3-Cyclopentene-1-acetaldehyde, 2,2,3-trimethyl-, (R)-
- Formula: C10H16O
- Molecular weight: 152.2334
- IUPAC Standard InChIKey: OGCGGWYLHSJRFY-UHFFFAOYSA-N
- CAS Registry Number: 4501-58-0
- Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript. - Species with the same structure:
- Other names: 3-Cyclopentene-1-acetaldehyde, 2,2,3-trimethyl-; α-Campholenal; α-Campholenic aldehyde; 2,2,3-Trimethyl-3-cyclopentacetaldehyde; (2,2,3-Trimethyl-3-cyclopenten-1-yl)acetaldehyde; (R)-α-Campholene aldehyde; (R)-2-(2,2,3-Trimethylcyclopent-3-en-1-yl)acetaldehyde; α-Compholene aldehyde; 2,2,3-Trimethyl-3-cyclopentacetaldehyde, (R)-; α-Campholen aldehyde; (R)-α-Campholenic aldehyde; (R)-2,2,3-Trimethylcyclopent-3-ene-1-acetaldehyde; 3-Cyclopentene-1-acetaldehyde, 2,2,3-trimethyl-, (1R)-; α-Campholene aldehyde; Campholenal; γ-Campholene aldehyde; α-Camphenal; Campholenic aldehyde; α-Camphene aldehyde; campholene aldehyde; α-camphonellal; Camphonealdehyde
- Information on this page:
- Other data available:
- Options:
Normal alkane RI, non-polar column, custom temperature program
Go To: Top, References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-1-MS | DB-5 | HP-5 | SLB-5 MS | SLB-5 MS |
Column length (m) | 60. | 30. | 30. | 30. | 30. |
Carrier gas | Helium | Helium | Helium | Helium | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.32 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | |
Program | not specified | 50 0C m6 0C/min -> 140 0C 5 0C/min -> 160 0C (1 min) 10 0C/min -> 200 0C | not specified | 50 0C 3 0C/min -> 250 0C (1 min) 10 0C/min -> 300 0C (5 min) | not specified |
I | 1103. | 1133. | 1126. | 1126. | 1122. |
Reference | Takeoka, Hobbs, et al., 2010 | Courtois, Paine, et al., 2009 | Riahi, Pourbasheer, et al., 2009 | Costa, De Fina, et al., 2008 | Costa, De Fina, et al., 2008 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | SPB-5 | SPB-5 | SLB-5 MS | HP-5MS | DB-1 |
Column length (m) | 30. | 30. | 30. | ||
Carrier gas | Helium | He | H2 | ||
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | ||
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | ||
Program | not specified | not specified | not specified | 40C(10min) => 3C/min => 200C => 2C/min => 220C | 45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min) |
I | 1134. | 1135. | 1126. | 1125. | 1088. |
Reference | Kilani, Ledauphin, et al., 2008 | Kilani, Ledauphin, et al., 2008 | Lo Presti, Sciarrone, et al., 2008 | Cole, Haber, et al., 2007 | Kamatou, Viljoen, et al., 2007 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | CP Sil 8 CB | HP-5 | BPX-5 | HP-5 MS | HP-5MS |
Column length (m) | 30. | 30. | 30. | 30. | 30. |
Carrier gas | He | Helium | He | Helium | He |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | ||
Program | 50C(3min) => 3C/min => 100C => 2.7C/min => 140C => 2.4C/min => 180C => 6C/min => 250C | not specified | 50C => 3C/min => 150C(10min) => 10C/min => 250C | 40 0C (10 min) 3 oC/min -> 200 0C 2 0C/min -> 220 0C | 40C(10min) => 3C/min => 200C => 2C/min => 220C |
I | 1093. | 1126. | 1134. | 1125. | 1130. |
Reference | Meekijjaroenroj, Bessière, et al., 2007 | Ristic, Krivokuca-Dokic, et al., 2007 | Salamci, Kordali, et al., 2007 | Setzer, Stokes, et al., 2007 | Takaku, Haber, et al., 2007 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | BPX-5 | BPX-5 | HP-5MS | SE-52 | DB-5MS |
Column length (m) | 30. | 30. | 30. | 30. | 30. |
Carrier gas | He | He | He | He | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.32 | 0.32 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.15 | 0.25 |
Program | 50C => 3C/min => 150C(10min) => 10C/min => 250C | 50C => 3C/min => 150C (10min) => 10C/min => 250C | 60C(1min) => 1.5C => 185C => 9C/min => 275C (2min) | 45C => 1C/min => 100C => 5C/min => 250C (10min) | 70C(2min) => 10C/min => 150C(15min) => 5C/min => 240C |
I | 1134. | 1133. | 1127. | 1126. | 1122. |
Reference | Baris, Güllüce, et al., 2006 | Ozer H., Kilic H., et al., 2006 | Singh G., Maurya S., et al., 2006 | Tognolini, Barocelli, et al., 2006 | Bagci and Baser, 2005 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-5MS | CP Sil 8 CB | DB-5 | BPX-5 | CP Sil 8 CB |
Column length (m) | 30. | 50. | 30. | 30. | 50. |
Carrier gas | He | He | He | He | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.32 | 0.25 | 0.32 | 0.32 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.5 | 0.25 |
Program | 70C(2min) => 10C/min => 150C(15min) => 5C/min => 240C | 50C(5min) => 2C/min => 90C => 15C/min => 240C(4min) | 40C(1min) => 9C/min => 130C => 2C/min => 230C | 60C(1min) => 3.5C/min => 180C => 20C/min => 280C(2min) | 50C(5min) => 2C/min => 90C => 15C/min => 240C(4min) |
I | 1088. | 1126. | 1119. | 1126. | 1126. |
Reference | Bagci and Baser, 2005 | Butkienë, Nivinskienë, et al., 2005 | Hamm, Bleton, et al., 2005 | Koutsoudaki, Krsek, et al., 2005 | Butkienë, Nivinskienë, et al., 2004 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | Methyl Silicone | OV-1 | DB-5 | DB-5 | DB-1 |
Column length (m) | 30. | 30. | 30. | 30. | |
Carrier gas | He | He | He | He | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | |
Program | not specified | 45 0C (4 min) 3 0C/min -> 75 0C 4 0C/min -> 115 0C 6 0C/min -> 312 0C | 40C(1min) => 9C/min => 130C => 2C/min => 230C | 60C(4min) => 6C/min => 240 => 10C/min => 280C | 45C => 3C/min => 175C => 15C/min => 300C (10min) |
I | 1121. | 1094. | 1119. | 1125. | 1088. |
Reference | Couladis, Özcan, et al., 2004 | Hafez and Abdel-Salam, 2004 | Hamm, Bleton, et al., 2004 | Letchamo, Ward, et al., 2004 | Miguel, Simões, et al., 2004 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-5 | SE-30 | AT-5 | HP-1 | HP-5 |
Column length (m) | 60. | 30. | 30. | ||
Carrier gas | He | He | |||
Substrate | |||||
Column diameter (mm) | 0.25 | 0.32 | 0.25 | ||
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | ||
Program | not specified | not specified | 50 0C 5 0C/min -> 135 0C (1 min) 5 0C/min -> 225 0C (5 min) 5 0C/min -> 260 0C | 40C(3min) => 5C/min => 180C => 15C/min => 240C(15min) | not specified |
I | 1125. | 1115. | 1125. | 1132. | 1120. |
Reference | Vilaseca, Guy, et al., 2004 | Vinogradov, 2004 | Usai, Atzei, et al., 2003 | Nogueira and Romano, 2002 | Aparicio, Romero, et al., 2001 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-1 | HP-5 | DB-1 | CP Sil 5 CB | CP Sil 5 CB |
Column length (m) | 30. | 30. | 30. | 25. | 25. |
Carrier gas | He | He | He | He | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | ||
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.39 | 0.39 |
Program | 45 0C 3 K/min -> 175 0C 15 K/min -> 300 0C (10 min) | 50 0C 3 K/min -> 200 0C 8 K/min -> 280 0C | 45C => 3C/min => 175C => 15C/min => 240C (10min) | not specified | not specified |
I | 1088. | 1121. | 1088. | 1099. | 1075. |
Reference | Figueiredo, Miguel, et al., 2001 | Usubillaga, Aparicio, et al., 2001 | Baratta, Dorman, et al., 1998 | Weyerstahl, Marschall, et al., 1998 | Weyerstahl, Marschall, et al., 1998 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | CP Sil 5 CB | DB-1 | CP Sil 5 CB | Polydimethyl siloxanes | DB-1 |
Column length (m) | 25. | 30. | 30. | 30. | |
Carrier gas | N2 | He | N2 | H2 | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | ||
Phase thickness (μm) | 0.39 | 0.25 | 0.25 | ||
Program | not specified | 45C => 3C/min => 175C => 15C/min => 280C | not specified | not specified | 45 0C 3 0C/min -> 175 0C 15 0C/min -> 240 0C (10 min) |
I | 1106. | 1088. | 1108. | 1115. | 1088. |
Reference | Weyerstahl, Marschall, et al., 1998, 2 | Gaspar, Palma, et al., 1997 | Weyerstahl, Marschall, et al., 1997 | Zenkevich, 1997 | Barroso, Figueiredo, et al., 1996 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
References
Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
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Hafez, S.S.; Abdel-Salam, H.A.,
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Composition and variability of the essential oil of Sardinian Thymus herba-barona Loisel,
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Nogueira and Romano, 2002
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Essential oils from micropropagated plants of Lavandula viridis,
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Aparicio, Romero, et al., 2001
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Composition of the essential oil of four species of Ruilopezia from the Venezuelan Andes,
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Usubillaga, Aparicio, et al., 2001
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Volatile constituents from the leaves of four Libanothamus species from the Venezuelan Andes,
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Weyerstahl, Marschall, et al., 1998
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Constituents of commercial Labdanum oil,
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Weyerstahl, Marschall, et al., 1998, 2
Weyerstahl, P.; Marschall, H.; Thefeld, K.; Subba, G.C.,
Constituents of the essential oil from the rhizomes of Hedychium gardnerianum Roscoe,
Flavour Fragr. J., 1998, 13, 6, 377-388, https://doi.org/10.1002/(SICI)1099-1026(199811/12)13:6<377::AID-FFJ755>3.0.CO;2-F
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Gaspar, Palma, et al., 1997
Gaspar, H.; Palma, F.M.S.B.; de la Torre, M.C.; Rodríguez, B.; Barroso, J.G.; Figueiredo, A.C.,
Composition of the essential oil of Teucrium haenseleri Boiss.,
Flavour Fragr. J., 1997, 12, 5, 355-357, https://doi.org/10.1002/(SICI)1099-1026(199709/10)12:5<355::AID-FFJ656>3.0.CO;2-B
. [all data]
Weyerstahl, Marschall, et al., 1997
Weyerstahl, P.; Marschall, H.; Seelmann, I.; Rustaiyan, A.,
Constituents of the essential oil of Achillea eriophora DC,
Flavour Fragr. J., 1997, 12, 2, 71-78, https://doi.org/10.1002/(SICI)1099-1026(199703)12:2<71::AID-FFJ620>3.0.CO;2-E
. [all data]
Zenkevich, 1997
Zenkevich, I.G.,
Analytical Parameters of Components of Essential Oils for their Chromatographic and Chromato-Spectral Identificaiton. Oxsigenated derivatives of Mono- and Sesquiterpene Hydrocarbons,
Rastit, Resursy (Rus.), 1997, 33, 1, 16-28. [all data]
Barroso, Figueiredo, et al., 1996
Barroso, J.G.; Figueiredo, A.C.; Pedro, L.G.; Antunes, T.; Sevinate-Pinto, I.; Fontinha, S.S.; Scheffer, J.J.C.,
Composition of the essential oil of teucrium heterophyllum L'Her. Grown on Madiera,
Flavour Fragr. J., 1996, 11, 2, 129-132, https://doi.org/10.1002/(SICI)1099-1026(199603)11:2<129::AID-FFJ550>3.0.CO;2-Z
. [all data]
Notes
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