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Bicyclo[2.2.1]heptane, 7,7-dimethyl-2-methylene-

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Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillarySE-30100.957.Saeed, Redant, et al., 197980. m/0.5 mm/0.8 «mu»m
CapillarySE-30110.956.8Saeed, Redant, et al., 197980. m/0.5 mm/0.8 «mu»m
CapillarySE-30130.965.2Saeed, Redant, et al., 197980. m/0.5 mm/0.8 «mu»m

Kovats' RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-5953.Adams, González Elizondo, et al., 200630. m/0.26 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillaryDB-5953.Adams, Morris, et al., 200530. m/0.26 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillaryDB-5953.Adams and Nguyen, 200530. m/0.26 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillaryCP Sil 5 CB941.Ogunwande, Olawore, et al., 200325. m/0.25 mm/0.15 «mu»m, H2, 3. K/min; Tstart: 50. C; Tend: 230. C
CapillaryDB-5958.Buchin, Salmon, et al., 200260. m/0.32 mm/1. «mu»m, He, 40. C @ 5. min, 3. K/min, 230. C @ 2. min
CapillaryHP-5951.Mita, Tsitsimpikou, et al., 200230. m/0.25 mm/0.25 «mu»m, He, 3. K/min, 240. C @ 20. min; Tstart: 60. C
CapillaryHP-5MS950.Salido, Altarejos, et al., 200230. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 50. C; Tend: 250. C
CapillaryDB-1941.Palá-Paúl, Velasco-Negueruela, et al., 200150. m/0.25 mm/0.25 «mu»m, N2, 4. K/min; Tstart: 80. C; Tend: 225. C
CapillarySE-54953.Adams, 200030. m/0.26 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillaryDB-5953.Adams, 2000, 230. m/0.26 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillarySE-54953.Adams, 2000, 330. m/0.26 mm/0.25 «mu»m, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillaryDB-5953.Adams, 2000, 430. m/0.26 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillarySE-30942.Kardali, Velasco-Negueruela, et al., 200025. m/0.22 mm/0.25 «mu»m, He, 5. K/min; Tstart: 70. C; Tend: 220. C
CapillaryDB-5953.Adams, 199930. m/0.26 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillaryCP Sil 5 CB951.Kaul and Vats, 19985. K/min; Column length: 25. m; Column diameter: 0.25 mm; Tstart: 60. C; Tend: 280. C
CapillaryBP-1949.Breheret, Talou, et al., 199750. m/0.22 mm/1. «mu»m, He, 3. K/min; Tstart: 50. C; Tend: 220. C

Kovats' RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-5953.Adams, 199830. m/0.26 mm/0.25 «mu»m; Program: not specified

Kovats' RI, polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillaryCarbowax 20M100.1089.7Saeed, Redant, et al., 1979Phase thickness: 0.5 «mu»m
CapillaryCarbowax 20M70.1070.7Saeed, Redant, et al., 1979Phase thickness: 0.5 «mu»m
CapillaryCarbowax 20M90.1081.9Saeed, Redant, et al., 1979Phase thickness: 0.5 «mu»m

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryZB-5951.Simoniatto, Bonani, et al., 200730. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 50. C; Tend: 250. C
CapillarySPB-1959.Blagojevic, Radulovic, et al., 200630. m/0.25 mm/0.25 «mu»m, He, 50. C @ 3. min, 5. K/min, 250. C @ 15. min
CapillaryDB-5950.Blagojevic, Radulovic, et al., 200630. m/0.2 mm/0.25 «mu»m, He, 50. C @ 3. min, 5. K/min, 250. C @ 15. min
CapillaryBP-1940.Boti, Bighelli, et al., 200650. m/0.22 mm/0.25 «mu»m, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryRTX-1942.Cavalli, Tomi, et al., 200660. m/0.22 mm/0.25 «mu»m, He, 2. K/min, 230. C @ 45. min; Tstart: 60. C
CapillaryDB-5952.Dob, Dahmane, et al., 200630. m/0.25 mm/0.25 «mu»m, N2, 60. C @ 3. min, 3. K/min, 240. C @ 3. min
CapillaryBP-1944.Gonny, Cavaleiro, et al., 200650. m/0.22 mm/0.25 «mu»m, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryDB-1951.Kuiate, Bessière, et al., 200630. m/0.25 mm/0.25 «mu»m, N2, 4. K/min; Tstart: 50. C; Tend: 220. C
CapillaryRTX-1940.Paolini J., Desjobert J.M., et al., 200660. m/0.22 mm/0.25 «mu»m, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C
CapillaryHP-5MS948.Saroglou, Dorizas, et al., 200630. m/0.25 mm/0.25 «mu»m, He, 60. C @ 5. min, 4. K/min; Tend: 280. C
CapillaryBP-1942.Boti J.B., Koukoua G., et al., 200550. m/0.22 mm/0.25 «mu»m, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryHP-5MS951.Pino, Mesa, et al., 200530. m/0.25 mm/0.25 «mu»m, He, 60. C @ 2. min, 4. K/min, 250. C @ 20. min
CapillaryRTX-5943.Dugo, Mondello, et al., 200430. m/0.25 mm/0.25 «mu»m, He, 45. C @ 6. min, 3. K/min, 300. C @ 10. min
CapillaryDB-5953.Flamini, Cioni, et al., 200430. m/0.25 mm/0.25 «mu»m, N2, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryBP-1944.Bianchini, Tomi, et al., 200350. m/0.22 mm/0.25 «mu»m, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C
CapillaryBP-1944.Bianchini, Tomi, et al., 200350. m/0.22 mm/0.25 «mu»m, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C
CapillaryRTX-1943.Cavalli, Tomi, et al., 200360. m/0.22 mm/0.25 «mu»m, He, 2. K/min, 230. C @ 45. min; Tstart: 60. C
CapillaryDB-5948.Jantan, Ling, et al., 200330. m/0.25 mm/0.25 «mu»m, He, 75. C @ 10. min, 3. K/min, 230. C @ 20. min
CapillaryHP-5951.Karioti, Skaltsa, et al., 200330. m/0.25 mm/0.25 «mu»m, He, 60. C @ 5. min, 4. K/min; Tend: 280. C
CapillaryDB-5933.Choi, Kim. M.-S.L., et al., 200230. m/0.25 mm/0.25 «mu»m, He, 70. C @ 2. min, 4. K/min, 230. C @ 20. min
CapillaryDB-5953.Flamini, Cioni, et al., 200230. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryHP-5950.Fokialakis, Magiatis, et al., 200230. m/0.25 mm/0.25 «mu»m, 60. C @ 5. min, 3. K/min; Tend: 280. C
CapillaryCP Sil 5 CB933.Pino, Marbot, et al., 200225. m/0.25 mm/0.25 «mu»m, N2, 60. C @ 6. min, 4. K/min; Tend: 280. C
CapillaryCP Sil 5 CB937.Pino, Marbot, et al., 2002, 230. m/0.25 mm/0.25 «mu»m, H2, 60. C @ 10. min, 2. K/min, 280. C @ 40. min
CapillaryCP Sil 5 CB937.Pino, Marbot, et al., 2002, 350. m/0.32 mm/0.4 «mu»m, He, 60. C @ 10. min, 3. K/min, 280. C @ 60. min
CapillaryDB-1942.Pintore, Usai, et al., 200250. m/0.22 mm/0.25 «mu»m, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryBP-1944.Bianchini, Tomi, et al., 200150. m/0.22 mm/0.25 «mu»m, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C
CapillaryDB-1946.Kim, 200160. m/0.32 mm/1. «mu»m, He, 40. C @ 5. min, 2. K/min; Tend: 220. C
CapillaryCP Sil 5 CB937.Pino, Marbot, et al., 200150. m/0.32 mm/0.4 «mu»m, He, 60. C @ 10. min, 3. K/min, 280. C @ 60. min
CapillaryCP Sil 5 CB945.Pfeifhofer, 200050. m/0.22 mm/0.13 «mu»m, H2, 4. K/min, 300. C @ 10. min; Tstart: 40. C
CapillaryDB-1953.9Helmig, Klinger, et al., 199960. m/0.32 mm/1. «mu»m, -50. C @ 2. min, 6. K/min; Tend: 175. C
CapillaryOV-1942.Bicchi, Rubiolo, et al., 199825. m/0.25 mm/0.3 «mu»m, 50. C @ 1. min, 3. K/min, 200. C @ 20. min

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-5MS949.3Andriamaharavo, 201430. m/0.25 mm/0.25 «mu»m, He; Program: 60C (1 min) => 5 C/min => 210C => 10 C/min => 280C (15 min)
CapillaryBPX-5949.Cardeal, da Silva, et al., 200630. m/0.25 mm/0.25 «mu»m; Program: 35C(5min) => 3C/min => 210C => 40C/min => 240C (4min)
CapillaryBP-1942.Cavalli, Ranarivelo, et al., 200150. m/0.22 mm/0.25 «mu»m; Program: not specified
CapillaryBPX-5965.Elmore, Erbahadir, et al., 199750. m/0.32 mm/0.5 «mu»m, He; Program: 0C (5min) => 40C/min => 40C (2min) => 10C/min => 280C
CapillarySE-52949.Mondello, Dugo, et al., 199560. m/0.32 mm/0.40 «mu»m, He; Program: 45 C (6 min) 3 C/min -> 111 0C 2 C/min -> 160 C 3 C/min -> 300 C (15 min)

Van Den Dool and Kratz RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryBP-201052.Boti, Bighelli, et al., 200650. m/0.22 mm/0.25 «mu»m, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryRTX-Wax1056.Cavalli, Tomi, et al., 200660. m/0.22 mm/0.25 «mu»m, He, 2. K/min, 230. C @ 45. min; Tstart: 60. C
CapillaryPolyethylene Glycol1068.Dob, Dahmane, et al., 200630. m/0.32 mm/0.25 «mu»m, N2, 50. C @ 10. min, 2. K/min, 230. C @ 15. min
CapillaryBP-201060.Gonny, Cavaleiro, et al., 200650. m/0.22 mm/0.25 «mu»m, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryRTX-Wax1046.Paolini J., Desjobert J.M., et al., 200660. m/0.22 mm/0.25 «mu»m, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C
CapillaryBP-201052.Boti J.B., Koukoua G., et al., 200550. m/0.22 mm/0.25 «mu»m, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryDB-Wax1060.Brophy, Goldsack, et al., 200460. m/0.32 mm/0.25 «mu»m, He, 3. K/min; Tstart: 32. C; Tend: 220. C
CapillaryRTX-Wax1048.Dugo, Mondello, et al., 200430. m/0.25 mm/0.25 «mu»m, He, 45. C @ 6. min, 3. K/min, 240. C @ 10. min
CapillaryBP-201059.Bianchini, Tomi, et al., 200350. m/0.22 mm/0.25 «mu»m, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C
CapillaryBP-201059.Bianchini, Tomi, et al., 200350. m/0.22 mm/0.25 «mu»m, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C
CapillaryRTX-Wax1054.Cavalli, Tomi, et al., 200360. m/0.22 mm/0.25 «mu»m, He, 2. K/min, 230. C @ 45. min; Tstart: 60. C
CapillaryDB-Wax1077.Choi, Kim. M.-S.L., et al., 200260. m/0.25 mm/0.25 «mu»m, N2, 2. K/min, 230. C @ 20. min; Tstart: 70. C
CapillaryAT-Wax1045.Pino, Marbot, et al., 2002, 360. m/0.32 mm/0.25 «mu»m, He, 65. C @ 10. min, 2. K/min, 250. C @ 60. min
CapillaryBP-201056.Pintore, Usai, et al., 200250. m/0.22 mm/0.25 «mu»m, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryBP-201059.Bianchini, Tomi, et al., 200150. m/0.22 mm/0.25 «mu»m, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C
CapillaryAT-Wax1045.Pino, Marbot, et al., 200160. m/0.32 mm/0.25 «mu»m, He, 65. C @ 10. min, 2. K/min, 250. C @ 60. min
CapillaryDB-Wax1060.Brophy, Goldsack, et al., 200060. m/0.50 mm/1.0 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 225. C
CapillaryDB-Wax1060.Brophy, Goldsack, et al., 2000, 260. m/0.53 mm/1.0 «mu»m, He, 3. K/min; Tstart: 50. C; Tend: 220. C
CapillaryDB-Wax1060.Brophy, Goldsack, et al., 2000, 360. m/0.53 mm/1.0 «mu»m, He, 3. K/min; Tstart: 50. C; Tend: 220. C
CapillaryDB-Wax1076.Choi and Sawamura, 200060. m/0.25 mm/0.25 «mu»m, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillaryDB-Wax1060.Brophy, Goldsack, et al., 1999He, 3. K/min; Column length: 60. m; Column diameter: 0.53 mm; Tstart: 50. C; Tend: 220. C
CapillaryDB-Wax1050.Brophy, Forster, et al., 1998He, 3. K/min; Column length: 60. m; Column diameter: 0.32 mm; Tstart: 35. C; Tend: 220. C
CapillarySP-10001060.Brophy, Forster, et al., 1998, 2He, 3. K/min; Column length: 85. m; Column diameter: 0.5 mm; Tstart: 60. C; Tend: 225. C
CapillaryDB-Wax1060.Brophy, Goldsack, et al., 1998He, 3. K/min; Column length: 60. m; Column diameter: 0.32 mm; Tstart: 65. C; Tend: 225. C
CapillaryDB-Wax1060.Brophy, Goldsack, et al., 1998, 2He, 3. K/min; Column length: 60. m; Column diameter: 0.32 mm; Tstart: 35. C; Tend: 220. C
CapillaryDB-Wax1060.Brophy, Goldsack, et al., 1997He, 3. K/min; Column length: 60. m; Column diameter: 0.32 mm; Tstart: 65. C; Tend: 225. C
CapillarySP-10001060.Brophy, Goldsack, et al., 1997, 2He, 3. K/min; Column length: 85. m; Column diameter: 0.5 mm; Tstart: 65. C; Tend: 225. C
CapillarySupelcowax-101064.Granicher, Christen, et al., 199560. m/0.25 mm/0.25 «mu»m, He, 60. C @ 5. min, 5. K/min, 230. C @ 20. min
CapillaryCarbowax 20M1054.Mondello, Dugo, et al., 199560. m/0.32 mm/0.425 «mu»m, He, 45. C @ 3. min, 3. K/min, 300. C @ 20. min

Van Den Dool and Kratz RI, polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryRTX-Wax1058.Cavalli, Ranarivelo, et al., 200160. m/0.25 mm/0.25 «mu»m; Program: not specified
CapillaryCarbowax 20M1052.Whitfield, Shea, et al., 1981Column length: 150. m; Column diameter: 0.75 mm; Program: not specified

Normal alkane RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillaryDB-525.951.Hemmateenejad, Jawadnia, et al., 2007 

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillarySPB-1943.Neves, Rosa, et al., 201030. m/0.20 mm/0.20 «mu»m, Helium, 3. K/min, 220. C @ 15. min; Tstart: 70. C
CapillarySLB-5 MS947.Scandinaro, Tranchida, et al., 201010. m/0.10 mm/0.10 «mu»m, Helium, 10. K/min; Tstart: 50. C; Tend: 250. C
CapillaryDB-5951.El-Massry, El-Ghorab, et al., 200930. m/0.25 mm/0.25 «mu»m, Helium, 3. K/min, 220. C @ 40. min; Tstart: 35. C
CapillarySPB-5938.Gilani, Shah, et al., 200930. m/0.53 mm/0.50 «mu»m, Nitrogen, 50. C @ 5. min, 3. K/min, 210. C @ 45. min
Capillary5 % Phenyl methyl siloxane951.Retta, Gattuso, et al., 200960. m/0.25 mm/0.25 «mu»m, Helium, 3. K/min, 225. C @ 3. min; Tstart: 90. C
CapillaryDB-5953.Scrivanti, Anton, et al., 200930. m/0.25 mm/0.25 «mu»m, Nitrogen, 2. K/min; Tstart: 40. C; Tend: 230. C
CapillaryHP-5 MS953.Adams, Beauchamp, et al., 200730. m/0.25 mm/0.25 «mu»m, Helium, 50. C @ 10. min, 3. K/min, 230. C @ 10. min
CapillaryHP-5953.Cheraif, Ben Jannet, et al., 200730. m/0.25 mm/0.25 «mu»m, N2, 50. C @ 1. min, 5. K/min, 240. C @ 4. min
CapillaryDB-5925.Moreno, Lima, et al., 200730. m/0.25 mm/0.25 «mu»m, Helium, 3. K/min; Tstart: 60. C; Tend: 300. C
CapillarySPB-5944.Raal, Orav, et al., 200730. m/0.25 mm/0.25 «mu»m, He, 2. K/min; Tstart: 50. C; Tend: 250. C
CapillaryHP-5MS939.Vichi, Riu-Aumatell, et al., 200730. m/0.25 mm/0.25 «mu»m, He, 40. C @ 5. min, 3. K/min, 250. C @ 10. min
CapillaryHP-5MS940.9Zizovic, Stamenic, et al., 200730. m/0.25 mm/0.25 «mu»m, He, 4. K/min; Tstart: 40. C; Tend: 260. C
CapillaryHP-5944.Abdelwahed, Hayder, et al., 200630. m/0.25 mm/0.25 «mu»m, N2, 50. C @ 3. min, 9. K/min, 280. C @ 3. min
CapillaryHP-5949.Abdelwahed, Hayder, et al., 200630. m/0.25 mm/0.25 «mu»m, N2, 50. C @ 3. min, 9. K/min, 280. C @ 3. min
CapillaryAT-5946.Borges, Rojas, et al., 200660. m/0.25 mm/0.25 «mu»m, He, 4. K/min, 200. C @ 20. min; Tstart: 60. C
CapillarySPB-1943.Cavaleiro, Pinto, et al., 200630. m/0.20 mm/0.20 «mu»m, Helium, 3. K/min, 220. C @ 15. min; Tstart: 70. C
CapillaryHP-5 MS950.Marzouk, Mansour, et al., 200630. m/0.25 mm/0.25 «mu»m, Nitrogen, 5. K/min, 280. C @ 5. min; Tstart: 50. C
CapillaryHP-5950.Marzouk, Neffati, et al., 200630. m/0.25 mm/0.52 «mu»m, N2, 5. K/min, 280. C @ 5. min; Tstart: 50. C
CapillaryHP-5951.Shafi, Jose, et al., 200625. m/0.2 mm/0.33 «mu»m, N2, 3. K/min; Tstart: 30. C; Tend: 280. C
CapillaryCP Sil 5 CB947.Ogunwande, Olawore, et al., 200525. m/0.25 mm/0.15 «mu»m, 3. K/min; Tstart: 50. C; Tend: 230. C
CapillaryHP-5MS953.Petrakis, Roussis, et al., 20053. K/min; Column length: 30. m; Column diameter: 0.2 mm; Tstart: 60. C; Tend: 280. C
CapillaryDB-1950.Palá-Paúl, García-Jiménez, et al., 200450. m/0.22 mm/0.25 «mu»m, He, 4. K/min; Tstart: 70. C; Tend: 220. C
CapillaryDB-5HT951.Yusufoglu, Celik, et al., 2004He, 50. C @ 2. min, 2. K/min, 250. C @ 20. min; Column length: 27. m; Column diameter: 0.25 mm
CapillaryHP-5MS948.Hajhashemi, Ghannadi, et al., 200330. m/0.25 mm/0.25 «mu»m, He, 4. K/min; Tstart: 60. C; Tend: 275. C
CapillaryRSL-200943.Jirovetz, Buchbauer, et al., 200330. m/0.32 mm/0.25 «mu»m, H2, 40. C @ 5. min, 6. K/min, 280. C @ 5. min
CapillaryDB-5947.Masotti, Juteau, et al., 200350. m/0.2 mm/0.25 «mu»m, He, 50. C @ 2. min, 3. K/min; Tend: 220. C
CapillaryHP-5924.Pitarokili, Tzakou, et al., 200330. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryHP-5951.Stashenko, Jaramillo, et al., 200360. m/0.25 mm/0.25 «mu»m, 40. C @ 15. min, 5. K/min; Tend: 250. C
CapillaryHP-1941.Cavaleiro, Salgueiro, et al., 200230. m/0.25 mm/0.25 «mu»m, He, 3. K/min, 220. C @ 15. min; Tstart: 70. C
Capillary5 % Phenyl methyl siloxane953.Cicció and Gómez-Laurito, 200230. m/0.25 mm/0.25 «mu»m, He, 75. C @ 4. min, 3. K/min, 200. C @ 8. min
CapillaryDB-5950.Ruberto, Biondi, et al., 200230. m/0.25 mm/0.25 «mu»m, He, 2. K/min; Tstart: 60. C; Tend: 300. C
CapillaryDB-1937.Velasco-Negueruela, Pérez-Alonso, et al., 200250. m/0.25 mm/0.25 «mu»m, N2, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillarySPB-1952.Fraternale, Giamperi, et al., 200030. m/0.2 mm/0.2 «mu»m, He, 80. C @ 3. min, 5. K/min; Tend: 300. C
CapillaryBP-1950.Mohagheghzadeh, Shams-Ardakani, et al., 200025. m/0.33 mm/1.0 «mu»m, N2, 4. K/min; Tstart: 60. C; Tend: 275. C
CapillaryDB-5961.Meynier, Novelli, et al., 199930. m/0.32 mm/1. «mu»m, 40. C @ 5. min, 3. K/min; Tend: 200. C
CapillarySPB-5949.Doneanu and Anitescu, 199850. m/0.32 mm/0.25 «mu»m, He, 3. K/min, 240. C @ 20. min; Tstart: 60. C
CapillaryCP Sil 5 CB930.Bos, Woerdenbag, et al., 199725. m/0.25 mm/0.25 «mu»m, He, 6. K/min; Tstart: 60. C; Tend: 300. C
CapillarySPB-Sulfur959.Mariaca, Berger, et al., 199730. m/0.32 mm/4. «mu»m, He, 45. C @ 13. min, 5. K/min, 240. C @ 5. min
CapillarySE-54945.Kollmannsberger, Nitz, et al., 199230. m/0.25 mm/0.25 «mu»m, Hydrogen, 60. C @ 5. min, 2. K/min, 250. C @ 2. min

Normal alkane RI, non-polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
Capillary5 % Phenyl polydimethyl siloxane949.Chaverri, Diaz, et al., 2011Program: not specified
CapillarySLB-5 MS948.Scandinaro, Tranchida, et al., 201010. m/0.10 mm/0.10 «mu»m, Helium; Program: not specified
CapillaryDB-1949.Delort and Jaquier, 200960. m/0.25 mm/0.25 «mu»m, Helium; Program: 50 0C (5 min) 3 0C/min -> 120 0C 5 0C/min -> 250 0C (3 min) 15 0C/min -> 300 0C (20 min)
Capillary5 % Phenyl methyl siloxane950.Huang, Qin, et al., 200930. m/0.25 mm/0.25 «mu»m, Helium; Program: 50 0C (2 min) 10 0C/min -> 150 0C 15 0C/min -> 300 0C (10 min)
CapillaryDB-5 MS947.Silva, Doria, et al., 200830. m/0.25 mm/0.25 «mu»m; Program: 80 0C (1.5 min) 4 pC/min -> 180 0C 10 0C/min -> 300 0C (10 min)
CapillarySE-30952.Vinogradov, 2004Program: not specified
CapillaryHP-5940.Aparicio, Romero, et al., 200130. m/0.25 mm/0.25 «mu»m; Program: not specified
CapillaryDB-1938.da Silva, Pedro, et al., 200030. m/0.25 mm/0.25 «mu»m, H2; Program: 40 0C 3 K/min -> 175 0C 15 K/min -> 240 0C (10 min)
CapillaryDB-5951.Isidorov, Zenkevich, et al., 1997Program: not specified
CapillarySPB-Sulfur940.Mariaca, Berger, et al., 199730. m/0.32 mm/4. «mu»m, He; Program: not specified
CapillaryMethyl Silicone948.Zenkevich, 1996Program: not specified

Normal alkane RI, polar column, temperature ramp

View large format table.

Column type Active phase I Reference Comment
CapillaryHP-Innowax1068.Feng, Cui, et al., 201160. m/0.25 mm/0.25 «mu»m, Helium, 60. C @ 1. min, 5. K/min, 220. C @ 5. min
CapillarySupelcowax-101064.Neves, Rosa, et al., 201030. m/0.20 mm/0.20 «mu»m, Helium, 3. K/min, 220. C @ 15. min; Tstart: 70. C
CapillaryHP-Innowax1044.Cheraif, Ben Jannet, et al., 200730. m/0.25 mm/0.25 «mu»m, N2, 50. C @ 1. min, 5. K/min, 240. C @ 4. min
CapillaryTC-FFAP1070.Kurose, Okamura, et al., 2007He, 3. K/min, 220. C @ 30. min; Column diameter: 0.25 mm; Phase thickness: 0.25 «mu»m; Tstart: 60. C
CapillaryTC-FFAP1069.Kurose, Okamura, et al., 2007He, 3. K/min, 220. C @ 30. min; Column diameter: 0.25 mm; Phase thickness: 0.25 «mu»m; Tstart: 60. C
CapillarySupelcowax-101060.Raal, Orav, et al., 200730. m/0.25 mm/0.25 «mu»m, He, 2. K/min; Tstart: 50. C; Tend: 250. C
CapillarySupelcowax-101050.Vichi, Riu-Aumatell, et al., 200730. m/0.25 mm/0.25 «mu»m, He, 40. C @ 5. min, 3. K/min, 250. C @ 10. min
CapillaryInnowax1059.Abdelwahed, Hayder, et al., 200630. m/0.25 mm/0.25 «mu»m, N2, 50. C @ 3. min, 9. K/min, 280. C @ 3. min
CapillaryInnowax1059.Abdelwahed, Hayder, et al., 200630. m/0.25 mm/0.25 «mu»m, N2, 50. C @ 3. min, 9. K/min, 280. C @ 3. min
CapillaryHP-Wax1059.Marzouk, Mansour, et al., 200630. m/0.25 mm/0.25 «mu»m, Nitrogen, 5. K/min, 280. C @ 5. min; Tstart: 50. C
CapillaryHP-20M1059.Marzouk, Neffati, et al., 200630. m/0.25 mm/0.25 «mu»m, N2, 5. K/min, 250. C @ 10. min; Tstart: 50. C
CapillarySupelcowax-101057.Wong, Lim, et al., 200630. m/0.25 mm/0.25 «mu»m, He, 50. C @ 1. min, 4. K/min, 220. C @ 10. min
CapillaryHP-Innowax1070.Stashenko, Jaramillo, et al., 200350. m/0.2 mm/0.2 «mu»m, 50. C @ 5. min, 4. K/min; Tend: 220. C
CapillaryDB-Wax1056.Christoph, 200160. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 45. C; Tend: 240. C
CapillaryDB-Wax1082.Jiang and Kubota, 2001He, 2. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tstart: 40. C; Tend: 220. C
CapillaryDB-Wax1076.Tamura, Boonbumrung, et al., 2000Nitrogen, 40. C @ 10. min, 2. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tend: 200. C
CapillarySupelcowax-101053.Choo, Wong, et al., 199930. m/0.25 mm/0.25 «mu»m, 4. K/min; Tstart: 60. C; Tend: 220. C
CapillaryDB-Wax1062.Ngassoum, Yonkeu, et al., 199960. m/0.25 mm/0.25 «mu»m, He, 4. K/min; Tstart: 60. C; Tend: 240. C
CapillaryBP-201084.Bignell, Dunlop, et al., 199825. m/0.33 mm/0.5 «mu»m, H2, 5. K/min; Tstart: 80. C; Tend: 220. C
CapillaryBP-201084.Bignell, Dunlop, et al., 199725. m/0.33 mm/0.5 «mu»m, H2, 5. K/min; Tstart: 80. C; Tend: 220. C
CapillaryBP-201084.Bignell, Dunlop, et al., 1997, 225. m/0.33 mm/0.5 «mu»m, H2, 5. K/min; Tstart: 80. C; Tend: 220. C
CapillarySP-10001060.Brophy, Goldsack, et al., 1996He, 3. K/min; Column length: 85. m; Column diameter: 0.50 mm; Tstart: 65. C; Tend: 225. C
CapillaryCarbowax 20M1073.Kollmannsberger, Nitz, et al., 199245. m/0.32 mm/1.0 «mu»m, Hydrogen, 60. C @ 5. min, 2. K/min; Tend: 200. C
CapillaryBP-201070.MacLeod and Snyder, 198570. C @ 5. min, 3. K/min; Column length: 25. m; Column diameter: 0.2 mm; Tend: 180. C

Normal alkane RI, polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryHP-Innowax1054.Feng, Cui, et al., 201160. m/0.25 mm/0.25 «mu»m, Helium; Program: not specified
CapillaryCarbowax 20M1080.Vinogradov, 2004Program: not specified
CapillaryHP-Innowax FSC1072.Demirci, Baser, et al., 200360. m/0.25 mm/0.25 «mu»m, He; Program: 60C (10min) => 4C/min => 220C (10min) => 1C/min => 240C
CapillaryInnowax FSC1072.Tunalier, Kirimer, et al., 200260. m/0.25 mm/0.25 «mu»m; Program: 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
CapillaryHP-Innowax FSC1072.Bagci, Baser, et al., 199960. m/0.25 mm/0.25 «mu»m, He; Program: 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Notes

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