics and Evolution, 2005, 253, 1-4, 23-32, https://doi.org/10.1007/s00606-005-0296-6 . [all data]

Srivastava, Srivastava, et al., 2005
Srivastava, A.K.; Srivastava, S.K.; Syamsundar, K.V., Bud and leaf essential oil composition of Syzygium aromaticum from India and Madagascar, Flavour Fragr. J., 2005, 20, 1, 51-53, https://doi.org/10.1002/ffj.1364 . [all data]

Suárez, Vásquez, et al., 2005
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Ramaswami, S.K.; Briscese, P.; Gargiullo, R.J.; von Geldern, T., Sesquiterpene hydrocarbons: from mass confusion to orderly line-up in Flavors and Fragrances: A World Perspective, Lawrence,B.M.; Mookherjee,B.D.; Willis,B.J., ed(s)., Proceedings of the 10th International Congress of Essential Oils, Fragrances, and Flavors, Washington, DC, 1986, 951-959. [all data]

Notes

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