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Resorcinol, 2TMS derivative


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-51389.Jaroszynska and Ligor, 200530. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 50. C; Tend: 320. C
CapillaryDB-51389.Jaroszynska and Ligor, 200530. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 50. C; Tend: 320. C
CapillaryDB-51390.Jaroszynska and Ligor, 200530. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 50. C; Tend: 320. C
CapillaryPE-5ht1386.Jaroszynska and Ligor, 200530. m/0.25 mm/0.1 «mu»m, He, 3. K/min; Tstart: 50. C; Tend: 320. C
CapillaryPE-5ht1387.Jaroszynska and Ligor, 200530. m/0.25 mm/0.1 «mu»m, He, 3. K/min; Tstart: 50. C; Tend: 320. C
CapillaryPE-5ht1389.Jaroszynska and Ligor, 200530. m/0.25 mm/0.1 «mu»m, He, 3. K/min; Tstart: 50. C; Tend: 320. C
CapillaryPE-5ms1378.Jaroszynska and Ligor, 200530. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 50. C; Tend: 320. C
CapillaryDB-51389.Jaroszynska, 200330. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 50. C; Tend: 240. C
CapillaryDB-51390.Jaroszynska, 200330. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 50. C; Tend: 240. C
CapillaryDB-51388.Jaroszynska, 200330. m/0.25 mm/0.25 «mu»m, He, 7. K/min; Tstart: 50. C; Tend: 240. C
CapillaryDB-51390.Jaroszynska, 200330. m/0.25 mm/0.25 «mu»m, He, 7. K/min; Tstart: 50. C; Tend: 240. C
PackedOV-11378.Mattsson and Petersson, 1977N2, Supelcoport, 4. K/min; Column length: 2. m; Tstart: 80. C; Tend: 240. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryVF-5MS1376.5Tret'yakov, 200830. m/0.25 mm/0.25 «mu»m, He; Program: Multi-step temperature program; T(initial)=60C; T(final)=270C

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-51390.Isidorov, Kotowska, et al., 200530. m/0.25 mm/0.25 «mu»m, He, 5. K/min; Tstart: 50. C; Tend: 300. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillarySE-301378.Zimmermann, Lauterbach, et al., 1985Program: not specified

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Jaroszynska and Ligor, 2005
Jaroszynska, J.; Ligor, T., The identification of phenolic compounds by a gas chromatographic method on three capillary columns with the same non-polar stationary phase, Anal. Chim. Acta., 2005, 539, 1-2, 11-15, https://doi.org/10.1016/j.aca.2005.03.024 . [all data]

Jaroszynska, 2003
Jaroszynska, J., Isolation of free phenolic compounds from arboreal leaves by use of the Florisil/C18 system, Anal. Bioanal. Chem., 2003, 377, 4, 702-708, https://doi.org/10.1007/s00216-003-2155-z . [all data]

Mattsson and Petersson, 1977
Mattsson, M.; Petersson, G., Reference GLC Data for the Analysis of Phenolic Compounds as Trimethylsilyl Derivatives, J. Chromatogr. Sci., 1977, 15, 12, 546-554, https://doi.org/10.1093/chromsci/15.12.546 . [all data]

Tret'yakov, 2008
Tret'yakov, K.V., Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2008. [all data]

Isidorov, Kotowska, et al., 2005
Isidorov, V.A.; Kotowska, U.; Vinogorova, V.T., GC Identification of organic compounds based on partition coefficients of their TMS derivatives in a hexane-acetonitrile system and retention indices, Anal. Sci., 2005, 21, 12, 1483-1489, https://doi.org/10.2116/analsci.21.1483 . [all data]

Zimmermann, Lauterbach, et al., 1985
Zimmermann, V.; Lauterbach, M.; Jaeger, G., Analytical characterization phenolic compounds obtained from phenosolvan-extracts by use of gas-chromatography with capillary columns, Chem. Tech. (Leipzig), 1985, 37, 11, 476-478. [all data]


Notes

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