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2,6,10-Dodecatrien-1-ol, 3,7,11-trimethyl-


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5BPX-5BPX-5BPX-5
Column length (m) 30.50.30.30.30.
Carrier gas HeliumNitrogenHydrogenHydrogenHydrogen
Substrate      
Column diameter (mm) 0.250.200.250.250.25
Phase thickness (mum) 0.250.320.250.250.25
Tstart (C) 50.60.100.60.60.
Tend (C) 220.220.999.999.999.
Heat rate (K/min) 4.5.3.3.3.
Initial hold (min) 2.3.   
Final hold (min) 2.5.   
I 1707.1722.1702.1701.1702.
ReferenceXu, Tang, et al., 2010Shafaghat and Sadeghi, 2009Bieri and Marriott, 2008Bieri and Marriott, 2008Bieri and Marriott, 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BPX-5BPX-5BPX-5HP-5Equity-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HydrogenHydrogenHydrogenNitrogenHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.50.40.
Tend (C) 999.999.999.280.260.
Heat rate (K/min) 3.3.5.5.1.5
Initial hold (min)    1. 
Final hold (min)    1. 
I 1704.1704.1706.1749.1716.
ReferenceBieri and Marriott, 2008Bieri and Marriott, 2008Bieri and Marriott, 2008Bousaada, Ammar, et al., 2008Mondello, Casilli, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5 MSDB-5HP-1HP-101BP-1
Column length (m) 30.30.30.25. 
Carrier gas HeHeHeHeHelium
Substrate      
Column diameter (mm) 0.250.250.250.2 
Phase thickness (mum) 0.250.250.250.2 
Tstart (C) 60.35.60.70.60.
Tend (C) 200.220.240.200.220.
Heat rate (K/min) 2.3.2.3.5.
Initial hold (min) 2.  2. 
Final hold (min) 10.40.20. 6.
I 1713.1690.1699.1664.1699.
ReferenceEdris, Chizzola, et al., 2007El-Ghorab A., El-Massry K.F., et al., 2007Hachicha, Skanji, et al., 2007Jerkovic, Mastelic, et al., 2007Kiran, Bhavani, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase NB-30DB-1DB-5DB-1Methyl Silicone
Column length (m) 30.30.30.30.12.5
Carrier gas He N2HeHe
Substrate      
Column diameter (mm) 0.20.320.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.60.50.50.
Tend (C) 250.230.240.265.270.
Heat rate (K/min) 2.3.4.2.54.
Initial hold (min)  3. 1. 
Final hold (min)  10. 20. 
I 1653.1710.1711.1673.1745.
ReferenceOrav, Raal, et al., 2006Tohar, Mohd, et al., 2006Trilles, Bombarda, et al., 2006Khanavi, Ghasemian, et al., 2005Ricci, Fraternale, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase NB-30NB-30NB-30NB-30NB-30
Column length (m) 50.50.50.50.50.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.20.20.20.20.2
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.50.50.50.50.
Tend (C) 250.250.250.250.250.
Heat rate (K/min) 2.2.2.2.2.
Initial hold (min)      
Final hold (min)      
I 1661.1667.1660.1667.1653.
ReferenceOrav, Stulova, et al., 2004Orav, Stulova, et al., 2004Orav, Stulova, et al., 2004Orav, Stulova, et al., 2004Raal, Arak, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase NB-30DB-1DB-1SPB-5OV-101
Column length (m) 50.30.30.30.50.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.200.250.250.320.2
Phase thickness (mum) 0.250.250.250.250.5
Tstart (C) 50.50.50.40.50.
Tend (C) 250.265.200.220.250.
Heat rate (K/min) 2.2.55.5.2.
Initial hold (min)  1. 1. 
Final hold (min)  20. 20. 
I 1700.1653.1682.1725.1652.
ReferenceRaal, Paaver, et al., 2004Sarkhail, Amin, et al., 2004Fekam Boyom, Ngouana, et al., 2003Ledauphin, Guichard, et al., 2003Orav, Kailas, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5RSL-200OV-101SPB-5
Column length (m) 60.30.30.50.60.
Carrier gas   H2HeHe
Substrate      
Column diameter (mm) 0.250.200.320.20.25
Phase thickness (mum) 0.250.330.25 0.25
Tstart (C) 40.60.40.50.70.
Tend (C) 250.290.280.250.240.
Heat rate (K/min) 5.3.6.2.5.
Initial hold (min) 15. 5. 8.
Final hold (min)  10.5. 20.
I 1740.1747.1699.1654.1680.
ReferenceStashenko, Jaramillo, et al., 2003Benevides, Young, et al., 2002Jirovetz L., Buchbauer G., et al., 2001Orav and Kann, 2001Kim, Kim, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1OV-1OV-101OV-101OV-101
Column length (m) 25.50.50.50.50.
Carrier gas N2He  N2
Substrate      
Column diameter (mm) 0.500.320.250.250.25
Phase thickness (mum) 0.250.25   
Tstart (C) 60.50.80.80.80.
Tend (C) 220.250.200.200.200.
Heat rate (K/min) 5.10.2.2.2.
Initial hold (min)  5.   
Final hold (min) 10.20.   
I 1664.1676.1698.1698.1698.
ReferenceMallavarapu, Kulkarni, et al., 1999Kökdil, Kurucu, et al., 1998Tamura, Yang, et al., 1993Tamura, Yang, et al., 1993Sugisawa, Yamamoto, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Xu, Tang, et al., 2010
Xu, X.; Tang, Z.; Liang, Y., Comparative analysis of plant essential oils by GC-MS coupled with integrated chemometric resolution methods, Anal. Methods, 2010, 2, 4, 359-367, https://doi.org/10.1039/b9ay00213h . [all data]

Shafaghat and Sadeghi, 2009
Shafaghat, A.; Sadeghi, H., Composition and antibacterial activity of essentia; oils from leaf, stem and root of Chrysanthemum parthenium (L.) Bernh. from Iran, Electronic J. of Environ., Agriculture and Food Chem. (EJEAFChe), 2009, 8, 9, 766-771. [all data]

Bieri and Marriott, 2008
Bieri, S.; Marriott, P.J., Dual-injection system with multiply injections for determining sidimentional retention indexes in comprehensive two-dimensional gas chromatography, Anal. Chem., 2008, 80, 3, 760-768, https://doi.org/10.1021/ac071367q . [all data]

Bousaada, Ammar, et al., 2008
Bousaada, O.; Ammar, S.; Saidana, D.; Chriaa, J.; Chraif, I.; Daami, M.; Helal, A.N.; Mighri, Z., Chemical composition and antimicrobial activity of volatile components from capitula and aerial parts of Rhaponticum acaule DC growing wild in Tunisia, Microbiol. Res., 2008, 163, 1, 87-95, https://doi.org/10.1016/j.micres.2007.02.010 . [all data]

Mondello, Casilli, et al., 2008
Mondello, L.; Casilli, A.; Tranchida, Q.; Sciarrone, D.; Dugo, P.; Dugo, G., Analysis of allergens in fragrances using multiple heart-cut multidimentional gas chromatography - mass spectrometry, LC-GC Europe, 2008, 21, 130. [all data]

Edris, Chizzola, et al., 2007
Edris, A.E.; Chizzola, R.; Franz, C., Isolation and characterization of the volatile aroma compounds from the concrete headspace and the absolute of Jasminum sambac (L.) Ait. (Oleaceae) flowers grown in Egypt, Eur. Food Res. Technol., 2007, https://doi.org/10.1007/s00217-007-0623-y . [all data]

El-Ghorab A., El-Massry K.F., et al., 2007
El-Ghorab A.; El-Massry K.F.; Shibamoto T., Chemical composition of the volatile extract and antioxidant activities of the volatile and nonvolatile extracts of Egyptian corn silk (Zea mays L.), J. Agric. Food Chem., 2007, 55, 22, 9124-9127, https://doi.org/10.1021/jf071646e . [all data]

Hachicha, Skanji, et al., 2007
Hachicha, S.F.; Skanji, T.; Barrek, S.; Ghrabi, Z.G.; Zarrouk, H., Composition of the essential oil of Teucrium ramosissimum Desf. (Lamiaceae) from Tunisia, Flavour Fragr. J., 2007, 22, 2, 101-104, https://doi.org/10.1002/ffj.1764 . [all data]

Jerkovic, Mastelic, et al., 2007
Jerkovic, I.; Mastelic, J.; Marijanovic, Z., Bound volatile compounds and essential oil from the fruit of Maclura pomifera (Raf.) Schneid. (osage orange), Flavour Fragr. J., 2007, 22, 1, 84-88, https://doi.org/10.1002/ffj.1763 . [all data]

Kiran, Bhavani, et al., 2006
Kiran, S.R.; Bhavani, K.; Devi, P.S.; Rao, B.R.R.; Reddy, K.J., Composition and alrvicidal activity of leaves and stem essential oils of Chloroxylon swietenia DC against Aedes aegypti and Anopheles stephensi, Biores. Technol., 2006, 97, 18, 2481-2484, https://doi.org/10.1016/j.biortech.2005.10.003 . [all data]

Orav, Raal, et al., 2006
Orav, A.; Raal, A.; Arak, E.; Müürisepp, M.; Kailas, T., Composition of the essential oil of Artemisia absinthium L. of different geographical origin, Proc. Est. Acad. Sci. Chem., 2006, 55, 3, 155-165. [all data]

Tohar, Mohd, et al., 2006
Tohar, N.; Mohd, M.A.; Jantan, I.; Awang, K., A comparative study of the essential oils of the genus Plumeria Linn. from Malaysia, Flavour Fragr. J., 2006, 21, 6, 859-863, https://doi.org/10.1002/ffj.1617 . [all data]

Trilles, Bombarda, et al., 2006
Trilles, B.L.; Bombarda, I.; Bouraïma-Madjebi, S.; Raharivelomanana, P.; Bianchini, J.-P.; Gaydou, E.M., Occurrence of various chemotypes in niaouli [Melaleuca quinquenervia (Cav.) S. T. Blake] essential oil from New Caledonia, Flavour Fragr. J., 2006, 21, 4, 677-682, https://doi.org/10.1002/ffj.1649 . [all data]

Khanavi, Ghasemian, et al., 2005
Khanavi, M.; Ghasemian, L.; Motlagh, E.H.; Hadjiakhoondi, A.; Shafiee, A., Chemical composition of the essential oils of Marrubium parviflorum Fisch. C.A. Mey. and Marrubium vulgare L. from Iran, Flavour Fragr. J., 2005, 20, 3, 324-326, https://doi.org/10.1002/ffj.1425 . [all data]

Ricci, Fraternale, et al., 2005
Ricci, D.; Fraternale, D.; Giamperi, L.; Bucchini, A.; Epifano, F.; Burini, G.; Curini, M., Chemical composition, antimicrobial and antioxidant activity of the essential oil of Teucrium marum (Lamiaceae), J. Ethnopharmacol., 2005, 98, 1-2, 195-200, https://doi.org/10.1016/j.jep.2005.01.022 . [all data]

Orav, Stulova, et al., 2004
Orav, A.; Stulova, I.; Kailas, T.; Müürisepp, M., Effect of storage on the essential oil composition of piper nigrum L. fruits of different ripening states, J. Agric. Food Chem., 2004, 52, 9, 2582-2586, https://doi.org/10.1021/jf030635s . [all data]

Raal, Arak, et al., 2004
Raal, A.; Arak, E.; Orav, A., Chemical composition of coriander seed essential oil and their conformity with EP standards, Agraarteadus, 2004, 15, 4, 234-239. [all data]

Raal, Paaver, et al., 2004
Raal, A.; Paaver, U.; Arak, E.; Orav, A., Content and composition of the essential oil of Thymus serpyllum L. growing wild in Estonia, Medicina (Kaunas), 2004, 40, 8, 795-800. [all data]

Sarkhail, Amin, et al., 2004
Sarkhail, P.; Amin, G.; Shafiee, A., Composition of the essential oil of Phlomis persica Boiss and Phlomis chorassanica Bunge from Iran, Flavour Fragr. J., 2004, 19, 6, 538-540, https://doi.org/10.1002/ffj.1338 . [all data]

Fekam Boyom, Ngouana, et al., 2003
Fekam Boyom, F.; Ngouana, V.; Amvam Zollo, P.H.; Menut, C.; Bessiere, J.M.; Gut, J.; Rosenthal, P.J., Composition and anti-plasmodial activities of essential oils from some Cameroonian medicinal plants, Phytochemistry, 2003, 64, 7, 1269-1275, https://doi.org/10.1016/j.phytochem.2003.08.004 . [all data]

Ledauphin, Guichard, et al., 2003
Ledauphin, J.; Guichard, H.; Saint-Clair, J.-F.; Picoche, B.; Barillier, D., Chemical and sensorial aroma characterization of freshly distilled calvados. 2. Identification of volatile compounds and key odorants, J. Agric. Food Chem., 2003, 51, 2, 433-442, https://doi.org/10.1021/jf020373e . [all data]

Orav, Kailas, et al., 2003
Orav, A.; Kailas, T.; Jegorova, A., Composition of the essential oil of dill, celery, and parsley from Estonia, Proc. Est. Acad. Sci. Chem., 2003, 52, 4, 147-154. [all data]

Stashenko, Jaramillo, et al., 2003
Stashenko, E.E.; Jaramillo, B.E.; Martínez, J.R., Comparación de la composición química y de la actividad antioxidante in vitro de los metabolitos secundarios volátiles de plantas de la familia verbenaceae, Rev. Acad. Colomb. Cienc. Exactas Fis. Nat., 2003, 27, 105, 579-597. [all data]

Benevides, Young, et al., 2002
Benevides, P.J.C.; Young, M.C.M.; Bolzani, V.S., Composição química e atevidade antifúngica do óleo essencial de psychotria spectabillis L. (Rubiaceae), 2002, retrieved from http://www.sbq.org.br/ranteriores/23/resumos/0131. [all data]

Jirovetz L., Buchbauer G., et al., 2001
Jirovetz L.; Buchbauer G.; Shafi P.M.; Rosamma M.K.; Geissler M., Analysis of the composition and aroma of the essential leaf oil of Syzygium travancoricum from South India by GC-FID, GC-MS, and olfactometry. Seasonal changes of composition, Chromatographia Sup., 2001, 53, S1, s372-s374, https://doi.org/10.1007/BF02490359 . [all data]

Orav and Kann, 2001
Orav, A.; Kann, J., Determination of peppermint and orange aroma compounds in food and beverages, Proc. Est. Acad. Sci. Chem., 2001, 50, 4, 217-225. [all data]

Kim, Kim, et al., 2000
Kim, H.-J.; Kim, K.; Kim, N.-S.; Lee, D.-S., Determination of floral fragrances of Rosa hybrida using solid-phase trapping-solvent extraction and gas chromatography-mass spectrometry, J. Chromatogr. A, 2000, 902, 2, 389-404, https://doi.org/10.1016/S0021-9673(00)00863-3 . [all data]

Mallavarapu, Kulkarni, et al., 1999
Mallavarapu, G.R.; Kulkarni, R.N.; Baskaran, K.; Rao, L.; Ramesh, S., Influence of plant growth stage on the essential oil content and composition in Davana (Artemisia pallens Wall.), J. Agric. Food Chem., 1999, 47, 1, 254-258, https://doi.org/10.1021/jf980624c . [all data]

Kökdil, Kurucu, et al., 1998
Kökdil, G.; Kurucu, S.; Yildiz, A., Essential oil composition of Nepeta nuda L. ssp. nuda, Flavour Fragr. J., 1998, 13, 4, 233-234, https://doi.org/10.1002/(SICI)1099-1026(1998070)13:4<233::AID-FFJ730>3.0.CO;2-7 . [all data]

Tamura, Yang, et al., 1993
Tamura, H.; Yang, R.-H.; Sugisawa, H., Aroma profiles of peel oils of acid citrus, ACS Sym. Ser., 1993, 525, 121-136. [all data]

Sugisawa, Yamamoto, et al., 1989
Sugisawa, H.; Yamamoto, M.; Tamura, H.; Takagi, N., The comparison of volatile components in peel oil from four species of navel orange, Nippon Shokuhin Kogio Gakkaishi, 1989, 36, 6, 455-462, https://doi.org/10.3136/nskkk1962.36.6_455 . [all data]


Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References