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3,3-Dimethylbutane-2-ol

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Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillaryMethyl Silicone100.722.Huber, Kenndler, et al., 1993H2; Column length: 5. m; Phase thickness: 2.65 «mu»m
CapillaryMethyl Silicone120.721.Huber, Kenndler, et al., 1993H2; Column length: 5. m; Phase thickness: 2.65 «mu»m
CapillaryMethyl Silicone80.723.Huber, Kenndler, et al., 1993H2; Column length: 5. m; Phase thickness: 2.65 «mu»m
CapillaryOV-10180.722.3Boneva, 1987N2; Column length: 100. m; Column diameter: 0.27 mm
CapillaryOV-10190.723.4Boneva, 1987N2; Column length: 100. m; Column diameter: 0.27 mm
PackedApiezon L120.717.Bogoslovsky, Anvaer, et al., 1978Celite 545
PackedApiezon L160.728.Bogoslovsky, Anvaer, et al., 1978Celite 545

Kovats' RI, polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillaryPEG-20M110.1114.Huber, Kenndler, et al., 1993Column length: 10. m; Phase thickness: 1.33 «mu»m
CapillaryPEG-20M90.1118.Huber, Kenndler, et al., 1993Column length: 10. m; Phase thickness: 1.33 «mu»m
CapillaryPEG-20M130.1109.1Huber, Kenndler, et al., 1993Column length: 10. m; Phase thickness: 1.33 «mu»m
CapillaryCarbowax 20M80.1112.Boneva, 1987N2; Column length: 50. m; Column diameter: 0.23 mm
CapillaryCarbowax 20M90.1114.Boneva, 1987N2; Column length: 50. m; Column diameter: 0.23 mm

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryVF-5MS740.6Tret'yakov, 200730. m/0.25 mm/0.25 «mu»m, He; Program: Multi-step temperature program; T(initial)=60C; T(final)=270C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryPolydimethyl siloxanes712.Zenkevich, 1998Program: not specified

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Huber, Kenndler, et al., 1993
Huber, J.F.K.; Kenndler, E.; Reich, G.; Hack, W.; Wolf, J., Optimal Selection of Gas Chromatographic Columns for the Analytical Control of Chemical Warfare Agents by Application of Information Theory to Retention Data, Anal. Chem., 1993, 65, 20, 2903-2906, https://doi.org/10.1021/ac00068a031 . [all data]

Boneva, 1987
Boneva, S., Gas Chromatographic Retention Indices for C6 Alkanols on OV-101 and Carbowax 20M Capillary Columns, Chromatographia, 1987, 23, 1, 50-52, https://doi.org/10.1007/BF02310419 . [all data]

Bogoslovsky, Anvaer, et al., 1978
Bogoslovsky, Yu.N.; Anvaer, B.I.; Vigdergauz, M.S., Chromatographic constants in gas chromatography (in Russian), Standards Publ. House, Moscow, 1978, 192. [all data]

Tret'yakov, 2007
Tret'yakov, K.V., Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2007. [all data]

Zenkevich, 1998
Zenkevich, I.G., The Principle of Structural Analogy in the Calculation of Gas Chromatographic Retention Indices using Physico-Chemical Constants of Organic Compounds, Zh. Anal. Khim. (Rus.), 1998, 53, 1, 43-49. [all data]


Notes

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