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1,6,10-Dodecatrien-3-ol, 3,7,11-trimethyl-, (E)-


Van Den Dool and Kratz RI, polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-20HP-InnowaxHP-InnowaxZB-WaxBP-20
Column length (m) 50.30.30.30.50.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.220.250.250.320.22
Phase thickness (mum) 0.250.250.50.250.25
Tstart (C) 60.60.60.40.60.
Tend (C) 220.280.260.250.220.
Heat rate (K/min) 2.3.3.5.2.
Initial hold (min)    2. 
Final hold (min) 20.  5.20.
I 2041.2051.2053.2033.2043.
ReferenceBoti, Koukoua, et al., 2007Kundakovic, Fokialakis, et al., 2007Saroglou, Marin, et al., 2007Wu, Zorn, et al., 2007Blanc, Bradesi, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-20RTX-WaxHP-WaxBP-20DB-Wax
Column length (m) 50.60.30.50.30.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.220.220.250.220.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.50.
Tend (C) 220.230.220.220.220.
Heat rate (K/min) 2.2.5.2.4.
Initial hold (min)   10. 4.
Final hold (min) 20.45. 20.20.
I 2033.2029.2006.2038.2017.
ReferenceBoti, Bighelli, et al., 2006Cavalli, Tomi, et al., 2006Flamini, Tebano, et al., 2006Gonny, Cavaleiro, et al., 2006Osorio, Alarcon, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-WaxPEG-20MBP-20DB-WaxDB-Wax
Column length (m) 60.25.50.60.30.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.220.250.220.250.25
Phase thickness (mum) 0.250.30.250.250.25
Tstart (C) 60.50.60.70.40.
Tend (C) 230.220.220.230.250.
Heat rate (K/min) 2.3.2.2.3.
Initial hold (min)  1. 2. 
Final hold (min) 35.5.20.20.20.
I 1991.2046.2039.2054.2028.
ReferencePaolini J., Desjobert J.M., et al., 2006Rubiolo P., Matteodo M., et al., 2006Boti J.B., Koukoua G., et al., 2005Choi, 2005Fanciullino, Gancel, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-20DB-WaxRTX-WaxDB-WaxHP-Wax
Column length (m) 50.30.60.60.30.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.220.250.220.320.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.40.60.32.60.
Tend (C) 220.250.230.220.220.
Heat rate (K/min) 2.3.2.3.5.
Initial hold (min)     10.
Final hold (min) 20.20.35.  
I 2037.2026.2013.2045.2045.
ReferenceFerrari, Tomi, et al., 2005Gancel, Ollitrault, et al., 2005Paolini, Costa, et al., 2005Brophy, Goldsack, et al., 2004Flamini, Luigi Cioni, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-20DB-WaxHP-WaxHP-WaxRTX-Wax
Column length (m) 50.30.30.30.60.
Carrier gas HeHeN2N2He
Substrate      
Column diameter (mm) 0.220.250.250.250.22
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.40.60.60.60.
Tend (C) 220.200.220.220.230.
Heat rate (K/min) 2.4.5.5.2.
Initial hold (min)  5.10.10. 
Final hold (min) 20.20.  45.
I 2032.2016.2045.1997.2031.
ReferenceTam, Thuam, et al., 2004Yu, Kim, et al., 2004Bader, Caponi, et al., 2003Campeol, Flamini, et al., 2003Cavalli, Tomi, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxDB-WaxHP-InnowaxDB-Wax
Column length (m) 60.60.60.30.60.
Carrier gas N2H2N2HeN2
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (mum) 0.250.250.250.50.25
Tstart (C) 70.40.40.60.70.
Tend (C) 230.245.210.260.230.
Heat rate (K/min) 2.1.52.3.2.
Initial hold (min) 2.    
Final hold (min) 20.20.40. 20.
I 2054.2026.2027.2053.2040.
ReferenceChoi, 2003Gancel, Ollitrault, et al., 2003Mau, Ko, et al., 2003Skaltsa, Demetzos, et al., 2003Choi, Kim. M.-S.L., et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase InnowaxRTX-WaxAT-WaxBP-20AT-Wax
Column length (m) 30.30.60.50.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.320.220.32
Phase thickness (mum) 0.50.250.250.250.25
Tstart (C) 60.45.65.60.65.
Tend (C) 260.250.250.220.250.
Heat rate (K/min) 3.3.2.2.2.
Initial hold (min)  6.10. 10.
Final hold (min) 10.10.60. 60.
I 1998.2020.2015.2031.2008.
ReferenceCouladis, Chinou, et al., 2002Mondello, Zappia, et al., 2002Pino, Marbot, et al., 2002Lota, Serra, et al., 2001Pino and Marbot, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase AT-WaxDB-WaxCP-Wax 52CBDB-WaxBP-20
Column length (m) 60.60.25.60.50.
Carrier gas HeHe N2He
Substrate      
Column diameter (mm) 0.320.530.250.250.22
Phase thickness (mum) 0.251.00.150.250.25
Tstart (C) 65.50.40.70.60.
Tend (C) 250.220.220.230.230.
Heat rate (K/min) 2.3.3.2.2.
Initial hold (min) 10. 5.2. 
Final hold (min) 60.  20.35.
I 2015.2049.2064.2050.2031.
ReferencePino, Marbot, et al., 2001Brophy, Goldsack, et al., 2000Chagonda, Makanda, et al., 2000Choi and Sawamura, 2000Lota, de Rocca Serra, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxBP-20BP-20Innowax
Column length (m) 60.60.50.50.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.530.530.220.220.25
Phase thickness (mum)   0.250.250.25
Tstart (C) 50.50.60.60.50.
Tend (C) 220.220.230.230.180.
Heat rate (K/min) 3.3.2.2.2.5
Initial hold (min)     5.
Final hold (min)   35.35. 
I 2049.2049.2031.2031.2008.
ReferenceBrophy, Goldsack, et al., 1999Brophy, Goldsack, et al., 1999, 2Lota, Serra, et al., 1999Lota, Serra, et al., 1999Stashenko, Cervantes, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Carbowax 20MDB-WaxDB-WaxCarbowax 20MBP-20
Column length (m) 25.60.60.25.50.
Carrier gas H2HeHe He
Substrate      
Column diameter (mm) 0.250.320.320.250.22
Phase thickness (mum) 0.3  0.30.25
Tstart (C) 50.35.35.50.60.
Tend (C) 200.220.220.200.230.
Heat rate (K/min) 3.3.3.3.2.
Initial hold (min) 1.  1. 
Final hold (min) 20.  20.35.
I 2048.2040.2049.2046.2031.
ReferenceBicchi, Rubiolo, et al., 1998Brophy, Forster, et al., 1998Brophy, Goldsack, et al., 1998Bicchi, Fresia, et al., 1997Mariotti, Costa, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase Carbowax 20MHP-20MHP-FFAP
Column length (m) 60.50.50.
Carrier gas HeHeHe
Substrate    
Column diameter (mm) 0.320.250.25
Phase thickness (mum) 0.425  
Tstart (C) 45.60.60.
Tend (C) 300.190.210.
Heat rate (K/min) 3.3.3.
Initial hold (min) 3.  
Final hold (min) 20.  
I 2025.2009.2055.
ReferenceMondello, Dugo, et al., 1995Chung, Eiserich, et al., 1993Chung, Eiserich, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Boti, Koukoua, et al., 2007
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Choi, 2005
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Gancel, Ollitrault, et al., 2003
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Mau, Ko, et al., 2003
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Couladis, Chinou, et al., 2002
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Mondello, Zappia, et al., 2002
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Pino, Marbot, et al., 2002
Pino, J.A.; Marbot, R.; Vázquez, C., Characterization of volatile in Cosa Rican Guava [Psidium friedrichsthalianum (Berg) Niedenzu] fruit, J. Agric. Food Chem., 2002, 50, 21, 6023-6026, https://doi.org/10.1021/jf011456i . [all data]

Lota, Serra, et al., 2001
Lota, M.-L.; Serra, D.R.; Jacquemond, C.; Tomi, F.; Casanova, J., Chemical variability of peel and leaf essential oils of sour orange, Flavour Fragr. J., 2001, 16, 2, 89-96, https://doi.org/10.1002/1099-1026(200103/04)16:2<89::AID-FFJ950>3.0.CO;2-D . [all data]

Pino and Marbot, 2001
Pino, J.A.; Marbot, R., Volatile flavor constituents of acerola (Malpighia emarginata DC.) fruit, J. Agric. Food Chem., 2001, 49, 12, 5880-5882, https://doi.org/10.1021/jf010270g . [all data]

Pino, Marbot, et al., 2001
Pino, J.A.; Marbot, R.; Vázquez, C., Characterization of volatiles in strawberry guava (Psidium cattleianum Sabine) fruit, J. Agric. Food Chem., 2001, 49, 12, 5883-5887, https://doi.org/10.1021/jf010414r . [all data]

Brophy, Goldsack, et al., 2000
Brophy, J.J.; Goldsack, R.J.; Punruckvong, A.; Bean, A.R.; Forster, P.I.; Lepschi, B.J.; Doran, J.C.; Rozefelds, A.C., Leaf essential oils of the genus Leptospermum (Myrtaceae) in eastern Australia. Part 7. Leptospermum petersonii, L. liversidgei and allies, Flavour Fragr. J., 2000, 15, 5, 342-351, https://doi.org/10.1002/1099-1026(200009/10)15:5<342::AID-FFJ924>3.0.CO;2-V . [all data]

Chagonda, Makanda, et al., 2000
Chagonda, L.S.; Makanda, C.D.; Chalchat, J.-C., The essential oils of Ocimum canum Sims (basilic camphor) and Ocimum urticifolia Roth from Zimbabwe, Flavour Fragr. J., 2000, 15, 1, 23-26, https://doi.org/10.1002/(SICI)1099-1026(200001/02)15:1<23::AID-FFJ866>3.0.CO;2-W . [all data]

Choi and Sawamura, 2000
Choi, H.-S.; Sawamura, M., Composition of the essential oil of Citrus tamurana Hort. ex Tanaka (Hyuganatsu), J. Agric. Food Chem., 2000, 48, 10, 4868-4873, https://doi.org/10.1021/jf000651e . [all data]

Lota, de Rocca Serra, et al., 2000
Lota, M.-L.; de Rocca Serra, D.; Tomi, F.; Casanova, J., Chemical variability of peel and leaf essential oils of mandarins from Citrus reticulata Blanco, Biochem. Syst. Ecol., 2000, 28, 1, 61-78, https://doi.org/10.1016/S0305-1978(99)00036-8 . [all data]

Brophy, Goldsack, et al., 1999
Brophy, J.J.; Goldsack, R.J.; Punruckvong, A.; Forster, P.I., The leaf essential oils of Pilidiostigma (Myrtaceae), Flavour Fragr. J., 1999, 14, 2, 143-146, https://doi.org/10.1002/(SICI)1099-1026(199903/04)14:2<143::AID-FFJ798>3.0.CO;2-P . [all data]

Brophy, Goldsack, et al., 1999, 2
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Lota, Serra, et al., 1999
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Notes

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