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Anethole

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Normal alkane RI, polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-FFAPNB-20MInnowaxDB-WaxDB-Wax
Column length (m) 30.30.50.30.60.
Carrier gas HeHeHeN2H2
Substrate      
Column diameter (mm) 0.320.20.20.250.32
Phase thickness (mum) 0.250.250.50.250.25
Tstart (C) 40.50.60.60.40.
Tend (C) 230.250.250.250.230.
Heat rate (K/min) 6.2.2.5.4.
Initial hold (min) 1.   5.
Final hold (min)   60.10.25.
I 1830.1834.1798.1802.1820.
ReferenceZeller and Rychlik, 2007Orav, Raal, et al., 2006Bendimerad and Bendiab, 2005Fakhari A.R., Sonboli A., et al., 2005Dregus and Engel, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxTC-WaxSW-10PEG-20MCW 20M
Column length (m) 30.60.50.50.25.
Carrier gas He HeHeHydrogen
Substrate      
Column diameter (mm) 0.250.250.200.20.32
Phase thickness (mum) 0.25 0.25 0.25
Tstart (C) 50.80.50.70.50.
Tend (C) 230.240.250.220.220.
Heat rate (K/min) 3.3.2.2.3.
Initial hold (min) 2.   1.
Final hold (min) 20.   10.
I 1818.1829.1820.1819.1805.
ReferenceLin, Cai, et al., 2003Miyazawa, Yamafuji, et al., 2003Raal, Arak, et al., 2003Orav and Kann, 2001Bicchi, Binello, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CW 20MCW 20MCW 20MCW 20MHP Innowax FSP
Column length (m) 25.25.25.25.60.
Carrier gas HydrogenHydrogenHydrogenHydrogenHe
Substrate      
Column diameter (mm) 0.320.320.320.320.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.50.50.50.60.
Tend (C) 220.220.220.220.220.
Heat rate (K/min) 3.3.3.3. 
Initial hold (min) 1.1.1.1.10.
Final hold (min) 10.10.10.10.10.
I 1807.1807.1807.1809.1845.
ReferenceBicchi, Binello, et al., 1999Bicchi, Binello, et al., 1999Bicchi, Binello, et al., 1999Bicchi, Binello, et al., 1999Kaya, Baser, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CarbowaxSupelcowax-10DB-WaxTC-WaxDB-Wax
Column length (m) 50.30.60.60.60.
Carrier gas N2HeHe He
Substrate      
Column diameter (mm) 0.20.250.320.250.25
Phase thickness (mum)   0.50 0.25
Tstart (C) 80.60.50.80.50.
Tend (C) 200.240.250.240.180.
Heat rate (K/min) 1.4.8.3.2.5
Initial hold (min)   1.5.5.
Final hold (min) 20. 6.  
I 1809.1829.1810.1839.1808.
ReferenceMenon, Chacko, et al., 1999Lamarque, Maestri, et al., 1998Sagrero-Nieves and Bartley, 1996Shuichi, Masazumi, et al., 1996Stashenko, Torres, et al., 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryPacked
Active phase Carbowax 20MDB-WaxCarbowax 20M
Column length (m) 80.30.2.
Carrier gas   Hydrogen
Substrate   Gas-Chrom Z (80-100 mesh)
Column diameter (mm) 0.20.32 
Phase thickness (mum)    
Tstart (C) 70.70.65.
Tend (C) 170.200.220.
Heat rate (K/min) 2.4.4.
Initial hold (min)  2. 
Final hold (min)    
I 1809.1845.1835.
ReferenceEgolf and Jurs, 1993Wyllie, Brophy, et al., 1990Stancher and Pertoldi, 1967
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Zeller and Rychlik, 2007
Zeller, A.; Rychlik, M., Impact of estragole and other odorants on the flavour of anise and tarragon, Flavour Fragr. J., 2007, 22, 2, 105-113, https://doi.org/10.1002/ffj.1765 . [all data]

Orav, Raal, et al., 2006
Orav, A.; Raal, A.; Arak, E.; Müürisepp, M.; Kailas, T., Composition of the essential oil of Artemisia absinthium L. of different geographical origin, Proc. Est. Acad. Sci. Chem., 2006, 55, 3, 155-165. [all data]

Bendimerad and Bendiab, 2005
Bendimerad, N.; Bendiab, S.A.T., Composition and antibacterial activity of Pseudocytisus integrifolius (Salisb.) essential oil from Algeria, J. Agric. Food Chem., 2005, 53, 8, 2947-2952, https://doi.org/10.1021/jf047937u . [all data]

Fakhari A.R., Sonboli A., et al., 2005
Fakhari A.R.; Sonboli A.; Heydari R., Composition of the essential oil of Rhabdosciadium strausii from Iran, Chem. Nat. Compd. (Engl. Transl.), 2005, 41, 4, 413-414, https://doi.org/10.1007/s10600-005-0164-1 . [all data]

Dregus and Engel, 2003
Dregus, M.; Engel, K.-H., Volatile constituents of uncooked Rhubarb (Rheum rhabarbarum L.) stalks, J. Agric. Food Chem., 2003, 51, 22, 6530-6536, https://doi.org/10.1021/jf030399l . [all data]

Lin, Cai, et al., 2003
Lin, P.; Cai, J.; Li, J.; Sang, W.; Su, Q., Constituents of the essential oil of Hemerocallis flava day lily, Flavour Fragr. J., 2003, 18, 6, 539-541, https://doi.org/10.1002/ffj.1264 . [all data]

Miyazawa, Yamafuji, et al., 2003
Miyazawa, M.; Yamafuji, C.; Kurose, K.; Ishikawa, Y., Volatile components of the rhizomes of Cirsium japonicum DC, Flavour Fragr. J., 2003, 18, 1, 15-17, https://doi.org/10.1002/ffj.1135 . [all data]

Raal, Arak, et al., 2003
Raal, A.; Arak, E.; Orav, A.; Ivask, K., Comparison of essential oil content of Matricaria recutita L. from different origins, Ars Pharm., 2003, 44, 2, 159-165, retrieved from http://www.ugr.es/~ars/abstract/44-159-03.pdf. [all data]

Orav and Kann, 2001
Orav, A.; Kann, J., Determination of peppermint and orange aroma compounds in food and beverages, Proc. Est. Acad. Sci. Chem., 2001, 50, 4, 217-225. [all data]

Bicchi, Binello, et al., 1999
Bicchi, C.; Binello, A.; D'Amato, A.; Rubiolo, P., Reliability of Van den Dool retention indices in the analysis of essential oils, J. Chromatogr. Sci., 1999, 37, 8, 288-294, https://doi.org/10.1093/chromsci/37.8.288 . [all data]

Kaya, Baser, et al., 1999
Kaya, A.; Baser, K.H.C.; Koca, F., Essential oils of Acinos troodi (Post) Leblebici subsp. vardaranus Leblebici and subsp. grandiflorus Hartvig Strid, Flavour Fragr. J., 1999, 14, 1, 50-54, https://doi.org/10.1002/(SICI)1099-1026(199901/02)14:1<50::AID-FFJ783>3.0.CO;2-7 . [all data]

Menon, Chacko, et al., 1999
Menon, A.N.; Chacko, S.; Narayanan, C.S., Free and glycosidically bound volatiles of cardamom (Eletteria cardamomum Maton var. miniscula Burkill), Flavour Fragr. J., 1999, 14, 1, 65-68, https://doi.org/10.1002/(SICI)1099-1026(199901/02)14:1<65::AID-FFJ789>3.0.CO;2-A . [all data]

Lamarque, Maestri, et al., 1998
Lamarque, A.L.; Maestri, D.M.; Zygadlo, J.A.; Grosso, N.R., Volatile constituents from flowers of Acacia caven (Mol.) Mol. var. caven, Acacia aroma Gill. ex Hook., Erythrina crista-galli L. and Calliandra tweedii Benth., Flavour Fragr. J., 1998, 13, 4, 266-268, https://doi.org/10.1002/(SICI)1099-1026(1998070)13:4<266::AID-FFJ739>3.0.CO;2-5 . [all data]

Sagrero-Nieves and Bartley, 1996
Sagrero-Nieves, L.; Bartley, J.P., Volatile components from the leaves of heterotheca inuloides Cass., Flavour Fragr. J., 1996, 11, 1, 49-51, https://doi.org/10.1002/(SICI)1099-1026(199601)11:1<49::AID-FFJ538>3.0.CO;2-J . [all data]

Shuichi, Masazumi, et al., 1996
Shuichi, H.; Masazumi, N.; Hiromu, K.; Kiyoshi, F., Comparison of volatile compounds berween the crude drugs, Onji-tsutsu and Onji-niki, Nippon nogei kagaku kaishi, 1996, 70, 2, 151-160. [all data]

Stashenko, Torres, et al., 1995
Stashenko, E.E.; Torres, W.; Morales, J.R.M., A study of the compositional variation of the essential oil of ylang-ylang (Cananga odorata Hook Fil. et Thomson, forma genuina) during flower development, J. Hi. Res. Chromatogr., 1995, 18, 2, 101-104, https://doi.org/10.1002/jhrc.1240180206 . [all data]

Egolf and Jurs, 1993
Egolf, L.M.; Jurs, P.C., Quantitative structure-retention and structure-odor intensity relationships for a diverse group of odor-active compounds, Anal. Chem., 1993, 65, 21, 3119-3126, https://doi.org/10.1021/ac00069a027 . [all data]

Wyllie, Brophy, et al., 1990
Wyllie, S.G.; Brophy, J.J.; Sarafis, V.; Hobbs, M., Volatile Components of the Fruit of Pistacia Lentiscus, J. Food. Sci., 1990, 55, 5, 1325-1326, https://doi.org/10.1111/j.1365-2621.1990.tb03926.x . [all data]

Stancher and Pertoldi, 1967
Stancher, B.; Pertoldi, M.G., Characterization of commercial materials used in synthetic essential oil production. Identification and gas-chromatographic determination of impurities, Rassegna chimica, 1967, 19, 3, 99-109. [all data]


Notes

Go To: Top, Normal alkane RI, polar column, temperature ramp, References