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1H-3a,7-Methanoazulene, 2,3,4,7,8,8a-hexahydro-3,6,8,8-tetramethyl-, [3R-(3«alpha»,3a«beta»,7«beta»,8a«alpha»)]-


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Optima-5DB-5 MSDB-5HP-5 MSDB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.50.100.40.
Tend (C) 246.270.250.220.250.
Heat rate (K/min) 3.3.2.2.10.
Initial hold (min) 1.   1.
Final hold (min)     3.
I 1415.1407.1412.1410.1412.
ReferenceAl-Qudah, Muhaidat, et al., 2012Cui, Yang, et al., 2011Ho, Wang, et al., 2010Pripdeevech, Chumpolsri, et al., 2010Yang, Zhang, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5HP-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumNitrogenN2Helium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 35.50.50.60.100.
Tend (C) 220.250.280.220.300.
Heat rate (K/min) 3.5.5.5.20.
Initial hold (min)  2.1.10.2.
Final hold (min) 40. 1. 10.
I 1409.1412.1436.1411.1409.
ReferenceEl-Massry, El-Ghorab, et al., 2009Ho, Wang, et al., 2009Bousaada, Ammar, et al., 2008Flamini, Tebano, et al., 2008Khokra, Prakash, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5MSHP-1HP-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeHeliumHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.320.250.250.320.25
Tstart (C) 60.60.70.60.50.
Tend (C) 250.240.200.250.280.
Heat rate (K/min) 5.3.10.5.9.
Initial hold (min) 30.  30.3.
Final hold (min)     3.
I 1408.1413.1413.1408.1420.
ReferenceYassa and Akhani, 2008Argyropoulou, Daferera, et al., 2007Dongmo, Tatsadjieu, et al., 2007Yassa and Akhani, 2007Abdelwahed, Hayder, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5BP-1DB-1HP-5
Column length (m) 30.30.50.50.30.
Carrier gas N2HeHeN2He
Substrate      
Column diameter (mm) 0.250.320.220.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.60.95.60.
Tend (C) 280.246.220.240.220.
Heat rate (K/min) 9.3.2.4.5.
Initial hold (min) 3.   10.
Final hold (min) 3. 20.  
I 1438.1410.1413.1397.1414.
ReferenceAbdelwahed, Hayder, et al., 2006Coronel, Cerda-Garcia-Rojas, et al., 2006Lesueur, Ban, et al., 2006Pala-Paul J., Perez-Alonso M.J., et al., 2006Pintore G., Chessa M., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5Ultra-2DB-5HP-1DB-1
Column length (m) 30.50.30.50.30.
Carrier gas HydrogenHeHe He
Substrate      
Column diameter (mm) 0.250.250.250.20.25
Phase thickness (mum) 0.250.320.250.250.25
Tstart (C) 120.50.40.60.50.
Tend (C) 180.270.260.250.265.
Heat rate (K/min) 2.2.2.2.2.5
Initial hold (min)   5.60.1.
Final hold (min)   20. 20.
I 1430.1434.1405.1389.1389.
ReferencePripdeevech, Wongpornchai, et al., 2006Schlumpberger B.O., Clery R.A., et al., 2006Senatore, Landolfi, et al., 2006Fernandez, Lizzani-Cuvelier, et al., 2005Khanavi, Ghasemian, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1CP Sil 5 CBCP Sil 5 CBHP-5MS
Column length (m) 30.50.30.30.30.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.95.40.40.60.
Tend (C) 265.240.220.220.280.
Heat rate (K/min) 2.54.4.4.3.
Initial hold (min) 1. 1.1. 
Final hold (min) 30.    
I 1390.1405.1412.1412.1408.
ReferenceKhalighi-Sigaroodi, Hadijiakhoondi, et al., 2005Palá-Paúl, Pérez-Alonso, et al., 2005Rohloff and Bones, 2005Rohloff and Bones, 2005Slavkovska, Couladis, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1SPB-5HP-5DB-5HP-1
Column length (m) 60.60.25.30.30.
Carrier gas N2HeH2HeHe
Substrate      
Column diameter (mm) 0.250.320.320.250.25
Phase thickness (mum) 0.251.0.520.250.25
Tstart (C) 70.60.40.60.70.
Tend (C) 230.200.240.240.200.
Heat rate (K/min) 2.4.4.4.10.
Initial hold (min) 2.    
Final hold (min) 20.30.   
I 1421.1409.1444.1411.1400.
ReferenceChoi, 2004Gauvin, Ravaomanarivo, et al., 2004Simic, Sokovic, et al., 2004Cabanillas, Lopez, et al., 2003Fekam Boyom, Amvam Zollo, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5MSDB-5MSDB-1DB-5
Column length (m) 30.30.30.50.30.
Carrier gas N2HeHeN2He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.60.95.60.
Tend (C) 200.280.240.240.240.
Heat rate (K/min) 5.4.3.4.3.
Initial hold (min)      
Final hold (min)      
I 1397.1409.1418.1394.1408.
ReferenceFekam Boyom, Ngouana, et al., 2003Ghasemi, Asghari, et al., 2003Maia, Taveira, et al., 2003Perez-Alonso, Velasco-Negueruela, et al., 2003da Silva, Luz, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5HP-5DB-5DB-1
Column length (m) 30.60.60.30.50.
Carrier gas He  HeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.40.40.35.80.
Tend (C) 240.250.250.280.225.
Heat rate (K/min) 3.5.5.4.4.
Initial hold (min)  15.15.2. 
Final hold (min)    15. 
I 1410.1420.1420.1420.1394.
Referenceda Silva, Luz, et al., 2003Stashenko, Jaramillo, et al., 2003Stashenko, Jaramillo, et al., 2003Krauze-Baranowska, Mardarowicz, et al., 2002Palá-Paúl, Pérez-Alonso, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-1OV-101DB-5
Column length (m) 30.30.25.50.30.
Carrier gas HeHeH2N2He
Substrate      
Column diameter (mm) 0.250.250.320.20.25
Phase thickness (mum) 0.250.250.17 0.25
Tstart (C) 60.60.40.80.60.
Tend (C) 300.240.260.200.240.
Heat rate (K/min) 2.3.3.1.3.
Initial hold (min)   5.  
Final hold (min)    20. 
I 1389.1409.1393.1433.1410.
ReferenceRuberto, Biondi, et al., 2002Tellez M., Estell R., et al., 2001Lopes, Koketsu, et al., 1999Menon, Chacko, et al., 1999Tellez, Canel, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-5DB-5DB-1HP-101
Column length (m) 25.30.30.60.50.
Carrier gas N2HeHeliumHeH2
Substrate      
Column diameter (mm) 0.320.250.250.250.32
Phase thickness (mum) 0.250.250.250.250.3
Tstart (C) 50.65.60.50.65.
Tend (C) 290.300.240.250.300.
Heat rate (K/min) 4.4.3.2.52.
Initial hold (min)  2. 5.5.
Final hold (min)      
I 1398.1420.1411.1435.1407.
ReferenceBos, Woerdenbag, et al., 1997Elias, Simoneit, et al., 1997Tellez, Estell, et al., 1997Stashenko, Puertas, et al., 1996Demarne and van der Walt, 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1SE-30SE-30SE-30SE-30+Igepal
Column length (m) 60.30.30.50.100.
Carrier gas    He 
Substrate      
Column diameter (mm) 0.32  0.50.25
Phase thickness (mum)      
Tstart (C) 50.50.50.40.70.
Tend (C) 230.240.240.170.170.
Heat rate (K/min) 4.4.4.3.1.
Initial hold (min)  2.2.3. 
Final hold (min) 10.10.10.  
I 1409.1411.1411.1434.1435.
ReferenceBinder, Benson, et al., 1990Ramaswami, Briscese, et al., 1988Ramaswami, Briscese, et al., 1986Heydanek and McGorrin, 1981Shibamoto and Jennings, 1977
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase SE-30+Igepal
Column length (m) 100.
Carrier gas  
Substrate  
Column diameter (mm) 0.25
Phase thickness (mum)  
Tstart (C) 70.
Tend (C) 170.
Heat rate (K/min) 1.
Initial hold (min)  
Final hold (min)  
I 1436.
ReferenceShibamoto and Jennings, 1977
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Al-Qudah, Muhaidat, et al., 2012
Al-Qudah, M.A.; Muhaidat, R.; Trawenh, I.N.; Jaber, H.I.; Abu Zarga, M.H.; Abu Orabi, S.T., Volatile constituents of leaves and bulbs of Gynandriris Sisyrinchicum and their antimicrobial activities, Jordan J. Chem., 2012, 7, 3, 287-295. [all data]

Cui, Yang, et al., 2011
Cui, J.; Yang, X.; Dong, A.-J.; Cheng, D.-Y.; Wang, J.; Zhao, H.-T.; Xu, R.-B.; Wang, P.; Li, W.-J., Chemical composition and antioxidant activity of Wuphorbia fischeriana essential oil from China, J. Med. Plants Res., 2011, 5, 19, 4894-4798. [all data]

Ho, Wang, et al., 2010
Ho, C.-L.; Wang, E.I.-C.; Yu, H.-T.; Yu, H.-M.; Su, Y.-C., Composition amd antioxidant activities of essential oils of different tissues from Cryptomeria japonica D. Don, Quarterly J. Chin. Forestry, 2010, 32, 1, 63-76. [all data]

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Yassa, N.; Akhani, H., The essential oils composition in two species of the genus Eriocycla Lindl. (Apiaceae) from Iran, 2007, retrieved from http://biology.ut.ac.ir/members/akhani/PdfReprintNumber/27.pdf. [all data]

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Choi, 2004
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Gauvin, Ravaomanarivo, et al., 2004
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Simic, Sokovic, et al., 2004
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Cabanillas, Lopez, et al., 2003
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Fekam Boyom, Amvam Zollo, et al., 2003
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Fekam Boyom, Ngouana, et al., 2003
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Ghasemi, Asghari, et al., 2003
Ghasemi, N.; Asghari, G.; Ardakani, M.S.; Siahpoush, A., Characterization of volatile constituents from aerial parts of varthemia persica DC (var. persica), Iran. J. Pharm. Res., 2003, 2, 241-243. [all data]

Maia, Taveira, et al., 2003
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Perez-Alonso, Velasco-Negueruela, et al., 2003
Perez-Alonso, M.J.; Velasco-Negueruela, A.; Palá-Paúl, J.; Sanz, J., Variations in the essential oil composition of Artemisia pedemontana gathered in Spain: chemotype camphor-1,8-cineole and chemotype davanone, Biochem. Syst. Ecol., 2003, 31, 1, 77-84, https://doi.org/10.1016/S0305-1978(02)00082-0 . [all data]

da Silva, Luz, et al., 2003
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Notes

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