1H-3a,7-Methanoazulene, 2,3,4,7,8,8a-hexahydro-3,6,8,8-tetramethyl-, [3R-(3α,3aβ,7β,8aα)]-


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillarySE-30100.1433.4Tudor, 199740. m/0.35 mm/0.35 μm
CapillaryOV-101100.1393.Diez, Guillen, et al., 1990N2; Column length: 25. m; Column diameter: 0.23 mm
CapillarySqualane100.1392.3Diez, Guillen, et al., 1990N2; Column length: 45. m; Column diameter: 0.5 mm
CapillarySE-54100.1403.3Diez, Guillen, et al., 1990N2; Column length: 25. m; Column diameter: 0.22 mm
CapillaryOV-101100.1393.Bermejo, Blanco, et al., 1987N2; Column length: 25. m; Column diameter: 0.23 mm
PackedSF-96150.1431.Maarse, 1975Chromosorb W-AW; Column length: 3.0 m
PackedSE-30130.1414.Andersen and Falcone, 1969He, Chromosorb G

Kovats' RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillarySPB-11403.Walde, Jyothirmayi, et al., 200630. m/0.32 mm/0.25 μm, He, 60. C @ 4. min, 4. K/min, 240. C @ 2. min
CapillaryHP-5MS1408.Juliani, Zygadlo, et al., 200430. m/0.25 mm/0.25 μm, He, 60. C @ 1. min, 4. K/min, 200. C @ 15. min
CapillarySPB-11405.Yadav, Chauhan, et al., 200430. m/0.32 mm/0.25 μm, He, 50. C @ 2. min, 2. K/min, 250. C @ 5. min
CapillaryDB-51404.Amparo Blázquez, Pérez, et al., 2003He, 40. C @ 5. min, 3. K/min, 280. C @ 5. min; Column length: 25. m; Column diameter: 0.25 mm
CapillaryDB-51412.Lucero, Estell, et al., 200330. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C
CapillarySE-301411.Palá-Paúl, Velasco-Negueruela, et al., 200225. m/0.22 mm/0.25 μm, He, 4. K/min; Tstart: 70. C; Tend: 220. C
CapillaryBP-11411.Jain, Aggarwal, et al., 200125. m/0.55 mm/0.25 μm, N2, 5. K/min, 220. C @ 15. min; Tstart: 60. C
CapillarySE-541409.Adams, 200030. m/0.26 mm/0.25 μm, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillaryDB-51409.Adams, 2000, 230. m/0.26 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillaryDB-51409.Adams, 199930. m/0.26 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillaryDB-51415.da Silva, Andrade, et al., 199930. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryHP-11398.Raharivelomanana, Cambon, et al., 19936. K/min, 240. C @ 10. min; Column length: 15. m; Column diameter: 0.32 mm; Tstart: 40. C
CapillaryOV-1011434.Gaydou, Randriamiharisoa, et al., 1986100. m/0.3 mm/0.15 μm, H2, 2. K/min; Tstart: 90. C; Tend: 220. C

Kovats' RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryBP-11414.Khan, Srivastava, et al., 200325. m/0.25 mm/0.25 μm, N2; Program: 60C => 5C/min => 220C (5min) => 3C/min => 245 C (5min)
CapillaryBP-11414.Khan, Srivastava, et al., 200230. m/0.32 mm/0.25 μm, N2; Program: 60 C 5 C/min -> 220 C (5 min) 3 C/min -> 245 C (5 min)

Kovats' RI, polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
PackedCarbowax 20M132.1598.Andersen and Falcone, 1969 
PackedCarbowax 20M132.1598.Andersen and Falcone, 1969 

Kovats' RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryCarbowax 20M1574.Gaydou, Randriamiharisoa, et al., 198650. m/0.3 mm/0.15 μm, H2, 2. K/min; Tstart: 70. C; Tend: 210. C

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-51409.Quijano, Salamanca, et al., 200730. m/0.25 mm/0.25 μm, He, 50. C @ 4. min, 4. K/min, 250. C @ 10. min
CapillaryHP-5MS1410.Saroglou, Marin, et al., 200730. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 4. K/min; Tend: 280. C
CapillaryZB-51408.Simoniatto, Bonani, et al., 200730. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 250. C
CapillaryHP-5MS1411.Zeng, Zhao, et al., 200730. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 80. C; Tend: 300. C
CapillaryHP-5MS1386.Basta, Tzakou, et al., 200630. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillarySPB-11405.Blagojevic, Radulovic, et al., 200630. m/0.25 mm/0.25 μm, He, 50. C @ 3. min, 5. K/min, 250. C @ 15. min
CapillaryDB-51411.Blagojevic, Radulovic, et al., 200630. m/0.2 mm/0.25 μm, He, 50. C @ 3. min, 5. K/min, 250. C @ 15. min
CapillaryRTX-11414.Cavalli, Tomi, et al., 200660. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 45. min; Tstart: 60. C
CapillaryBP-11419.Duquesnoy, Dinh, et al., 200650. m/0.22 mm/0.25 μm, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryHP-51419.Flamini, Tebano, et al., 200630. m/0.25 mm/0.25 μm, N2, 60. C @ 10. min, 5. K/min; Tend: 220. C
CapillaryBP-11415.Gonny, Cavaleiro, et al., 200650. m/0.22 mm/0.25 μm, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryDB-11404.Kuiate, Bessière, et al., 200630. m/0.25 mm/0.25 μm, N2, 4. K/min; Tstart: 50. C; Tend: 220. C
CapillaryHP-5MS1409.Saroglou, Dorizas, et al., 200630. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 4. K/min; Tend: 280. C
CapillaryDB-51412.Su, Ho, et al., 200630. m/0.25 mm/0.25 μm, He, 50. C @ 2. min, 5. K/min; Tend: 250. C
CapillaryDB-51412.Su, Ho, et al., 2006, 230. m/0.25 mm/0.25 μm, He, 50. C @ 2. min, 5. K/min; Tend: 250. C
CapillaryHP-5MS1403.Vujisic L., Vuckovic I., et al., 200630. m/0.25 mm/0.25 μm, H2, 4.3 K/min; Tstart: 50. C; Tend: 285. C
CapillarySPB-11434.Boskovic, Radulovic, et al., 200530. m/0.25 mm/0.25 μm, He, 50. C @ 3. min, 5. K/min, 250. C @ 15. min
CapillaryDB-51422.Boskovic, Radulovic, et al., 200530. m/0.2 mm/0.25 μm, He, 50. C @ 3. min, 5. K/min, 250. C @ 15. min
CapillaryHP-5MS1409.Pino, Mesa, et al., 200530. m/0.25 mm/0.25 μm, He, 60. C @ 2. min, 4. K/min, 250. C @ 20. min
CapillaryDB-51396.Sati and Mathela, 200530. m/0.25 mm/0.26 μm, He, 3. K/min; Tstart: 60. C; Tend: 210. C
CapillaryHP-5MS1406.Aligiannis, Kalpoutzakis, et al., 200430. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryHP-51411.Bertoli, Menichini, et al., 200430. m/0.25 mm/0.25 μm, N2, 60. C @ 10. min, 5. K/min; Tend: 220. C
CapillaryBP-11415.Gonny, Bradesi, et al., 200450. m/0.22 mm/0.25 μm, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryHP-5MS1408.Grujic-Jovanovic, Skaltsa, et al., 200430. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 4. K/min; Tend: 280. C
CapillarySPB-51409.Pino, Marbot, et al., 200430. m/0.25 mm/0.25 μm, He, 60. C @ 2. min, 4. K/min, 250. C @ 20. min
CapillaryHP-51411.Angelini, Carpanese, et al., 200330. m/0.25 mm/0.25 μm, N2, 60. C @ 10. min, 5. K/min; Tend: 220. C
CapillaryRTX-11414.Cavalli, Tomi, et al., 200360. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 45. min; Tstart: 60. C
CapillaryHP-51411.Ertugrul, Dural, et al., 200330. m/0.25 mm/0.25 μm, N2, 60. C @ 10. min, 5. K/min; Tend: 220. C
CapillaryHP-51408.Skaltsa, Demetzos, et al., 200330. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 4. K/min; Tend: 280. C
CapillaryDB-51411.Flamini, Cioni, et al., 200230. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryRTX-51409.Shellie, Mondello, et al., 200230. m/0.25 mm/0.25 μm, He, 45. C @ 6. min, 3. K/min; Tend: 250. C
CapillaryRTX-51410.Shellie, Mondello, et al., 200230. m/0.25 mm/0.25 μm, He, 45. C @ 6. min, 3. K/min; Tend: 250. C
CapillaryHP-51407.Aligiannis, Kalpoutzakis, et al., 200130. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 3. K/min; Tend: 280. C
CapillaryDB-51408.Nogueira, Bittrich, et al., 200130. m/0.25 mm/0.25 μm, H2, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryHP-5MS1408.Skaltsa, Mavrommati, et al., 200130. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 4. K/min; Tend: 280. C
CapillaryHP-51409.Lazari, Skaltsa, et al., 200030. m/0.25 mm/0.25 μm, He, 50. C @ 5. min, 4. K/min; Tend: 280. C
CapillaryMethyl Silicone1435.Sumathykutty, Rao, et al., 199950. m/0.25 mm/0.17 μm, N2, 2. K/min; Tstart: 80. C; Tend: 200. C
CapillaryDB-11438.Stashenko, Prada, et al., 199660. m/0.25 mm/0.25 μm, He, 50. C @ 5. min, 3.5 K/min; Tend: 250. C
CapillaryCP Sil 5 CB1409.Chanegriha and Baaliouamer, 199325. m/0.22 mm/0.11 μm, He, 80. C @ 8. min, 1. K/min, 230. C @ 16. min
CapillaryOV-1011422.Yang, Sugisawa, et al., 1992N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillaryOV-1011423.Yang, Sugisawa, et al., 1992N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-5MS1416.7Andriamaharavo, 201430. m/0.25 mm/0.25 μm, He; Program: 60C (1 min) => 5 C/min => 210C => 10 C/min => 280C (15 min)
CapillaryCP-Sil5 CB MS1413.0Helmig, Bocquet, et al., 200460. m/0.32 mm/0.25 μm, He; Program: 40C(1min) => 25C/min => 120C => 2C/min => 190C => 25C/min => 250C (5min)
CapillaryDB-11383.1Helmig, Bocquet, et al., 200430. m/0.32 mm/0.1 μm, He; Program: 40C(5min) => 20C/min => 100C => 2C/min => 160C => 40C/min => 250C (5min)
CapillaryDB-11396.9Helmig, Bocquet, et al., 200430. m/0.32 mm/0.25 μm, He; Program: 40C(5min) => 20C/min => 100C => 2C/min => 160C => 40C/min => 250C (5min)
CapillaryCP Sil 5 CB1436.Chanegriha, Baaliouamer, et al., 1998Program: not specified
CapillarySE-521421.Mondello, Dugo, et al., 199560. m/0.32 mm/0.40 μm, He; Program: 45 C (6 min) 3 C/min -> 111 0C 2 C/min -> 160 C 3 C/min -> 300 C (15 min)

Van Den Dool and Kratz RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryRTX-Wax1566.Cavalli, Tomi, et al., 200660. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 45. min; Tstart: 60. C
CapillaryBP-201565.Duquesnoy, Dinh, et al., 200650. m/0.22 mm/0.25 μm, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryHP-Wax1568.Flamini, Tebano, et al., 200630. m/0.25 mm/0.25 μm, N2, 60. C @ 10. min, 5. K/min; Tend: 220. C
CapillaryBP-201570.Gonny, Cavaleiro, et al., 200650. m/0.22 mm/0.25 μm, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryDB-Wax1571.Njoroge, Koaze, et al., 200560. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillaryDB-Wax1579.Bertoli, Menichini, et al., 200430. m/0.25 mm/0.25 μm, N2, 60. C @ 10. min, 5. K/min; Tend: 220. C
CapillaryBP-201565.Gonny, Bradesi, et al., 200450. m/0.22 mm/0.25 μm, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryRTX-Wax1562.Cavalli, Tomi, et al., 200360. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 45. min; Tstart: 60. C
CapillaryDB-Wax1574.Choi and Sawamura, 200060. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillaryDB-Wax1599.Stashenko, Prada, et al., 199660. m/0.25 mm/0.25 μm, He, 50. C @ 5. min, 2.5 K/min; Tend: 180. C
CapillaryCarbowax 20M1576.Mondello, Dugo, et al., 199560. m/0.32 mm/0.425 μm, He, 45. C @ 3. min, 3. K/min, 300. C @ 20. min

Van Den Dool and Kratz RI, polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryBP-201600.Chanegriha, Baaliouamer, et al., 1998He; Program: not specified

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryOptima-51415.Al-Qudah, Muhaidat, et al., 201230. m/0.25 mm/0.25 μm, Helium, 60. C @ 1. min, 3. K/min; Tend: 246. C
CapillaryDB-5 MS1407.Cui, Yang, et al., 201130. m/0.25 mm/0.25 μm, Helium, 3. K/min; Tstart: 60. C; Tend: 270. C
CapillaryDB-51412.Ho, Wang, et al., 201030. m/0.25 mm/0.25 μm, Helium, 2. K/min; Tstart: 50. C; Tend: 250. C
CapillaryHP-5 MS1410.Pripdeevech, Chumpolsri, et al., 201030. m/0.25 mm/0.25 μm, Helium, 2. K/min; Tstart: 100. C; Tend: 220. C
CapillaryDB-51412.Yang, Zhang, et al., 201030. m/0.25 mm/0.25 μm, Helium, 40. C @ 1. min, 10. K/min, 250. C @ 3. min
CapillaryDB-51409.El-Massry, El-Ghorab, et al., 200930. m/0.25 mm/0.25 μm, Helium, 3. K/min, 220. C @ 40. min; Tstart: 35. C
CapillaryDB-51412.Ho, Wang, et al., 200930. m/0.25 mm/0.25 μm, Helium, 50. C @ 2. min, 5. K/min; Tend: 250. C
CapillaryHP-51436.Bousaada, Ammar, et al., 200830. m/0.25 mm/0.25 μm, Nitrogen, 50. C @ 1. min, 5. K/min, 280. C @ 1. min
CapillaryHP-51411.Flamini, Tebano, et al., 200830. m/0.25 mm/0.25 μm, N2, 60. C @ 10. min, 5. K/min; Tend: 220. C
CapillaryDB-51409.Khokra, Prakash, et al., 200830. m/0.25 mm/0.25 μm, Helium, 100. C @ 2. min, 20. K/min, 300. C @ 10. min
CapillaryHP-51408.Yassa and Akhani, 200830. m/0.25 mm/0.32 μm, Helium, 60. C @ 30. min, 5. K/min; Tend: 250. C
CapillaryHP-5MS1413.Argyropoulou, Daferera, et al., 200730. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryHP-11413.Dongmo, Tatsadjieu, et al., 200730. m/0.25 mm/0.25 μm, Helium, 10. K/min; Tstart: 70. C; Tend: 200. C
CapillaryHP-51408.Yassa and Akhani, 200730. m/0.25 mm/0.32 μm, He, 60. C @ 30. min, 5. K/min; Tend: 250. C
CapillaryHP-51420.Abdelwahed, Hayder, et al., 200630. m/0.25 mm/0.25 μm, N2, 50. C @ 3. min, 9. K/min, 280. C @ 3. min
CapillaryHP-51438.Abdelwahed, Hayder, et al., 200630. m/0.25 mm/0.25 μm, N2, 50. C @ 3. min, 9. K/min, 280. C @ 3. min
CapillaryHP-51410.Coronel, Cerda-Garcia-Rojas, et al., 200630. m/0.32 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillaryBP-11413.Lesueur, Ban, et al., 200650. m/0.22 mm/0.25 μm, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryDB-11397.Pala-Paul J., Perez-Alonso M.J., et al., 200650. m/0.25 mm/0.25 μm, N2, 4. K/min; Tstart: 95. C; Tend: 240. C
CapillaryHP-51414.Pintore G., Chessa M., et al., 200630. m/0.25 mm/0.25 μm, He, 60. C @ 10. min, 5. K/min; Tend: 220. C
CapillaryDB-51430.Pripdeevech, Wongpornchai, et al., 200630. m/0.25 mm/0.25 μm, Hydrogen, 2. K/min; Tstart: 120. C; Tend: 180. C
CapillaryUltra-21434.Schlumpberger B.O., Clery R.A., et al., 200650. m/0.25 mm/0.32 μm, He, 2. K/min; Tstart: 50. C; Tend: 270. C
CapillaryDB-51405.Senatore, Landolfi, et al., 200630. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 2. K/min, 260. C @ 20. min
CapillaryHP-11389.Fernandez, Lizzani-Cuvelier, et al., 200550. m/0.2 mm/0.25 μm, 60. C @ 60. min, 2. K/min; Tend: 250. C
CapillaryDB-11389.Khanavi, Ghasemian, et al., 200530. m/0.25 mm/0.25 μm, He, 50. C @ 1. min, 2.5 K/min, 265. C @ 20. min
CapillaryDB-11390.Khalighi-Sigaroodi, Hadijiakhoondi, et al., 200530. m/0.25 mm/0.25 μm, He, 50. C @ 1. min, 2.5 K/min, 265. C @ 30. min
CapillaryDB-11405.Palá-Paúl, Pérez-Alonso, et al., 200550. m/0.25 mm/0.25 μm, N2, 4. K/min; Tstart: 95. C; Tend: 240. C
CapillaryCP Sil 5 CB1412.Rohloff and Bones, 200530. m/0.25 mm/0.25 μm, He, 40. C @ 1. min, 4. K/min; Tend: 220. C
CapillaryCP Sil 5 CB1412.Rohloff and Bones, 200530. m/0.25 mm/0.25 μm, He, 40. C @ 1. min, 4. K/min; Tend: 220. C
CapillaryHP-5MS1408.Slavkovska, Couladis, et al., 200530. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryDB-11421.Choi, 200460. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillarySPB-51409.Gauvin, Ravaomanarivo, et al., 200460. m/0.32 mm/1. μm, He, 4. K/min, 200. C @ 30. min; Tstart: 60. C
CapillaryHP-51444.Simic, Sokovic, et al., 200425. m/0.32 mm/0.52 μm, H2, 4. K/min; Tstart: 40. C; Tend: 240. C
CapillaryDB-51411.Cabanillas, Lopez, et al., 200330. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 60. C; Tend: 240. C
CapillaryHP-11400.Fekam Boyom, Amvam Zollo, et al., 200330. m/0.25 mm/0.25 μm, He, 10. K/min; Tstart: 70. C; Tend: 200. C
CapillaryDB-11397.Fekam Boyom, Ngouana, et al., 200330. m/0.25 mm/0.25 μm, N2, 5. K/min; Tstart: 50. C; Tend: 200. C
CapillaryHP-5MS1409.Ghasemi, Asghari, et al., 200330. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 60. C; Tend: 280. C
CapillaryDB-5MS1418.Maia, Taveira, et al., 200330. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-11394.Perez-Alonso, Velasco-Negueruela, et al., 200350. m/0.25 mm/0.25 μm, N2, 4. K/min; Tstart: 95. C; Tend: 240. C
CapillaryDB-51408.da Silva, Luz, et al., 200330. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-51410.da Silva, Luz, et al., 200330. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryHP-51420.Stashenko, Jaramillo, et al., 200360. m/0.25 mm/0.25 μm, 40. C @ 15. min, 5. K/min; Tend: 250. C
CapillaryHP-51420.Stashenko, Jaramillo, et al., 200360. m/0.25 mm/0.25 μm, 40. C @ 15. min, 5. K/min; Tend: 250. C
CapillaryDB-51420.Krauze-Baranowska, Mardarowicz, et al., 200230. m/0.25 mm/0.25 μm, He, 35. C @ 2. min, 4. K/min, 280. C @ 15. min
CapillaryDB-11394.Palá-Paúl, Pérez-Alonso, et al., 200250. m/0.25 mm/0.25 μm, N2, 4. K/min; Tstart: 80. C; Tend: 225. C
CapillaryDB-51389.Ruberto, Biondi, et al., 200230. m/0.25 mm/0.25 μm, He, 2. K/min; Tstart: 60. C; Tend: 300. C
CapillaryDB-51409.Tellez M., Estell R., et al., 200130. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryHP-11393.Lopes, Koketsu, et al., 199925. m/0.32 mm/0.17 μm, H2, 40. C @ 5. min, 3. K/min; Tend: 260. C
CapillaryOV-1011433.Menon, Chacko, et al., 1999N2, 1. K/min, 200. C @ 20. min; Column length: 50. m; Column diameter: 0.2 mm; Tstart: 80. C
CapillaryDB-51410.Tellez, Canel, et al., 199930. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryCP Sil 5 CB1398.Bos, Woerdenbag, et al., 199725. m/0.32 mm/0.25 μm, N2, 4. K/min; Tstart: 50. C; Tend: 290. C
CapillaryDB-51420.Elias, Simoneit, et al., 199730. m/0.25 mm/0.25 μm, He, 65. C @ 2. min, 4. K/min; Tend: 300. C
CapillaryDB-51411.Tellez, Estell, et al., 199730. m/0.25 mm/0.25 μm, Helium, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-11435.Stashenko, Puertas, et al., 199660. m/0.25 mm/0.25 μm, He, 50. C @ 5. min, 2.5 K/min; Tend: 250. C
CapillaryHP-1011407.Demarne and van der Walt, 199350. m/0.32 mm/0.3 μm, H2, 65. C @ 5. min, 2. K/min; Tend: 300. C
CapillaryDB-11409.Binder, Benson, et al., 19904. K/min, 230. C @ 10. min; Column length: 60. m; Column diameter: 0.32 mm; Tstart: 50. C
CapillarySE-301411.Ramaswami, Briscese, et al., 198850. C @ 2. min, 4. K/min, 240. C @ 10. min; Column length: 30. m
CapillarySE-301411.Ramaswami, Briscese, et al., 198650. C @ 2. min, 4. K/min, 240. C @ 10. min; Column length: 30. m
CapillarySE-301434.Heydanek and McGorrin, 1981He, 40. C @ 3. min, 3. K/min; Column length: 50. m; Column diameter: 0.5 mm; Tend: 170. C
CapillarySE-30+Igepal1435.Shibamoto and Jennings, 19771. K/min; Column length: 100. m; Column diameter: 0.25 mm; Tstart: 70. C; Tend: 170. C
CapillarySE-30+Igepal1436.Shibamoto and Jennings, 19771. K/min; Column length: 100. m; Column diameter: 0.25 mm; Tstart: 70. C; Tend: 170. C

Normal alkane RI, non-polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryCBP-51411.de Morais, Oliveira, et al., 201230. m/0.25 mm/0.25 μm, Helium; Program: 60 0C 3 0C/min -> 240 0C 10 0C/min -> 280 0C (10 min)
CapillaryPolydimethyl siloxane with 5 % Ph groups1410.Robinson, Adams, et al., 2012Program: not specified
CapillaryPolydimethyl siloxane with 5 % Ph groups1419.Robinson, Adams, et al., 2012Program: not specified
CapillaryHP-5 MS1409.Liu, Chu, et al., 201030. m/0.25 mm/0.25 μm, Helium; Program: 60 0C (1 min) 10 0C/min -> 180 0C (1 min) 20 0C/min -> 280 0C (15 min)
CapillaryDB-51416.Courtois, Paine, et al., 200930. m/0.25 mm/0.25 μm, Helium; Program: 50 0C m6 0C/min -> 140 0C 5 0C/min -> 160 0C (1 min) 10 0C/min -> 200 0C
CapillaryHP-51413.Custer, 200925. m/0.32 mm/0.17 μm, Helium; Program: 60 0C (5 min) 4 0C/min -> 220 0C 11 0C/min -> 280 0C (15 min)
CapillaryHP-51411.Custer, 200925. m/0.32 mm/0.17 μm, Helium; Program: not specified
CapillaryHP-5 MS1411.Mancini, Arnold, et al., 200930. m/0.25 mm/0.25 μm, Helium; Program: 40 0C (5 min) 2 0C/min -> 270 0C -> 260 0C (20 min)
CapillaryHP-5 MS1383.Zellner, Amorim, et al., 200930. m/0.25 mm/0.25 μm, Helium; Program: 32 0C (1 min) 50 0C/min -> 115 0C 1.5 0C/min -> 145 0C 12 0C/min -> 240 0C (10 min)
CapillaryCP Sil 8 CB1415.Meekijjaroenroj, Bessière, et al., 200730. m/0.25 mm/0.25 μm, He; Program: 50C(3min) => 3C/min => 100C => 2.7C/min => 140C => 2.4C/min => 180C => 6C/min => 250C
CapillaryHP-5MS1410.Moronkola, Ogunwande, et al., 200730. m/0.25 mm/0.25 μm, He; Program: 40C(10min) => 3C/min => 200C => 2C/min => 220C
CapillaryCP-Sil1372.Proffit, 200730. m/0.25 mm/0.25 μm, Helium; Program: 50 0C (3 min) 3 0C/min -> 100 0C 2.7 0C/min -> 140 0C 2.4 0C/min -> 180 0C 6 0C/min -> 250 0C
CapillaryHP-5MS1432.Deng, Xu, et al., 200630. m/0.25 mm/0.25 μm, He; Program: 50C(2min) => 6C/min => 200C => 10C/min => 270C(10min)
CapillaryDB-51412.Pripdeevech, Wongpornchai, et al., 200630. m/0.25 mm/0.25 μm, Hydrogen; Program: not specified
CapillaryHP-5MS1411.Senatore, Apostolides Arnold, et al., 200630. m/0.25 mm/0.25 μm, He; Program: 40C(5min) => 2C/min => 250C (15min) => 10C/min => 270C
CapillarySE-521412.Tognolini, Barocelli, et al., 200630. m/0.32 mm/0.15 μm, He; Program: 45C => 1C/min => 100C => 5C/min => 250C (10min)
CapillaryOV-11386.Hafez and Abdel-Salam, 200430. m/0.25 mm/0.25 μm, He; Program: 45 0C (4 min) 3 0C/min -> 75 0C 4 0C/min -> 115 0C 6 0C/min -> 312 0C
CapillarySE-301410.Vinogradov, 2004Program: not specified
CapillaryDB-11383.1Helmig, Revermann, et al., 200330. m/0.32 mm/0.1 μm, He; Program: 40C (2min) => 20C/min => 80C => 3C/min => 145C => 45C/min => 225C (3min)
CapillarySE-541400.Lima, Veiga, et al., 200325. m/0.25 mm/0.25 μm, H2; Program: 110C(2min) => 3C/min => 130C => 8.5C => 290C
CapillaryMethyl Silicone1406.Bakshu and Raju, 2002Program: not specified
CapillaryCP Sil 5 CB1407.Weyerstahl, Marschall, et al., 2000Column length: 25. m; Program: not specified
CapillaryMethyl Silicone1410.Zenkevich, 1996Program: not specified
CapillaryOV-1011436.Shibamoto, 1987Program: not specified

Normal alkane RI, polar column, temperature ramp

View large format table.

Column type Active phase I Reference Comment
CapillaryHP-Innowax1587.Bousaada, Ammar, et al., 200830. m/0.25 mm/0.25 μm, Nitrogen, 50. C @ 1. min, 5. K/min, 280. C @ 1. min
CapillaryDB-Wax1574.Choi, 200660. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillaryBP-201563.Lesueur, Ban, et al., 200650. m/0.22 mm/0.25 μm, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryCarbowax 20M1608.Fernandez, Lizzani-Cuvelier, et al., 200550. m/0.2 mm/0.25 μm, 60. C @ 60. min, 2. K/min; Tend: 250. C
CapillaryDB-Wax1571.Njoroge, Koaze, et al., 2005, 260. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillaryCP-Wax 52CB1582.Rohloff and Bones, 200530. m/0.32 mm/0.25 μm, He, 40. C @ 1. min, 4. K/min; Tend: 220. C
CapillaryCP-Wax 52CB1582.Rohloff and Bones, 200530. m/0.32 mm/0.25 μm, He, 40. C @ 1. min, 4. K/min; Tend: 220. C
CapillaryDB-Wax1572.Choi, 200460. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillaryDB-Wax1572.Choi, 2004, 260. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillarySupelcowax-101556.Gauvin, Ravaomanarivo, et al., 200460. m/0.2 mm/0.2 μm, He, 4. K/min, 200. C @ 40. min; Tstart: 60. C
CapillarySupelcowax-101611.Cabanillas, Lopez, et al., 200330. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 60. C; Tend: 240. C
CapillaryHP-Innowax1600.Stashenko, Jaramillo, et al., 200350. m/0.2 mm/0.2 μm, 50. C @ 5. min, 4. K/min; Tend: 220. C
CapillaryHP-Innowax1599.Stashenko, Jaramillo, et al., 200350. m/0.2 mm/0.2 μm, 50. C @ 5. min, 4. K/min; Tend: 220. C
CapillaryDB-Wax1577.Tu, Thanh, et al., 200260. m/0.25 mm/0.25 μm, N2, 2. K/min; Tstart: 70. C; Tend: 230. C
CapillaryCarbowax1600.Menon, Chacko, et al., 1999N2, 1. K/min, 200. C @ 20. min; Column length: 50. m; Column diameter: 0.2 mm; Tstart: 80. C
CapillaryDB-Wax1582.Ngassoum, Yonkeu, et al., 199960. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-Wax1601.Stashenko, Puertas, et al., 199660. m/0.25 mm/0.25 μm, He, 50. C @ 5. min, 2.5 K/min; Tend: 180. C
CapillaryDB-Wax1565.Binder, Benson, et al., 19904. K/min, 230. C @ 10. min; Column length: 60. m; Column diameter: 0.32 mm; Tstart: 50. C
CapillarySupelcowax-101578.Ramaswami, Briscese, et al., 198850. C @ 2. min, 4. K/min, 240. C @ 10. min; Column length: 30. m
CapillarySupelcowax-101578.Ramaswami, Briscese, et al., 1986He, 50. C @ 2. min, 4. K/min, 240. C @ 10. min; Column length: 30. m
CapillaryCarbowax 20M1600.Shibamoto and Jennings, 19771. K/min; Column length: 100. m; Column diameter: 0.25 mm; Tstart: 70. C; Tend: 170. C
CapillaryCarbowax 20M1600.Shibamoto and Jennings, 19771. K/min; Column length: 100. m; Column diameter: 0.25 mm; Tstart: 70. C; Tend: 170. C

Normal alkane RI, polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryHP Innowax1568.Mancini, Arnold, et al., 200950. m/0.20 mm/0.25 μm, Helium; Program: 40 0C (5 min) 2 0C/min -> 270 0C -> 260 0C (20 min)
CapillaryHP-20M1562.Zellner, Amorim, et al., 200925. m/0.20 mm/0.20 μm, Helium; Program: 30 0C (1 min) 50 0C/min -> 110 0C 1.5 0C/min -> 145 0C 4 0C/min -> 220 0C (10 min)
CapillarySupelcowax-101545.Vichi, Guadayol, et al., 200730. m/0.25 mm/0.25 μm, He; Program: 40C(3min) => 4C/min => 75C => 8C/min => 250C(5min)
CapillaryHP-Innowax1568.Senatore, Apostolides Arnold, et al., 200650. m/0.2 mm/0.2 μm, He; Program: 40C(5min) => 2C/min => 250C (15min) => 10C/min => 270C
CapillarySupelcowax-101542.Vichi, Guadayol, et al., 200630. m/0.25 mm/0.25 μm, He; Program: 40C(3min) => 4C/min => 75C => 8C/min => 260C(5min)
CapillaryHP-Innowax FSC1577.Sezik E., Kocakulak E., et al., 200560. m/0.25 mm/0.25 μm, He; Program: 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
CapillaryHP-Innowax FSC1577.Viljoen, Subramoney, et al., 200560. m/0.25 mm/0.25 μm, He; Program: 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
CapillaryCarbowax 20M1620.Vinogradov, 2004Program: not specified
CapillaryInnowax1577.Tunaher, Kirimer, et al., 200360. m/0.25 mm/0.25 μm, He; Program: 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C (20min)
CapillaryInnowax FSC1577.Tunalier, Kirimer, et al., 200260. m/0.25 mm/0.25 μm; Program: 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
CapillaryCarbowax 20M1600.Chanegriha and Baaliouamer, 1993He; Program: not specified
CapillaryCarbowax 20M1600.Shibamoto, 1987Program: not specified

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Tudor, 1997
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Su, Y.C.; Ho, C.L.; Wang, E.I.C., Analysis of leaf essential oils from the indigenous five conifers of Taiwan, Flavour Fragr. J., 2006, 21, 3, 447-452, https://doi.org/10.1002/ffj.1685 . [all data]

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Su, Y.-C.; Ho, C.-L.; Wang, E.I.-C.; Chang, S.-T., Antifungal activities and chemical compositions of essential oils from leaves of four eucalypts, Taiwan J. For. Sci., 2006, 21, 1, 49-61. [all data]

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Vujisic L.; Vuckovic I.; Tesevic V.; Dokovic D.; Ristic M.S.; Janackovic P.; Milosavljevic S., Comparative examination of the essential oils of Anthemis ruthenica and A-arvensis wild-growing in Serbia, Flavour Fragr. J., 2006, 21, 3, 458-461, https://doi.org/10.1002/ffj.1681 . [all data]

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Boskovic, Z.; Radulovic, N.; Stojanovic, G., Essential oil composition of four Achillea species from the balkans and its chemotaxonomic significance, Chem. Nat. Compd. (Engl. Transl.), 2005, 41, 6, 674-678, https://doi.org/10.1007/s10600-006-0009-6 . [all data]

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Pino, J.A.; Mesa, J.; Muñoz, Y.; Martí, M.P.; Marbot, R., Volatile components from mango (Mangifera indica L.) cultivars, J. Agric. Food Chem., 2005, 53, 6, 2213-2223, https://doi.org/10.1021/jf0402633 . [all data]

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Sati, S.; Mathela, C.S., Essential oil composition of Valeriana hardwickii var. arnottiana from the Himalayas, Flavour Fragr. J., 2005, 20, 3, 299-301, https://doi.org/10.1002/ffj.1415 . [all data]

Aligiannis, Kalpoutzakis, et al., 2004
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Notes

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